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RESEARCH PAPER · ACS Catalysis · 2022

Role of Bifunctional Ru/Acid Catalysts in the Selective Hydrocracking of Polyethylene and Polypropylene Waste to Liquid Hydrocarbons

Julie E. Rorrer, Amani M. Ebrahim, Ydna M. Questell‐Santiago, Jie Zhu, Clara Troyano-Valls, Arun S. Asundi, Anna E. Brenner, Simon R. Bare, Christopher J. Tassone, Gregg T. Beckham, Yuriy Román‐Leshkov

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Role of Bifunctional Ru/Acid Catalysts in the Selective Hydrocracking of Polyethylene and Polypropylene Waste to Liquid HydrocarbonsOriginalDual-Pathway Polyolefin Upcycling over an Unexpectedly Bifunctional Low-Loading Ru/TiO2-Anatase Catalyst54Catalytic hydroconversion processes for upcycling plastic waste to fuels and chemicals94Enhanced Production of Liquid Alkanes from Waste Polyethylene via the Electronic Effect‐Favored Csecondary−Csecondary Bond Cleavage42Recent Advances in Catalytic Chemical Recycling of Polyolefins104Zeolite Supported Pt for Depolymerization of Polyethylene by Induction Heating18Conversion of polyethylene waste to short chain hydrocarbons under mild temperature and hydrogen pressure with metal-free and metal-loaded MFI zeolites69Ni/HZSM-5 catalysts for hydrodeoxygenation of polycarbonate plastic wastes into cycloalkanes for sustainable aviation fuels77Hydrogen-free catalytic depolymerization of waste polyolefins at mild temperatures43Upcycling of polyethylenes by catalysis0Treasuring trash: Pt/SrTiO3 catalysts process plastic waste into high-value materials25Investigating the influence of Ru structures and supports on hydrogenolysis of polyethylene plastic waste41Quantifying synergy for mixed end-scission and random-scission catalysts in polymer upcycling12Toward Intrinsic Catalytic Rates and Selectivities of Zeolites in the Presence of Limiting Diffusion and Deactivation50Boosting the catalytic performance of metal–zeolite catalysts in the hydrocracking of polyolefin wastes by optimizing the nanoscale proximity56Thermochemical degradation of agricultural mulch films for potential organic fertilizer precursors: Low-temperature pyrolysis in nitric acid4Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism14Rapid Polyolefin Hydrogenolysis by a Single‐Site Organo‐Tantalum Catalyst on a Super‐Acidic Support: Structure and Mechanism5End-of-Life Plastics Management: A Review7Total revalorization of high impact polystyrene (HIPS): enhancing styrene recovery and upcycling of the rubber phase33Thermodynamic and Kinetic Insights into Hydrogen Adsorption and Dissociation on the Ru (0001) Surface under STM and Catalytic Conditions11Chemical recycling of plastic wastes via homogeneous catalysis: A review78Precise activation of C–C bonds for recycling and upcycling of plastics81Mechanistic understanding of metal–acid synergetic hydroconversion of polyethylene under mild conditions over a Ru/MOR catalyst22Valorisation of Plastic Waste via Catalytic Hydrocracking: a Technological Survey4Rapid Polyolefin Plastic Hydrogenolysis Mediated by Single-Site Heterogeneous Electrophilic/Cationic Organo-group IV Catalysts19Direct amination of poly( p -phenylene oxide) to substituted anilines over bimetallic Pd–Ru catalysts13Synergistic catalysis for promoting selective C–C/C–O cleavage in plastic waste: structure–activity relationship and rational design of heterogeneous catalysts for liquid hydrocarbon production18Silica as support and binder in bifunctional catalysts with ultralow Pt loadings for the hydroconversion of n-alkanes3Polyethylene Upgrading to Liquid Fuels Boosted by Atomic Ce Promoters74Polyethylene Upgrading to Liquid Fuels Boosted by Atomic Ce Promoters21Catalytic Strategies for the Upcycling of Polyolefin Plastic Waste30The catalytic pyrolysis of waste polyolefins by zeolite-based catalysts: A critical review on the structure-acidity synergies of catalysts47Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes3Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes29High-efficiency Ce-modified ZSM-5 nanosheets for waste plastic upgrading43Enhanced hydroconversion of polyethylene via dual-functional catalysis: Exploiting ZSM-22 pore-mouth catalysis and Ru electronic effect24Unlocking naphtha from polyolefins using Ni-based hydrocracking catalysts59Catalytic hydrogenolysis of polypropylene and polyethylene mixtures: Effect of temperature on liquid alkane components18Hierarchical FAU Zeolites Boosting the Hydrocracking of Polyolefin Waste into Liquid Fuels38Catalytic Consequences of Hierarchical Pore Architectures within MFI and FAU Zeolites for Polyethylene Conversion54Selective Upcycling of Polyethylene over Ru/H‐ZSM‐5 Bifunctional Catalyst into High‐Quality Liquid Fuel at Mild Conditions31Recent progress of waste plastic upcycling based on multifunctional zeolite catalysts13Influence of Autoclave Liner on Polyethylene Hydrogenolysis Selectivity7Polyethylene hydrogenolysis over bimetallic catalyst with suppression of methane formation15Recent advances in polyolefin plastic waste upcycling via mild heterogeneous catalysis route from catalyst development to process design25Active species in chloroaluminate ionic liquids catalyzing low-temperature polyolefin deconstruction22Unlocking opportunities: Supported metal catalysts for the chemical upcycling of waste plastics26Parameter selection for the hydroconversion of waste polyethylene plastic under mild conditions: A comprehensive evaluation8Catalytic Approaches to Tackle Mixed Plastic Waste Challenges: A Review27Catalytic Synergy between Lewis Acidic Alumina and Pt in Hydrodechlorination for Plastic Chemical Recycling38Catalytic Upcycling of Polyolefins316Selective Hydrogenolysis Conversion of Polyethylene into Alkyl Oil Over Iridium‐based Catalyst9Catalytic recycling of plastics into value-added products28Pore-Structure Engineering of Hierarchical β Zeolites for the Enhanced Hydrocracking of Waste Plastics to Liquid Fuels51Role of Bifunctional Metal-Promoted Zeolitic Catalyst in Microwave-Assisted Pyrolysis of Polyethylene to Monocyclic Aromatics21Selective catalytic conversion of model olefin and diolefin compounds of waste plastic pyrolysis oil: Insights for light olefin production and coke minimization25Hydroconversion of waste polyethylene plastics under mild conditions using mechanically mixed bifunctional catalysts: Impact of metal-acid balance and proximity9Hydrogen-free upcycling of polyethylene waste to methylated aromatics over Ni/ZSM-5 under mild conditions19An in Silico Investigation into Polyester Adsorption onto Alumina toward an Improved Understanding of Hydrogenolysis Catalysts1Efficient Hydrogenolysis of Consumer-Grade High-Density Polyethylene Wastes over MgAl-Layered Double Oxide-Supported Ru Catalysts11Unraveling the role of water in mechanism changes for economically viable catalytic plastic upcycling43Polyethylene hydrogenolysis by dilute RuPt alloy to achieve H2-pressure-independent low methane selectivity70Kinetic Models for Polymer Upcycling by Tag-and-Cut Strategies6Advances and Challenges for Catalytic Recycling and Upgrading of Real-World Mixed Plastic Waste100Complementary acid site mechanisms in hydrogen-free polyethylene upcycling: elucidating the distinct roles of Brønsted and Lewis sites in Ce-modified zeolites14Computational insights into hydrogen interaction with the Ru (1011) and Ru (1010) surfaces: implications for alkane and polyolefin hydrogenolysis1Enhancing liquified petroleum gas selectivity through hierarchical porosity in MWW-type MCM-49 zeolite for polyethylene hydrocracking0Hydrocracking of polyolefins over ceria-promoted Ni/BEA catalysts23Low temperature polyolefin deconstruction via tandem cracking-hydrogenation2Selective hydrocracking of polyolefin waste into branched liquid fuels over a non-noble metal bifunctional Ni–W/ZrO 2 catalyst4Catalytic and engineering strategies for enhanced hydrogenation reactions: A review of heterogeneous catalysts and process optimization15Hydrocracking of polyethylene to high quality liquid fuels over bimetallic catalyst PdAg/HZSM-58Recent advancements in upcycling of polyolefins by hydrocracking: Effect of various heterogeneous catalysts and reaction parameters8Effects of Pretreatment Conditions and Branched Alkanes on Mo/MCM-41 Catalysts in Tandem Alkane Cross-metathesis for Non-hydrogen Polyolefin Recycling3Effective Methane Suppression in Upcycling of Polyethylene into Fuels via Alloying Platinum with Ruthenium Supported on ZSM-5 Zeolite17Catalytic deconstruction of organic additive-containing plastics44Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis25Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis2Reductive Upcycling of Polyolefins, Polyesters and Mixed Plastic Wastes to Valuable Chemicals: Bridging Chemical Catalysis With Plastic Waste Management35The role of the Pt-group dehydrogenation catalyst in alkane metathesis for polyolefin deconstruction9Optimization of low-temperature catalytic cracking of polyolefin waste in open-batch reactors using zeolite beta with controlled intrinsic properties20Tailored Ru Catalysts on Gamma Alumina: Enhancing Polyethylene Hydrogenolysis for High-Value Liquid Fuel Production10Upcycling of Waste Plastics into Value-Added Chemicals6Hydrocracking of Polyethylene to Gasoline-Range Hydrocarbons over a Ruthenium-Zeolite Bifunctional Catalyst System with Optimal Synergy of Metal and Acid Sites9Polyolefin Recycling with Binary Cobalt–Nickel Nanosheets6Zeolites in the epoch of catalytic recycling plastic waste: Toward circular economy and sustainability20Advances in catalytic transformations of waste plastic resources with zeolites0Ru-Catalyzed Polyethylene Hydrogenolysis under Quasi-Supercritical Conditions25Synergistic Catalysis for Recycling and Upcycling of Plastics35Coordinating cracking and hydrogenation of polyethylene waste via acid-metal site isolation for selective hydrocarbon production10Catalytic Transformation of LDPE into Aromatic-Rich Fuel Oil2Molecular conversion of polypropylene pyrolysis revealed by Ag+ complexation ESI Orbitrap MS0One-Step Production of Isoalkane-Rich Sustainable Aviation Fuel Fractions via Catalytic Pyrolysis of Low-Density Polyethylene over Y-Type Zeolite10Polyethylene Hydrogenolysis over Ru Supported on Mesoporous MFI Zeolite: Effects of Mesoporosity and External Acid Sites16Phase Selective Synthesis of SBT and FAU‐SBT‐SBS Intergrown Zeolites Using Asymmetric Organic Structure‐Directing Agents for Upgrading of Polyethylene Pyrolysis Oil1Optimizing Olefin Production in Microwave Slurry Catalytic Pyrolysis of Low-Density Polyethylene4Methods for Carbon Mass Closure in Polyolefin Hydrocracking6Integrated low-temperature PVC and polyolefin upgrading38Dual-catalyst system without supported metals toward polyethylene waste upcycling3Stable single-site organonickel catalyst preferentially hydrogenolyses branched polyolefin C–C bonds12Closed-loop recycling of polyethylene to ethylene and propylene via a kinetic decoupling–recoupling strategy32Hydrogen-Free Catalytic Strategies for the Upcycling of Polyolefin Plastics3Synergy Effects in a Bimetallic Ru ─ Pt Alloy Catalyst for Low‐H 2 ‐Pressure Hydrogenolysis of Low‐Density Polyethylene3Water-Modulated Ru Catalysis: Overcoming the Activity-Selectivity Trade-Off in C–O Bond Cleavage1Plasma Catalysis for Plastic Waste Conversion into Value‐Added Products: Advancements and Perspectives11Polyethylene hydrogenolysis to liquid products over bimetallic catalysts with favorable environmental footprint and economics17TiO 2 ‐Supported Ru–Fe Catalysts for the Hydrodeoxygenation of Bis(2‐hydroxyethyl) Terephthalate (BHET) Prepared by the Glycolysis of Polyethylene Terephthalate (PET)1Recent advancement on heterogeneous metal catalysts for the upgradation of polyethylene terephthalate plastic waste into bis(2-hydroxyethyl) terephthalate2A review of recent advances in thermal-catalytic cracking of plastic waste8Surface and Interface Properties of Metal Species for Waste Plastic Hydroconversion6Selective polyethylene hydrocracking to liquid and gaseous hydrocarbons over Co–Ni catalysts supported on H-BEA zeolite10Intrinsically Bifunctional and Tunable Tungsten Carbide Catalysts Enable Efficient PVC-Compatible Polyolefin Hydrocracking8Synergy between acidity and Pt in Pt/HY zeolite for boosting the hydrocracking of polyethylene to C5-C7 liquid fuels0Single-Atom Ni on Tungsten Oxides Drives Hydrogen Spillover for Efficient Plastic Waste Upcycling13Sustainable polyolefin upcycling using liquid organic hydrogen carrier based hydrogen delivery and hydrocracking11A self-regenerative Sn–W/γ-Al 2 O 3 catalyst for low-carbon and scalable polyolefin upcycling via tandem dehydrogenation–metathesis2Acidified montmorillonite (MMT)-supported ultrafine Ru nanoparticles for polyethylene plastic upcycling0Benchmarking electro-Fenton-driven decomposition of synthetic polymers0Carbon–carbon bond cleavage for lignin and plastics deconstruction0Catalytic solvothermal liquefaction of mixed polyolefin waste over USY-based zeolites: Selectivity, kinetics, and reusability0Catalytic solvothermal liquefaction of mixed polyolefin waste over USY-based zeolites: Selectivity, kinetics, and reusability0Catalytic solvothermal upcycling of mixed polyolefin waste into gasoline-range liquid fuels: solvent-assisted selectivity and coke kinetics over USY zeolite0Constructing Ru–O–Nb interfaces in RuO x /NbOPO 4 nanosheets for the one-pot conversion of lignin-derived phenol and benzyl alcohol to polycycloalkane aviation biofuels2Enhancing aromatic yield by zeolites in polypropylene hydrocracking to jet fuel over Ru 1 -ZrO 2 without forming CH 40Enhancing selectivity and yield in polyethylene hydrogenolysis using goal-aware Bayesian algorithm execution0Highly selective hydrocracking of polypropylene to gasoline-range fuels over the Pt/MCM-22 catalyst0Highly selective production of gasoline-range hydrocarbons via hydroconversion of polyolefins over Ru/CeO 2 and BEA hybrid catalysts0Plastic Waste Conversion into Monomers Using Microwaves0Tuning ruthenium states for enhanced polyethylene hydroconversion over HZSM-5 catalysts0Enhancing Hydrogen Spillover via Crystalline-Phase Engineering of Ru/ZrO 2 for Selective Liquid Alkane Production in Polyethylene Hydrogenolysis6Mild‐Condition Upcycling of Polyolefins Enabled by Micropore Confinement in Zeolites3Mild‐Condition Upcycling of Polyolefins Enabled by Micropore Confinement in Zeolites5Acid sites in hydrogen-involved polyolefin upcycling: mechanistic insights and design principles0Efficient polyolefin upcycling to liquid fuels via Ru–zeolite physical mixtures and pathway control2Selective Conversion of Polyolefin Waste to Branched Alkanes via Methane‐Free Tandem Hydrocracking–Isomerization2Hydrocracking Polyolefins to Jet Fuel over a NiW/WO x Catalyst2Rational design of bifunctional catalysts for hydrocracking of polyethylene waste plastics to narrow-distributed liquid fuels4Synergistic bifunctional catalysis and plasma activation for valorizing polypropylene and CO2 to gasoline-range olefins1Recent advancements in catalytic processes for plastic upcycling into fuels: a major step in sustainable waste management and energy production3Thermo-chemical upgrading of waste polyethylene and polypropylene plastics0Hydrogenolysis Versus Hydrocracking for Polyolefin Upcycling0Polymer Deconstruction and Redesign Strategies for Plastics Recycling0Preparing methane‐resistant Ru catalysts via moderate metal‐support interactions for polyethylene hydrogenolysis0Shape-Selective Conversion of High-Density Polyethylene into Benzene with Zeolite-Encapsulated Subnanometer Pt Catalysts6Techno-economic analysis and life cycle assessment for the catalytic hydrogenolysis and hydrocracking of polyethylene6Compressed CO 2 -Assisted Catalytic Hydrocracking of Polyethylene over Ru-Loaded Zeolites0Catalytic Upcycling of Polyolefins and Polystyrene: Integrating Active Site Design With Mass Transfer Considerations4Beyond Recycling: Vitrimer and Chemical Valorization Strategies for Thermoplastic Polyolefin Upcycling0Highly Selective Gasoline Production by Polyethylene Hydrogenolysis Using Ternary RuNiPt Nanoalloy Catalyst1iPDA-Assisted Design of Hierarchical Beta Zeolites for the Sustainable Upcycling of Polyethylene to Naphtha with Ultra-Low Pt Loading1

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  42. Recent progress of waste plastic upcycling based on multifunctional zeolite catalysts

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