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RESEARCH PAPER · Inorganic Chemistry · 2007

A Novel Helical Double-Layered Cobalt(II)−Organic Framework with Tetranuclear [Co4(μ3-OH)2] Clusters Linked by an Unsymmetrical Pyridylbenzoate Ligand

Junhua Luo, Yusheng Zhao, Hongwu Xu, Tiffany L. Kinnibrugh, Dali Yang, Tatiana V. Timofeeva, Luke L. Daemen, Jianzhong Zhang, Wei Bao, Joe D. Thompson, Robert P. Currier

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A Novel Helical Double-Layered Cobalt(II)−Organic Framework with Tetranuclear [Co4(μ3-OH)2] Clusters Linked by an Unsymmetrical Pyridylbenzoate LigandOriginalA novel 2D (4,4) cobalt(II)-organic framework based on tetranuclear cluster nodes and double stranded organic linkers9Oligo- and Polymeric PdII and PtII Using Pyridyl Carboxylate Spacers for Topology Control43A novel pentanuclear Zn(II) coordination polymer with double helices: Synthesis, structure and luminescent property23Assembly of Metal−Organic Frameworks with Helical Layer: From 2D Parallel Interpenetrated Layer to 3D Self-Penetrating Network77Self-Assembly of a Series of Cobalt(II) Coordination Polymers Constructed from H2tbip and Dipyridyl-Based Ligands210Magnetic metal–organic frameworks2448Structural Variation from 1D to 3D: Effects of Temperature and pH Value on the Construction of Co(II)-H2tbip/bpp Mixed Ligands System207A New 4-Connected Co(II) Coordination Framework With an Uncommon Two-Fold Interpenetrating Net: Synthesis, Structure and Luminescence Property73-(4-Pyridyl)benzoic acid1Structure and Magnetic Property of a Cobalt(II) Complex Synthesized Through in situ Hydrothermal Reaction2Quasi-2D XY Magnetic Properties and Slow Relaxation in a Body Centered Metal Organic Network of [Co4] Clusters129Synthesis, crystal structures, and characterization of two Co(II) coordination polymers with 3-pyrid-3-ylbenzoic acid7Constructions of helical coordination compounds153A unique 2D framework containing rhombic tetrameric cobalt(II) of mixed Td and Oh geometries linked by two different rigid ligands: Synthesis, crystal structure and magnetic properties25Synthesis, Structure, and Magnetic Properties of Cobalt(II) Coordination Polymers from a New Tripodal Carboxylate Ligand: Weak Ferromagnetism and Metamagnetism127Synthesis, crystal structure and characterization of a new layered gallium phosphite Ga(HPO3)F3·(trans-C6N2H16) with left- and right-handed helical chains12Tuning of unusual secondary ligands to construct fluorescent zinc coordination polymers of an unsymmetrical pyridylbenzoate ligand from 1D chain to interdigital or porous 2D layers and interpenetrated 3D frameworks24Construction of Metal−Organic Frameworks with Tetranuclear Metal Clusters: Hydrothermal Synthesis, Structure, and Magnetic Properties35Synthesis, Magnetic Properties, and STM Spectroscopy of Cobalt(II) Cubanes [CoII4(Cl)4(HL)4]38A 3-D cobalt(II)-coordination polymer with mixed-connected network topology constructed from 4-pyridin-3-yl-benzoic acid10Microporous La(III) Metal−Organic Framework Using a Semirigid Tricarboxylic Ligand: Synthesis, Single-Crystal to Single-Crystal Sorption Properties, and Gas Adsorption Studies72Coordination assemblies of CdII/ZnII/CoII with the 3-(pyridin-4-yl) benzoate tecton: Structural diversity and properties18Three-dimensional iron-series coordination networks based on antiferromagnetic and ferromagnetic dinuclear motifs with mixed carboxylate and aqua bridges13pH-Tuned self-assembly of organic–inorganic hybrids based on different vanadate chains, Zn( ii ) ions and flexible ligands: crystallizing in polar and centrosymmetric space group28Anion exchange induced tunable catalysis properties of an uncommon butterfly-like tetranuclear copper(ii) cluster and magnetic characterization17CoII, MnII and CuII-directed coordination polymers with mixed tetrazolate–dicarboxylate heterobridges exhibiting spin-canted, spin-frustrated antiferromagnetism and a slight spin-flop transition58Three three-dimensional anionic metal–organic frameworks with (4,8)-connected alb topology constructed from a semi-rigid ligand and polynuclear metal clusters21pH Dependent Structural Diversity of Metal Complexes with 5-(4 H -1,2,4-Triazol-4-yl)benzene-1,3-dicarboxylic Acid128A Series of Two-Dimensional Co(II), Mn(II), and Ni(II) Coordination Polymers with Di- or Trinuclear Secondary Building Units Constructed by 1,1′-Biphenyl-3,3′-Dicarboxylic Acid: Synthesis, Structures, and Magnetic Properties81A one-dimensional copper(II) coordination polymer constructed by pyridyl-2,5-dicarboxylate: Helical structure and magnetic property3Coordination polymers of unsymmetrical angular ligand 3-pyridin-4-ylbenzoate acid: Syntheses, structural diversity and properties12One-Dimensional Cd(II) and Co(II) Coordination Polymers with Dinuclear Secondary Building Units Constructed by 1,1′-Biphenyl-3,3′-Dicarboxylic Acid: Synthesis, Structures, Luminescent and Magnetic Properties5Three New Isostructural Coordination Polymers with Cd(II) Clusters as the SBU: Synthesis, Structural Characterization, and Luminescence Properties24Structural Diversity for a Series of Metal(II) Complexes Based on Flexible 1,2-Phenylenediacetate and Dipyridyl-type Coligand89A Novel Twofold Interpenetrating 2D (3,5)-Connected Cd(II) Coordination Framework with (52.6)(55.64.7) Topology9Tetraaquabis[3-(pyridin-4-yl)benzoato-κN]cobalt(II)1Divalent metal coordination polymers assembled from dual linkers – semirigid carboxyphenylpropionate and dipyridyl type molecule41Magnetic Modulation and Cation-Exchange in a Series of Isostructural (4,8)-Connected Metal–Organic Frameworks with Butterfly-like [M4(OH)2(RCO2)8] Building Units64Three unprecedented open frameworks based on a pyridyl-carboxylate: synthesis, structures and properties18Three two-dimensional cobalt(II) and nickel(II) coordination polymers with dinuclear secondary building units constructed by one unsymmetric dicarboxylic acid: Synthesis, structures, and magnetic property4Highly-connected, porous coordination polymers based on [M4(μ3-OH)2] (M = CoII and NiII) clusters: different networks, adsorption and magnetic properties72Synthesis, structures and luminescent properties of cadmium(ii) metal organic frameworks based on 3-pyrid-4-ylbenzoic acid, 4-pyrid-4-ylbenzoic acid ligands39Structural Transformation from a Discrete CuII4 Cluster to Two Extended CuII4 + CuII1 Chain-Based Three-Dimensional Frameworks by Changing the Spacer Functionality: Synthesis, Crystal Structures, and Magnetic Properties50Syntheses, Crystal Structures, and Magnetic Properties of Metal–Organic Hybrid Materials of Co(II) Using Flexible and Rigid Nitrogen-Based Ditopic Ligands as Spacers98Co(II) Coordination Polymers with Co-Ligand Dependent Dinuclear to Tetranuclear Core: Spin-Canting, Weak Ferromagnetic, and Antiferromagnetic Behavior56Four Low-Dimensional Cobalt(II) Coordination Polymers Based on a New Isophthalic Acid Derivative: Syntheses, Crystal Structures, and Properties55Preparation and characterization of two new 2-D double helical networks based on 1,3-bis(4-pyridyl)propane8Two new 2-D coordination polymers based on a purine-containing carboxylate7Solvent Influence on Sizes of Channels in Three New Co(II) Complexes, Exhibiting an Active Replaceable Coordinated Site63Luminescence, magnetism and structures of 1D 3-pyridin-yl-benzoic lanthanide coordination complexes5Functionalized Adamantane Tectons Used in the Design of Mixed-Ligand Copper(II) 1,2,4-Triazolyl/Carboxylate Metal–Organic Frameworks62Diverse assemblies of the (4,4) grid layers exemplified in Zn(II)/Co(II) coordination polymers with dual linear ligands6Structural Diversity and Luminescence Properties of Coordination Polymers Built With a Rigid Linear Dicarboxylate and Zn(II)/Pb(II) Ion73Solvothermal Synthesis and Crystal Structure of a New Cd(II) Coordination Polymer With bcu Topology Constructed by Pyridine-Carboxylate Ligand4Poly[bis[μ2-3-(pyridin-4-yl)benzoato-κ3N:O,O′]lead(II)]1Solvent-Induced Structural Diversity of Partially Fluorinated, Stable Pb(II) Metal–Organic Frameworks and Their Luminescence Properties84Structure and characterization of A 2D cobalt(II) complex [Co(L)2] n (L = 3-nitro-5-(pyridine-4-yl)benzoate)0Two Coordination Polymers Based on 3‐(Carboxymethoxy)benzene‐1,2‐dioic Acid and N‐donor Ancillary Ligands: Synthesis, Crystal structures, and Magnetic Properties2Structural diversity and luminescence properties of the novel {[Cd3(TBIB)4(BTC)2]·2C2H5OH·11H2O}n and {[Zn(TBIB)(HBTC)]·3H2O}n coordination polymers12An unprecedented ten-connected 3D metal–organic framework based on hexanuclear cobalt(II) cluster building blocks7Unusual Magnetic Behaviors and Electronic Configurations Driven by Diverse Co(II) or Mn(II) MOF Architectures30Recent advances in metal–organic frameworks based on pyridylbenzoate ligands: properties and applications19Self-assembly of heterometallic Ln III –Co II coordination polymers: syntheses, structures, and magnetic studies10Synthesis of cobalt cluster-based supramolecular triple-stranded helicates18Solvothermal Syntheses and Crystal Structures of Two New Mn(II) Coordination Polymers Constructed by Pyridine-Carboxylate Ligands0Syntheses and structures of three transition metal coordination polymers based on 5-Aminonicotinic acid5A three-dimensional pillared-layer metal-organic framework: Synthesis, structure and gas adsorption studies23Three coordination compounds of cobalt with organic carboxylic acids and 1,10-phenanthroline as ligands: syntheses, structures and photocatalytic properties12Metal–Organic Frameworks Built from a Linear Rigid Dicarboxylate and Different Colinkers: Trap of the Keto Form of Ethylacetoacetate, Luminescence and Ferroelectric Studies34Hydrothermal Synthesis, Crystal Structure, and Luminescent Property of a Novel Zn(II)-Organic Framework With Tetranuclear [Zn4(μ3-OH)2] Clusters Linked by an Unsymmetrical Pyridylbenzoate Ligand With Helical Chains0Syntheses, Structures, and Magnetic Properties of Two Cobalt(II) Metal‐Organic Frameworks Based on Y‐shaped 3,5,4′‐Azobenzenetricarboxylic Acid and Different N‐donor Ligands2Syntheses, crystal structures, and magnetic studies of two cobalt(II) coordination polymers based on concurrent ligand extension27A new strategy to obtain tetranuclear cobalt( ii ) metal–organic frameworks based on the [Co 4 (μ 3 -OH) 2 ] cluster: synthesis, structures and properties44Four Pb( ii ) metal–organic frameworks with increasing dimensions: structural diversities by varying the ligands14Structure and Photocatalytic Property of a Novel Three-Dimensional Supramolecular Cu(ΙΙ) Coordination Polymer with pcu Topology Based on the Rigid Multifunctional Ligand3A highly-flexible cyclic-decavanadate ligand for interconversion of dinuclear- and trinuclear-cobalt( ii ) and manganese( ii ) cores10Fluorescent sensing and selective adsorption properties of metal–organic frameworks with mixed tricarboxylate and 1H-imidazol-4-yl-containing ligands61Vapor Sorption and Solvatochromism in a Metal–Organic Framework of an Asymmetric Pyridylcarboxylate21Tuning of Luminescent and Magnetic Properties via Metal Doping of Zn-BTC Systems7Magneto-structural correlations of novel kagomé-type metal organic frameworks17Syntheses, Structures and Topology Variations of Metal Organic Frameworks Built From a Semi‐Rigid Tetracarboxylate Ligand23Syntheses, Structures and Magnetic Properties of Cobalt(II) Coordination Polymers Based on Semi-Rigid Polycarboxylic Acid Ligand7Synthesis, Structure and Properties of a Dicubane-Like Tetracobalt Cluster1A new two-dimensional homochiral cadmium(II) coordination polymer: synthesis, structure determination, optical properties, and fluorescent sensing1

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  1. A novel 2D (4,4) cobalt(II)-organic framework based on tetranuclear cluster nodes and double stranded organic linkers

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  2. Oligo- and Polymeric PdII and PtII Using Pyridyl Carboxylate Spacers for Topology Control

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  3. A novel pentanuclear Zn(II) coordination polymer with double helices: Synthesis, structure and luminescent property

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  4. Assembly of Metal−Organic Frameworks with Helical Layer: From 2D Parallel Interpenetrated Layer to 3D Self-Penetrating Network

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  5. Self-Assembly of a Series of Cobalt(II) Coordination Polymers Constructed from H2tbip and Dipyridyl-Based Ligands

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  6. Magnetic metal–organic frameworks

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  7. Structural Variation from 1D to 3D: Effects of Temperature and pH Value on the Construction of Co(II)-H2tbip/bpp Mixed Ligands System

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  8. A New 4-Connected Co(II) Coordination Framework With an Uncommon Two-Fold Interpenetrating Net: Synthesis, Structure and Luminescence Property

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  9. 3-(4-Pyridyl)benzoic acid

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  10. Structure and Magnetic Property of a Cobalt(II) Complex Synthesized Through in situ Hydrothermal Reaction

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  11. Quasi-2D XY Magnetic Properties and Slow Relaxation in a Body Centered Metal Organic Network of [Co4] Clusters

    Journal of the American Chemical Society · 2009-07-06

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  12. Synthesis, crystal structures, and characterization of two Co(II) coordination polymers with 3-pyrid-3-ylbenzoic acid

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  13. Constructions of helical coordination compounds

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  14. A unique 2D framework containing rhombic tetrameric cobalt(II) of mixed Td and Oh geometries linked by two different rigid ligands: Synthesis, crystal structure and magnetic properties

    Inorganic Chemistry Communications · 2009-10-16

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  15. Synthesis, Structure, and Magnetic Properties of Cobalt(II) Coordination Polymers from a New Tripodal Carboxylate Ligand: Weak Ferromagnetism and Metamagnetism

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  16. Synthesis, crystal structure and characterization of a new layered gallium phosphite Ga(HPO3)F3·(trans-C6N2H16) with left- and right-handed helical chains

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    Liangliang Huang, Tianyou Song, Lirong Zhang, Yanli Chen, Jinhua Jiang, Jianing Xu, Li Wang

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  17. Tuning of unusual secondary ligands to construct fluorescent zinc coordination polymers of an unsymmetrical pyridylbenzoate ligand from 1D chain to interdigital or porous 2D layers and interpenetrated 3D frameworks

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    Cao‐Yuan Niu, Xian‐Fu Zheng, Yong He, Zhiqiang Feng, Chun-Hong Kou

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  18. Construction of Metal−Organic Frameworks with Tetranuclear Metal Clusters: Hydrothermal Synthesis, Structure, and Magnetic Properties

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  19. Synthesis, Magnetic Properties, and STM Spectroscopy of Cobalt(II) Cubanes [CoII4(Cl)4(HL)4]

    Chemistry - A European Journal · 2010-03-20

    Andreas Scheurer, A.M. Ako, Rolf W. Saalfrank, Frank W. Heinemann, Frank Hampel, K. Petukhov, Klaus Gieb, Michael Stocker, Paul Müller

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  20. A 3-D cobalt(II)-coordination polymer with mixed-connected network topology constructed from 4-pyridin-3-yl-benzoic acid

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  21. Microporous La(III) Metal−Organic Framework Using a Semirigid Tricarboxylic Ligand: Synthesis, Single-Crystal to Single-Crystal Sorption Properties, and Gas Adsorption Studies

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  22. Coordination assemblies of CdII/ZnII/CoII with the 3-(pyridin-4-yl) benzoate tecton: Structural diversity and properties

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  23. Three-dimensional iron-series coordination networks based on antiferromagnetic and ferromagnetic dinuclear motifs with mixed carboxylate and aqua bridges

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  24. pH-Tuned self-assembly of organic–inorganic hybrids based on different vanadate chains, Zn( ii ) ions and flexible ligands: crystallizing in polar and centrosymmetric space group

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  25. Anion exchange induced tunable catalysis properties of an uncommon butterfly-like tetranuclear copper(ii) cluster and magnetic characterization

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  26. CoII, MnII and CuII-directed coordination polymers with mixed tetrazolate–dicarboxylate heterobridges exhibiting spin-canted, spin-frustrated antiferromagnetism and a slight spin-flop transition

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  27. Three three-dimensional anionic metal–organic frameworks with (4,8)-connected alb topology constructed from a semi-rigid ligand and polynuclear metal clusters

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  28. pH Dependent Structural Diversity of Metal Complexes with 5-(4 H -1,2,4-Triazol-4-yl)benzene-1,3-dicarboxylic Acid

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  29. A Series of Two-Dimensional Co(II), Mn(II), and Ni(II) Coordination Polymers with Di- or Trinuclear Secondary Building Units Constructed by 1,1′-Biphenyl-3,3′-Dicarboxylic Acid: Synthesis, Structures, and Magnetic Properties

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  30. A one-dimensional copper(II) coordination polymer constructed by pyridyl-2,5-dicarboxylate: Helical structure and magnetic property

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  31. Coordination polymers of unsymmetrical angular ligand 3-pyridin-4-ylbenzoate acid: Syntheses, structural diversity and properties

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  32. One-Dimensional Cd(II) and Co(II) Coordination Polymers with Dinuclear Secondary Building Units Constructed by 1,1′-Biphenyl-3,3′-Dicarboxylic Acid: Synthesis, Structures, Luminescent and Magnetic Properties

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  33. Three New Isostructural Coordination Polymers with Cd(II) Clusters as the SBU: Synthesis, Structural Characterization, and Luminescence Properties

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  34. Structural Diversity for a Series of Metal(II) Complexes Based on Flexible 1,2-Phenylenediacetate and Dipyridyl-type Coligand

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  35. A Novel Twofold Interpenetrating 2D (3,5)-Connected Cd(II) Coordination Framework with (52.6)(55.64.7) Topology

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  36. Tetraaquabis[3-(pyridin-4-yl)benzoato-κN]cobalt(II)

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  37. Divalent metal coordination polymers assembled from dual linkers – semirigid carboxyphenylpropionate and dipyridyl type molecule

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  38. Magnetic Modulation and Cation-Exchange in a Series of Isostructural (4,8)-Connected Metal–Organic Frameworks with Butterfly-like [M4(OH)2(RCO2)8] Building Units

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  39. Three unprecedented open frameworks based on a pyridyl-carboxylate: synthesis, structures and properties

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  40. Three two-dimensional cobalt(II) and nickel(II) coordination polymers with dinuclear secondary building units constructed by one unsymmetric dicarboxylic acid: Synthesis, structures, and magnetic property

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  41. Highly-connected, porous coordination polymers based on [M4(μ3-OH)2] (M = CoII and NiII) clusters: different networks, adsorption and magnetic properties

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  42. Synthesis, structures and luminescent properties of cadmium(ii) metal organic frameworks based on 3-pyrid-4-ylbenzoic acid, 4-pyrid-4-ylbenzoic acid ligands

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  43. Structural Transformation from a Discrete CuII4 Cluster to Two Extended CuII4 + CuII1 Chain-Based Three-Dimensional Frameworks by Changing the Spacer Functionality: Synthesis, Crystal Structures, and Magnetic Properties

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  44. Syntheses, Crystal Structures, and Magnetic Properties of Metal–Organic Hybrid Materials of Co(II) Using Flexible and Rigid Nitrogen-Based Ditopic Ligands as Spacers

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  45. Co(II) Coordination Polymers with Co-Ligand Dependent Dinuclear to Tetranuclear Core: Spin-Canting, Weak Ferromagnetic, and Antiferromagnetic Behavior

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  46. Four Low-Dimensional Cobalt(II) Coordination Polymers Based on a New Isophthalic Acid Derivative: Syntheses, Crystal Structures, and Properties

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  47. Preparation and characterization of two new 2-D double helical networks based on 1,3-bis(4-pyridyl)propane

    Journal of Coordination Chemistry · 2012-07-18

    Lijuan Zhang, Donghua Xu, Yunshan Zhou, Yan Hong Guo, Waqar Ahmad

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  48. Two new 2-D coordination polymers based on a purine-containing carboxylate

    Journal of Coordination Chemistry · 2012-08-23

    Xin-Qi Liu, Zhongyuan Li, Xiao-Ju Yuan, Ben‐Lai Wu

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  49. Solvent Influence on Sizes of Channels in Three New Co(II) Complexes, Exhibiting an Active Replaceable Coordinated Site

    Crystal Growth & Design · 2012-11-15

    Wenhuan Huang, Guo‐Ping Yang, Jun Chen, Xin V. Chen, Cuiping Zhang, Yao‐Yu Wang, Qi‐Zhen Shi

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  50. Luminescence, magnetism and structures of 1D 3-pyridin-yl-benzoic lanthanide coordination complexes

    Synthetic Metals · 2013-01-01

    Guang‐Feng Hou, Ruiqiang Ding, Peng‐Fei Yan, Hongfeng Li, Peng Chen, Guangming Li

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