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RESEARCH PAPER · ACS Catalysis · 2022

Disordered, Sub-Nanometer Ru Structures on CeO2 are Highly Efficient and Selective Catalysts in Polymer Upcycling by Hydrogenolysis

Linxiao Chen, Laura C. Meyer, Libor Kovařík, Debora Motta Meira, Xavier Isidro Pereira-Hernández, Honghong Shi, Konstantin Khivantsev, Oliver Y. Gutiérrez, János Szanyi

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Disordered, Sub-Nanometer Ru Structures on CeO2 are Highly Efficient and Selective Catalysts in Polymer Upcycling by HydrogenolysisOriginalHydrogenolysis of N-Eicosane Over Ru-Based Catalysts in a Continuous Flow Reactor13Plastic Waste Valorization by Leveraging Multidisciplinary Catalytic Technologies169Dual-Pathway Polyolefin Upcycling over an Unexpectedly Bifunctional Low-Loading Ru/TiO2-Anatase Catalyst54A general strategy and a consolidated mechanism for low-methane hydrogenolysis of polyethylene over ruthenium107Recycling and Upgrading Utilization of Polymer Plastics †34Role of Bifunctional Ru/Acid Catalysts in the Selective Hydrocracking of Polyethylene and Polypropylene Waste to Liquid Hydrocarbons172Ni/SiO2 catalysts for polyolefin deconstruction via the divergent hydrogenolysis mechanism121Near-zero-waste hydrogenolysis of poly(lactic acid) to biofuel9Rapid atom-efficient polyolefin plastics hydrogenolysis mediated by a well-defined single-site electrophilic/cationic organo-zirconium catalyst82Understanding the Structure–Activity Relationships in Catalytic Conversion of Polyolefin Plastics by Zeolite-Based Catalysts: A Critical Review269Catalytic hydroconversion processes for upcycling plastic waste to fuels and chemicals94Enhanced Production of Liquid Alkanes from Waste Polyethylene via the Electronic Effect‐Favored Csecondary−Csecondary Bond Cleavage42IrO2 clusters loaded on dendritic mesoporous silica nanospheres with superior peroxidase-like activity for sensitive detection of acetylcholinesterase and its inhibitors20Site-Selective Polyolefin Hydrogenolysis on Atomic Ru for Methanation Suppression and Liquid Fuel Production90Ruthenium Metal–Organic Frameworks as Stable Nanostructures for Selective Hydrogen Production from Acetaldehyde and Water under Mild Conditions4Strategic use of thermo-chemical processes for plastic waste valorization23Identifying selective catalysts in polypropylene hydrogenolysis by decoupling scission pathways31Ruthenium/TiO2‐Catalyzed Hydrogenolysis of Polyethylene Terephthalate: Reaction Pathways Dominated by Coordination Environment86Ruthenium/TiO2‐Catalyzed Hydrogenolysis of Polyethylene Terephthalate: Reaction Pathways Dominated by Coordination Environment29Recent Advances in Catalytic Chemical Recycling of Polyolefins104Boosting Polyethylene Hydrogenolysis Performance of Ru‐CeO2 Catalysts by Finely Regulating the Ru Sizes66Dynamic Evolution of Palladium Single Atoms on Anatase Titania Support Determines the Reverse Water–Gas Shift Activity82Investigating the impact of TiO2 crystalline phases on catalytic properties of Ru/TiO2 for hydrogenolysis of polyethylene plastic waste47A reusable, impurity-tolerant and noble metal–free catalyst for hydrocracking of waste polyolefins113A two-stage strategy for upcycling chlorine-contaminated plastic waste141Conversion of polyethylene waste to short chain hydrocarbons under mild temperature and hydrogen pressure with metal-free and metal-loaded MFI zeolites69Structure–Property Relationships for Nickel Aluminate Catalysts in Polyethylene Hydrogenolysis with Low Methane Selectivity61Efficient upcycling of high-density polyethylene into separable cyclic hydrocarbons1Upcycling of polyethylenes by catalysis0SMSI-induced charge transfer for selective hydrogenolysis of polyolefins76Two Mesoporous Domains Are Better Than One for Catalytic Deconstruction of Polyolefins62Enhanced production and control of liquid alkanes in the hydrogenolysis of polypropylene over shaped Ru/CeO2 catalysts23Investigating the influence of Ru structures and supports on hydrogenolysis of polyethylene plastic waste41Conversion of polyethylene to gasoline: Influence of porosity and acidity of zeolites14Controlling the selectivity of the hydrogenolysis of polyamides catalysed by ceria-supported metal nanoparticles26Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism14Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism5Thermodynamic and Kinetic Insights into Hydrogen Adsorption and Dissociation on the Ru (0001) Surface under STM and Catalytic Conditions11Influence of Pore Length on Hydrogenolysis of Polyethylene within a Mesoporous Support Architecture17Precise activation of C–C bonds for recycling and upcycling of plastics81Mechanistic understanding of metal–acid synergetic hydroconversion of polyethylene under mild conditions over a Ru/MOR catalyst22Consumer Grade Polyethylene Recycling via Hydrogenolysis on Ultrafine Supported Ruthenium Nanoparticles2Boosting strong metal-support interactions between Ru and sodium titanate nanowire for hydrogenolysis of polyolefins under mild conditions44Consumer Grade Polyethylene Recycling via Hydrogenolysis on Ultrafine Supported Ruthenium Nanoparticles38Direct amination of poly( p -phenylene oxide) to substituted anilines over bimetallic Pd–Ru catalysts13Synergistic catalysis for promoting selective C–C/C–O cleavage in plastic waste: structure–activity relationship and rational design of heterogeneous catalysts for liquid hydrocarbon production18Controlling Product Distribution of Polyethylene Hydrogenolysis Using Bimetallic RuM3 (M = Fe, Co, Ni) Catalysts28Review on Catalytic Depolymerization of Polyolefin Waste by Hydrogenolysis: State-of-the-Art and Outlook57Catalytic Hydrogenolysis of Polyethylene Under Reactive Separation46Hydrogen Production through Distinctive C−C Cleavage during Acetic Acid Reforming at Low Temperature6Size and Structure Effects of Carbon-Supported Ruthenium Nanoparticles on Waste Polypropylene Hydrogenolysis Activity, Selectivity, and Product Microstructure40Recent Progresses and Challenges in Upcycling of Plastics through Selective Catalytic Oxidation15Stable Interfacial Ruthenium Species for Highly Efficient Polyolefin Upcycling104Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes3Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes29Enhanced hydroconversion of polyethylene via dual-functional catalysis: Exploiting ZSM-22 pore-mouth catalysis and Ru electronic effect24Unlocking naphtha from polyolefins using Ni-based hydrocracking catalysts59Upcycling of Plastic Waste Using Photo-, Electro-, and Photoelectrocatalytic Approaches: A Way toward Circular Economy159Polystyrene Hydrogenolysis to High-Quality Lubricants Using Ni/SiO230Layered Double Hydroxide Derivatives for Polyolefin Upcycling103Oxidative Redispersion-Derived Single-Site Ru/CeO 2 Catalysts with Mobile Ru Complexes Trapped by Surface Hydroxyls Instead of Oxygen Vacancies91Upcycling of polyethylene to gasoline through a self-supplied hydrogen strategy in a layered self-pillared zeolite166Hydrogenolysis of Poly(Ethylene‐co‐Vinyl Alcohol) and Related Polymer Blends over Ruthenium Heterogeneous Catalysts7Pt enhanced C–H bond activation for efficient and low-methane-selectivity hydrogenolysis of polyethylene over alloyed RuPt/ZrO264Hydrogen Spillover Is Regulating Minority Rh1 Active Sites on TiO2 in Room-Temperature Ethylene Hydrogenation7A US perspective on closing the carbon cycle to defossilize difficult-to-electrify segments of our economy60Selective Upcycling of Polyethylene over Ru/H‐ZSM‐5 Bifunctional Catalyst into High‐Quality Liquid Fuel at Mild Conditions31Recent advances in polyolefinic plastic pyrolysis to produce fuels and chemicals60Recent progress of waste plastic upcycling based on multifunctional zeolite catalysts13Chemical Upcycling of Polyolefin Plastics Using Structurally Well-defined Catalysts35Polyethylene hydrogenolysis over bimetallic catalyst with suppression of methane formation15Selective Hydrodeoxygenation of Lignin‐Derived Phenolic Monomers to Cyclohexanol over Tungstated Zirconia Supported Ruthenium Catalysts27Creating CoRu Dual Active Sites Codecorated Stable Porous Ceria Support for Enhanced Li–CO 2 Batteries Cathodes10Economically attractive production of commercial-grade gasoline from waste plastics1Chemical Upcycling of Polylactic Acid Plastic Waste into Alanine over Ru/CeO 2 with Decoration of Indium20PP upcycling employing FCC spent catalyst: The role of contaminants, atmosphere and pressure5Unlocking opportunities: Supported metal catalysts for the chemical upcycling of waste plastics26Parameter selection for the hydroconversion of waste polyethylene plastic under mild conditions: A comprehensive evaluation8Catalytic Approaches to Tackle Mixed Plastic Waste Challenges: A Review27Constructing the Al deficiency in Si-O(H)-Al units based on Pt/ZSM-5 for enhanced hydrocracking of polyethylene into high-quality liquid fuel20Catalytic Upcycling of Polyolefins316The role of size and structure of catalytic active sites in polyolefin hydrogenolysis12Selective Hydrogenolysis Conversion of Polyethylene into Alkyl Oil Over Iridium‐based Catalyst9Catalytic recycling of plastics into value-added products28Alanine Production by Chemical Upcycling of Polylactic Acid Waste Over Fe‐Doped Ru/CeO210Plasmonic Copper‐Ruthenium Superstructure for Efficient Photothermal Conversion and Plastic Recycling39One-pot catalytic conversion of polyethylene wastes to gasoline through a dual-catalyst system41Production of Branched Alkanes by Upcycling of Waste Polyethylene over Controlled Acid Sites of SO 4 /ZrO 2 ‐Al 2 O 3 Catalyst27Production of Branched Alkanes by Upcycling of Waste Polyethylene over Controlled Acid Sites of SO 4 /ZrO 2 ‐Al 2 O 3 Catalyst6Hydrogen-free upcycling of polyethylene waste to methylated aromatics over Ni/ZSM-5 under mild conditions19Efficient Hydrogenolysis of Consumer-Grade High-Density Polyethylene Wastes over MgAl-Layered Double Oxide-Supported Ru Catalysts11Unraveling the role of water in mechanism changes for economically viable catalytic plastic upcycling43Polyethylene hydrogenolysis by dilute RuPt alloy to achieve H2-pressure-independent low methane selectivity70Elucidating the effect of nanocube support morphology on the hydrogenolysis of polypropylene over Ni/CeO 2 catalysts7Current methods for plastic waste recycling: Challenges and opportunities64Induction Heating for the Electrification of Catalytic Processes51Reaction engineering of the hydrogenolysis of liquid n-Alkanes: Comparison of flow and batch reaction systems2Effective production of liquid/wax fuels from polyethylene plastics using Ru/Al 2 O 3 catalysts10Highly energy-efficient hydrogenolysis of high-density polyethylene via hydrogen nonthermal plasma reaction engineering4Hydrocracking of polyolefins over ceria-promoted Ni/BEA catalysts23Hydrogen/solvent-free plastic valorization via loosely coordinated ruthenium sites steering selective aromatization7Low temperature polyolefin deconstruction via tandem cracking-hydrogenation2Recent developments in recycling of post-consumer polyethylene waste33Surface-confined growth of Ru amorphous sub-nanoclusters on reductive Mn 3 O 4 : a strongly coupled interface engineering for efficient neutral hydrogen production62Synergistic effect of acidic sites and mesoporous confinement in Ce-doped Ru/SBA-15 catalysts for efficient hydrogenolysis of low-density polyethylene to liquid fuels7Upgrading of waste polyolefins with non-noble metal catalysts21Conversion of Polypropylene to Light Olefins by HMFI Catalysts below Pyrolytic Temperature: Catalytic, Spectroscopic, and Theoretical Studies3Mechanistic Insights into Polypropylene Hydrogenolysis Using Ni/Al2O3 Catalysts17Hydrocracking of polyethylene to high quality liquid fuels over bimetallic catalyst PdAg/HZSM-58Investigation on polyethylene hydrogenolysis over a nickel catalyst via ReaxFF molecular dynamic simulation5Sequential hydrogenation enhanced by bidirectional hydrogen spillover over cascade catalyst2Effective Methane Suppression in Upcycling of Polyethylene into Fuels via Alloying Platinum with Ruthenium Supported on ZSM-5 Zeolite17Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis25Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis2Efficient Upcycling of Polyolefin Waste to Light Aromatics via Coupling C─C Scission and Carbonylation26Efficient Upcycling of Polyolefin Waste to Light Aromatics via Coupling C─C Scission and Carbonylation5Upgrading polyolefin plastics: experiences from petroleum refining and distinct characteristics19Reductive Upcycling of Polyolefins, Polyesters and Mixed Plastic Wastes to Valuable Chemicals: Bridging Chemical Catalysis With Plastic Waste Management35Conversion of Compositionally Diverse Plastic Waste over Earth-Abundant Sulfides26Upcycling polyolefins to methane-free liquid fuel by a Ru1-ZrO2 catalyst47Hydrocracking of Polyethylene to Gasoline-Range Hydrocarbons over a Ruthenium-Zeolite Bifunctional Catalyst System with Optimal Synergy of Metal and Acid Sites9Ru-Catalyzed Polyethylene Hydrogenolysis under Quasi-Supercritical Conditions25Enhancing Waste Plastic Hydrogenolysis on Ru/CeO 2 Through Concurrent Incorporation of Fe Single Atoms and FeO x Nanoclusters27Enhancing Waste Plastic Hydrogenolysis on Ru/CeO 2 Through Concurrent Incorporation of Fe Single Atoms and FeO x Nanoclusters4Co-recycling of plastics and other waste materials70Predicting a generalized mechanism of branched alkane hydrogenolysis on Ru, Ir, and Pt surfaces relevant to polymer upcycling applications3Recent Advances in the Thermo-Catalytic Upcycling of Polyethylene Waste13Polyethylene Hydrogenolysis over Ru Supported on Mesoporous MFI Zeolite: Effects of Mesoporosity and External Acid Sites16In-line NMR guided orthogonal transformation of real-life plastics63Plastic-waste hydrogenolysis over two-dimensional MXene-supported ruthenium catalysts with tunable interlayer spacing3Ni/Nb2O5 as a noble-metal-free catalyst for the chemical upcycling of waste polyolefin plastics9Methods for Carbon Mass Closure in Polyolefin Hydrocracking6Poisoning effects of impurities on hydrogenolysis of polyethylenes over supported Ru catalysts3Tuning Catalytic Reactivity via Wetting Control through Oxygen Vacancies: Ru Clusters on Anatase TiO2 and CeO2 Supports22Tandem Catalysis to Mitigate Coke Formation in the Upcycling of Mixed Polyolefin Wastes11CO-promoted polyethylene hydrogenolysis with renewable formic acid as hydrogen donor20The silent partner in catalysis: How support architectures dictate efficiency in polyolefin hydrogenolysis1Stable single-site organonickel catalyst preferentially hydrogenolyses branched polyolefin C–C bonds12Catalytic Depolymerization of Plastics to Valuable Products7Chemical recycling of polyethylenes with low gas products by catalytic hydrogenolysis with heterogeneous CeO2-supported Cu-doped Ru catalyst5Polymer Upcycling by Catalytic Hydrogenolysis: The Role of Polyolefin Short-Chain Branching3Orchestrating catalytic hotspots and macromolecular architectures: molecular engineering toward zero-waste polymer circularity4Fine regulation of Ru species improved the polyethylene hydrogenolysis performance over Ru/Al 2 O 3 catalyst5Hydrogen-Free Catalytic Strategies for the Upcycling of Polyolefin Plastics3Synergy Effects in a Bimetallic Ru ─ Pt Alloy Catalyst for Low‐H 2 ‐Pressure Hydrogenolysis of Low‐Density Polyethylene3Polyethylene hydrogenolysis to liquid products over bimetallic catalysts with favorable environmental footprint and economics17Unraveling the nitrate-mediated Mars-van Krevelen mechanism in NO oxidation over single-site Ru1-modified CeO2 and Pr6O11: Roles of oxygen vacancy dynamics7Advances of rare earth-based catalysts for recycling CO 2 and plastic waste17Selective Hydrocracking of Polyethylene to Gasoline Over Bi‐Functional Ir/HBEA Catalysts Under Mild Condition2Surface and Interface Properties of Metal Species for Waste Plastic Hydroconversion6

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  1. Hydrogenolysis of N-Eicosane Over Ru-Based Catalysts in a Continuous Flow Reactor

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  4. A general strategy and a consolidated mechanism for low-methane hydrogenolysis of polyethylene over ruthenium

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  5. Recycling and Upgrading Utilization of Polymer Plastics †

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  7. Ni/SiO2 catalysts for polyolefin deconstruction via the divergent hydrogenolysis mechanism

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  10. Understanding the Structure–Activity Relationships in Catalytic Conversion of Polyolefin Plastics by Zeolite-Based Catalysts: A Critical Review

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  16. Strategic use of thermo-chemical processes for plastic waste valorization

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  17. Identifying selective catalysts in polypropylene hydrogenolysis by decoupling scission pathways

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  30. SMSI-induced charge transfer for selective hydrogenolysis of polyolefins

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  31. Two Mesoporous Domains Are Better Than One for Catalytic Deconstruction of Polyolefins

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  32. Enhanced production and control of liquid alkanes in the hydrogenolysis of polypropylene over shaped Ru/CeO2 catalysts

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  33. Investigating the influence of Ru structures and supports on hydrogenolysis of polyethylene plastic waste

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  34. Conversion of polyethylene to gasoline: Influence of porosity and acidity of zeolites

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  35. Controlling the selectivity of the hydrogenolysis of polyamides catalysed by ceria-supported metal nanoparticles

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  36. Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism

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  37. Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism

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  39. Influence of Pore Length on Hydrogenolysis of Polyethylene within a Mesoporous Support Architecture

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  40. Precise activation of C–C bonds for recycling and upcycling of plastics

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  41. Mechanistic understanding of metal–acid synergetic hydroconversion of polyethylene under mild conditions over a Ru/MOR catalyst

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  42. Consumer Grade Polyethylene Recycling via Hydrogenolysis on Ultrafine Supported Ruthenium Nanoparticles

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  43. Boosting strong metal-support interactions between Ru and sodium titanate nanowire for hydrogenolysis of polyolefins under mild conditions

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  44. Consumer Grade Polyethylene Recycling via Hydrogenolysis on Ultrafine Supported Ruthenium Nanoparticles

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