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RESEARCH PAPER · Inorganic Chemistry · 2002

From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds

Paul A. Maggard, Amy L. Kopf, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier, Kang Min Ok, P. Shiv Halasyamani

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From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) CompoundsOriginalCadmium and Mercury23Salt-Inclusion Synthesis of Ba2MnSi2O7Cl. A Fresnoite-Type Polar Framework Containing the Acentric [Si2O7]6- Polyanion in the Anti-ReO3 Type [(Ba2Mn)Cl]6+ Cage39Hydrothermal synthesis and structure of [Ni(tpyrpyz)2]2[Mo4O12F2][Mo6O19] · 2H2O, a material exhibiting an unusual tetranuclear polyoxofluoromolybdate cluster [Mo4O12F2]2−35Probing helix formation in chains of vertex-linked octahedra44A 3D silver coordination polymer with novel topology structure17Organic–inorganic hybrid materials constructed from copper-organoimine subunits and molybdoarsonate clusters60New trends in crystal engineering412Polar ordering of polar octahedra in [C2N2H10][VOF4(H2O)]40Water-assisted self-assembly of harmonic single and triple helices in a polymeric coordination complex61Examining the Out-of-Center Distortion in the [NbOF5]2- Anion271New d0 Transition Metal Iodates: Synthesis, Structure, and Characterization of BaTi(IO3)6, LaTiO(IO3)5, Ba2VO2(IO3)4·(IO3), K2MoO2(IO3)4, and BaMoO2(IO3)4·H2O64Salt-Inclusion Synthesis of Two New Polar Solids, Ba6Mn4Si12O34Cl3 and Ba6Fe5Si11O34Cl344Synthesis and Characterization of the Face-Sharing Bioctahedral [Mo2O6F3]3- Anion23Synthesis and properties of pyrazine-pillared Ag3Mo2O4F7 and AgReO4 layered phases13Phase transitions in oxyfluoride (NH4)2WO2F416A Novel Chiral Cd(II) Coordination Polymer Based on Achiral Unsymmetrical 3-Amino-1,2,4-triazole with an Unprecedented μ4-Bridging Mode117Homochiral metal–organic coordination networks from l-typtophan14Metallacycles of Iron, Zinc, and Cadmium Assembled by Polytopic Bis(pyrazolyl)methane Ligands and Fluoride Abstraction from BF4-59Syntheses, Structures, and Magnetic Properties of Mononuclear CuIIand Tetranuclear CuII3MII(M = Cu, Co, or Mn) Compounds Derived fromN,N‘-Ethylenebis(3-ethoxysalicylaldimine): Cocrystallization Due to Potential Encapsulation of Water138Binuclear Fluoro-Bridged Zinc and Cadmium Complexes of a Schiff Base Expanded Porphyrin: Fluoride Abstraction from the Tetrafluoroborate Anion77A Novel Helical Double-Layered Cobalt(II)−Organic Framework with Tetranuclear [Co4(μ3-OH)2] Clusters Linked by an Unsymmetrical Pyridylbenzoate Ligand84A new hybrid framework based on a ‘superoctahedral’ [V7O6F30]14− polyanion14Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?0Spontaneous Resolution of Chiral Polyoxometalate‐Based Compounds Consisting of 3D Chiral Inorganic Skeletons Assembled from Different Helical Units124Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F429Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions21New Inorganic Helical Chain: Synthesis, Structure, Characterization, and Interconversion of BaGa2O2(OH)44Magnetoelastic Coupling through the Antiferromagnet-to-Ferromagnet Transition of Quasi-Two-Dimensional [Cu(HF2)(pyz)2]BF4 Using Infrared Spectroscopy28Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids34Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F416pH-Tuned self-assembly of organic–inorganic hybrids based on different vanadate chains, Zn( ii ) ions and flexible ligands: crystallizing in polar and centrosymmetric space group28“Fluoride molecular scissors”: A rational construction of new Mo(VI) oxofluorido/1,2,4-triazole MOFs16Investigation of Trimetallic Ligand-Pillared Oxyfluorides: Ag2Cu(pzc)2MO x F6−x (M = Mo, Nb, and W)1Orientational order of [VOF5]2− and [NbOF5]2− polar units in chains40Syntheses, Structures Tuned by 4,4′-Bipyridine and Magnetic Properties of a Series of Transition Metal Compounds Containing o-Carboxylphenoxyacetate Acid40Raman spectroscopic study of the lattice dynamics in the Rb2KMoO3F3 oxyfluoride10Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State21From Racemic Units to Polar Materials23Unprecedented Trapping of Difluorooctamolybdate Anions within an α-Polonium Type Coordination Network13Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model16Synthesis and crystal structures of (pyH)2[Mo2O4F6] and (pipH2)[Mo2O4F6]; vibrational band assignment for [Mo2O4F6]2− anion4Measurement of Raman-Scattering Spectra of Rb2KMoO3F3 Crystal: Evidence for Controllable Disorder in the Lattice Structure28Na 2 MoO 2− δ F 4+ δ – a perovskite with a unique combination of atomic orderings and octahedral tilts7On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units55A Nearly Ideal One-Dimensional S = 5/2 Antiferromagnet FeF3(4,4′-bpy) (4,4′-bpy =4,4′-bipyridyl) with Strong Intrachain Interactions51Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships16Cyclohexylammonium sulfanilate: A simple representative of the chiral materials containing only achiral building units8Effect of Deuteration on Phase Transitions in Vanadium Dioxotetrafluoride2Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands9Periodic Tendril Perversion and Helices in the AMoO2F3 (A = K, Rb, NH4, Tl) Family44Rare example of chiral and achiral polymorphs of a metal-oxide/organic hybrid compound2Ba(MoO 2 F) 2 (QO 3 ) 2 (Q = Se, Te): Partial Fluorination of MoO 6 Octahedra Enabling Two Polar Solids with Strong and Phase Matchable SHG Response69Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship24Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph31RACEMIC TWINNING OF 7-CHLORINE-2,3,4a,6- TETRAHYDROFURO[2,3-b][1,4]OXATHIIN-6-ONE CRYSTALS3The First Sulfate‐Pillared Hybrid Ultramicroporous Material, SOFOUR‐1‐Zn, and Its Acetylene Capture Properties7The First Sulfate‐Pillared Hybrid Ultramicroporous Material, SOFOUR‐1‐Zn, and Its Acetylene Capture Properties66Novel layered heterobimetallic fluorides with large optical band gaps3Prediction of Large Second Harmonic Generation in the Metal-Oxide/Organic Hybrid Compound CuMoO3(p2c)2Mixed anion materials0Metal-organic frameworks for C2H2/CO2 separation: Recent development146Construction of Ideal One-Dimensional Spin Chains by Topochemical Dehydration/Rehydration Route13

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  1. Cadmium and Mercury

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  2. Salt-Inclusion Synthesis of Ba2MnSi2O7Cl. A Fresnoite-Type Polar Framework Containing the Acentric [Si2O7]6- Polyanion in the Anti-ReO3 Type [(Ba2Mn)Cl]6+ Cage

    Inorganic Chemistry · 2003-05-30

    Xunhua Mo, Shiou‐Jyh Hwu

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  3. Hydrothermal synthesis and structure of [Ni(tpyrpyz)2]2[Mo4O12F2][Mo6O19] · 2H2O, a material exhibiting an unusual tetranuclear polyoxofluoromolybdate cluster [Mo4O12F2]2−

    Inorganica Chimica Acta · 2003-09-16

    Eric M. Burkholder, Jon Zubieta

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  4. Probing helix formation in chains of vertex-linked octahedra

    CrystEngComm · 2004-01-01

    Paul A. Maggard, Amy L. Kopf, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  5. A 3D silver coordination polymer with novel topology structure

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    Shoubo Qin, Sheming Lu, Yanxiong Ke, Jianmin Li, Xintao Wu, Wen‐Xin Du

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  6. Organic–inorganic hybrid materials constructed from copper-organoimine subunits and molybdoarsonate clusters

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  7. New trends in crystal engineering

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  8. Polar ordering of polar octahedra in [C2N2H10][VOF4(H2O)]

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  9. Water-assisted self-assembly of harmonic single and triple helices in a polymeric coordination complex

    Chemical Communications · 2005-01-01

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  10. Examining the Out-of-Center Distortion in the [NbOF5]2- Anion

    Inorganic Chemistry · 2005-01-20

    Heather K. Izumi, Janet E. Kirsch, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  11. New d0 Transition Metal Iodates: Synthesis, Structure, and Characterization of BaTi(IO3)6, LaTiO(IO3)5, Ba2VO2(IO3)4·(IO3), K2MoO2(IO3)4, and BaMoO2(IO3)4·H2O

    Inorganic Chemistry · 2005-03-08

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  12. Salt-Inclusion Synthesis of Two New Polar Solids, Ba6Mn4Si12O34Cl3 and Ba6Fe5Si11O34Cl3

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  13. Synthesis and Characterization of the Face-Sharing Bioctahedral [Mo2O6F3]3- Anion

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    Janet E. Kirsch, Heather K. Izumi, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  14. Synthesis and properties of pyrazine-pillared Ag3Mo2O4F7 and AgReO4 layered phases

    Journal of Solid State Chemistry · 2005-11-29

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  15. Phase transitions in oxyfluoride (NH4)2WO2F4

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  16. A Novel Chiral Cd(II) Coordination Polymer Based on Achiral Unsymmetrical 3-Amino-1,2,4-triazole with an Unprecedented μ4-Bridging Mode

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    Wei Li, Hongpeng Jia, Zhanfeng Ju, Jie Zhang

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  17. Homochiral metal–organic coordination networks from l-typtophan

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  18. Metallacycles of Iron, Zinc, and Cadmium Assembled by Polytopic Bis(pyrazolyl)methane Ligands and Fluoride Abstraction from BF4-

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    Daniel L. Reger, Russell P. Watson, J.R. Gardinier, Mark D. Smith, Perry J. Pellechia

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  19. Syntheses, Structures, and Magnetic Properties of Mononuclear CuIIand Tetranuclear CuII3MII(M = Cu, Co, or Mn) Compounds Derived fromN,N‘-Ethylenebis(3-ethoxysalicylaldimine): Cocrystallization Due to Potential Encapsulation of Water

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    Malabika Nayak, R. Koner, Hsin‐Huang Lin, Ülrich Flörke, Ho‐Hsiang Wei, Sasankasekhar Mohanta

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  20. Binuclear Fluoro-Bridged Zinc and Cadmium Complexes of a Schiff Base Expanded Porphyrin: Fluoride Abstraction from the Tetrafluoroborate Anion

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  21. A Novel Helical Double-Layered Cobalt(II)−Organic Framework with Tetranuclear [Co4(μ3-OH)2] Clusters Linked by an Unsymmetrical Pyridylbenzoate Ligand

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  22. A new hybrid framework based on a ‘superoctahedral’ [V7O6F30]14− polyanion

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  23. Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?

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  24. Spontaneous Resolution of Chiral Polyoxometalate‐Based Compounds Consisting of 3D Chiral Inorganic Skeletons Assembled from Different Helical Units

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  25. Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F4

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  26. Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions

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  27. New Inorganic Helical Chain: Synthesis, Structure, Characterization, and Interconversion of BaGa2O2(OH)4

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  28. Magnetoelastic Coupling through the Antiferromagnet-to-Ferromagnet Transition of Quasi-Two-Dimensional [Cu(HF2)(pyz)2]BF4 Using Infrared Spectroscopy

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  29. Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids

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  30. Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F4

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  31. pH-Tuned self-assembly of organic–inorganic hybrids based on different vanadate chains, Zn( ii ) ions and flexible ligands: crystallizing in polar and centrosymmetric space group

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  32. “Fluoride molecular scissors”: A rational construction of new Mo(VI) oxofluorido/1,2,4-triazole MOFs

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  33. Investigation of Trimetallic Ligand-Pillared Oxyfluorides: Ag2Cu(pzc)2MO x F6−x (M = Mo, Nb, and W)

    Journal of Chemical Crystallography · 2011-06-11

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  34. Orientational order of [VOF5]2− and [NbOF5]2− polar units in chains

    Journal of Solid State Chemistry · 2012-01-24

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  35. Syntheses, Structures Tuned by 4,4′-Bipyridine and Magnetic Properties of a Series of Transition Metal Compounds Containing o-Carboxylphenoxyacetate Acid

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  36. Raman spectroscopic study of the lattice dynamics in the Rb2KMoO3F3 oxyfluoride

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  37. Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State

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  38. From Racemic Units to Polar Materials

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  39. Unprecedented Trapping of Difluorooctamolybdate Anions within an α-Polonium Type Coordination Network

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  40. Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model

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  41. Synthesis and crystal structures of (pyH)2[Mo2O4F6] and (pipH2)[Mo2O4F6]; vibrational band assignment for [Mo2O4F6]2− anion

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  42. Measurement of Raman-Scattering Spectra of Rb2KMoO3F3 Crystal: Evidence for Controllable Disorder in the Lattice Structure

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  43. Na 2 MoO 2− δ F 4+ δ – a perovskite with a unique combination of atomic orderings and octahedral tilts

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  44. On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units

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  45. A Nearly Ideal One-Dimensional S = 5/2 Antiferromagnet FeF3(4,4′-bpy) (4,4′-bpy =4,4′-bipyridyl) with Strong Intrachain Interactions

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  46. Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships

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  47. Cyclohexylammonium sulfanilate: A simple representative of the chiral materials containing only achiral building units

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  48. Effect of Deuteration on Phase Transitions in Vanadium Dioxotetrafluoride

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  49. Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands

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  50. Periodic Tendril Perversion and Helices in the AMoO2F3 (A = K, Rb, NH4, Tl) Family

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