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RESEARCH PAPER · Inorganic Chemistry · 2006

Metallacycles of Iron, Zinc, and Cadmium Assembled by Polytopic Bis(pyrazolyl)methane Ligands and Fluoride Abstraction from BF4-

Daniel L. Reger, Russell P. Watson, J.R. Gardinier, Mark D. Smith, Perry J. Pellechia

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Metallacycles of Iron, Zinc, and Cadmium Assembled by Polytopic Bis(pyrazolyl)methane Ligands and Fluoride Abstraction from BF4-OriginalMetallomacrocycles from ditopic chiral scorpionate ligands26Zinc, cadmium and mercury3Synthesis of an anthracene-based bis(pyrazolyl)methane ligand and the structural characterization of its dinuclear tricarbonylrhenium(I) complex12Metallacyclic Zinc Complexes of Alkylidene-Linked Bitopic Bis(pyrazolyl)methane Ligands: Unusual Exocyclic Bridging Fluoride Ligands12Binuclear Fluoro-Bridged Zinc and Cadmium Complexes of a Schiff Base Expanded Porphyrin: Fluoride Abstraction from the Tetrafluoroborate Anion77Silver(I) Double and Multiple Salts Containing the 1,3‐Butadiynediide Dianion: Coordination Diversity and Assembly with the Supramolecular Synthon Ag4⊂CCCC⊃Ag418Solid-State Characterization of the Nuclear and Electronic Environments in a Boron−Fluoride Co-doped TiO2Visible-Light Photocatalyst69An Organoplatinum(II) Complex of a Bitopic, Propylene-linked Bis(pyrazolyl)methane Ligand2Zinc, cadmium and mercury3First-Row Transition-Metal Complexes of a New Pentadentate Ligand, α,α,α′,α′-Tetra(pyrazolyl)lutidine24Di- and Tritopic Poly(pyrazol-1-yl)borate Ligands: Synthesis, Characterization, and Reactivity toward [Mn(CO) 5 Br]24Chemical etching with tetrafluoroborate: a facile method for resizing of CdTe nanocrystals under mild conditions19SiF6 2 − anionic hydrogen-bonds in [Co(im)6] · (SiF6) · (im)2 and cis-[Cd2(bipy)2(H2O)4(μ-F)2] · SiF6 complexes4Halido‐Bridged Dinuclear Nickel and Zinc Complexes with a Bis(tripodal) Octaamine Ligand – Unusual Coordination Mode of an ortho‐Phenylenediamine9Unusual Reactivity of the Bis(pyrazolyl)borate Chelate: B−H for B−X (X = F, Cl, OH) Substitution in Complexes of Ruthenium17Monofluoride Bridged, Binuclear Metallacycles of First Row Transition Metals Supported by Third Generation Bis(1-pyrazolyl)methane Ligands: Unusual Magnetic Properties44Anion-directed genuine meso-helical supramolecular isomers of two 1D Ag(i) complexes based on arene-linked bis(pyrazolyl)methane ligands30Spectroscopic and functional models for Hmd hydrogenase0Synthesis and Coordination Chemistry of a New N4-Polydentate Class of Pyridyl-Functionalized Scorpionate Ligands: Complexes of FeII, ZnII, NiII, VIV, PdII and Use for Heterobimetallic Systems23Synthesis and Coordination Chemistry of Two N2-Donor Chelating Di(indazolyl)methane Ligands: Structural Characterization and Comparison of Their Metal Chelation Aptitudes18Synthesis, structure and properties of one 2-D Ag(I) complex based on trinuclear silver(I) cluster and arene-linked bis(pyrazolyl)methane ligand9Ditopic tris(2-mercaptoimidazol-1-yl)borate ligands and their coordination behavior toward [Ru(p-cymene)]2+5Solvent control: dinuclear versus tetranuclear complexes of a bis-tetradentate pyrimidine-based ligand23The multifunctional roles of the ionic liquid [Bmim][BF4] in the creation of cadmium metal–organic frameworks37Structural Variations in Copper(II) Complexes of a Bitopic Bis(pyrazolyl)methane Ligand14Halide and Hydroxide Linearly Bridged Bimetallic Copper(II) Complexes: Trends in Strong Antiferromagnetic Superexchange Interactions47Synthesis, structural, and biological evaluation of the arene-linked pyrazolyl methane ligands and their d9/d10 metal complexes24Dinuclear Complexes Containing Linear M–F–M [M = Mn(II), Fe(II), Co(II), Ni(II), Cu(II), Zn(II), Cd(II)] Bridges: Trends in Structures, Antiferromagnetic Superexchange Interactions, and Spectroscopic Properties84Self-assembly of transition metal ion complexes of a hybrid pyrazine–terpyridine ligand17Group 11 complexes with the bidentate di(1H-indazol-1-yl)methane and di(2H-indazol-2-yl)methane) ligands18Rhodium and Iridium Complexes with a New Scorpionate Phosphane Ligand12Di‐ and Tetranuclear Complexes of Bis‐Tetradentate Pyrimidine‐Based Ligands with All‐Methylene‐ Versus Mixed Methylene/Ethylene‐Linked Arms12Zinc(II) and Cadmium(II) Monohydroxide Bridged, Dinuclear Metallacycles: A Unique Case of Concerted Double Berry Pseudorotation15Synthesis, Structure, and Reactivity of a Terminal Organozinc Fluoride Compound: Hydrogen Bonding, Halogen Bonding, and Donor–Acceptor Interactions40Structure, Stability, and Catalytic Activity of Fluorine-Bridged Complexes IPr·GaCl2(μ-F)EFn–1 (EFn– = SbF6–, PF6–, or BF4–)55Dinuclear Metallacycles with Single M–O(H)–M Bridges [M = Fe(II), Co(II), Ni(II), Cu(II)]: Effects of Large Bridging Angles on Structure and Antiferromagnetic Superexchange Interactions26Beyond the Balz–Schiemann Reaction: The Utility of Tetrafluoroborates and Boron Trifluoride as Nucleophilic Fluoride Sources210Conversion of a Monodentate Amidinate–Germylene Ligand into Chelating Imine–Germanate Ligands (on Mononuclear Manganese Complexes)34Base‐Free Non‐Noble‐Metal‐Catalyzed Hydrogen Generation from Formic Acid: Scope and Mechanistic Insights61A trigonal prismatic Cu 6 -pyrazolato complex containing a μ 6 -F ligand18Fluoride-coordination chemistry in molecular and low-dimensional magnetism67How Innocent are Potentially Redox Non-Innocent Ligands? Electronic Structure and Metal Oxidation States in Iron-PNN Complexes as a Representative Case Study95The transition-metal chemistry of amidinatosilylenes, -germylenes and -stannylenes240Intramolecularly Stabilized Heavier Tetrylenes: From Monodentate to Bidentate Ligands63A Boron‐Fluorinated Tris(pyrazolyl)borate Ligand (FTp*) and Its Mono‐ and Dinuclear Copper Complexes [Cu(FTp*)2] and [Cu2(FTp*)2]: Synthesis, Structures, and DFT Calculations12Diiron(III)–μ‐Fluoro Bisporphyrins: Effect of Bridging Ligand on the Metal Spin State40A Hydrophobic Metal–Organic Framework Based on Cubane‐Type [Co 4 (μ 3 ‐F) 3 (μ 3 ‐SO 4 )] 3+ Clusters for Gas Storage and Adsorption Selectivity of Benzene over Cyclohexane48Spontaneous Si–C bond cleavage in (Triphos Si )-nickel complexes20Multiple coordination modes of a new ditopic bis(pyrazolyl)methane-based ligand10A tetranuclear fluorido-bridged iron compound: Fluoride abstraction from the tetrafluoridoborate anion7An Innovative Design of an Efficient Layered Electrochemical Sensor for Determination of Tyrosine and Tryptophan in the Presence of Interfering Compounds in Biological Fluids22Experimental and Theoretical Investigation of an SN2-type Pathway for Borate–Fluorine Bond Cleavage by Electron-Rich Late-Transition Metal Complexes8Self-assembly of a trigonal bipyramidal architecture with stabilisation of iron in three spin states4Hydrogen-atom and oxygen-atom transfer reactivities of iron( iv )-oxo complexes of quinoline-substituted pentadentate ligands22Binuclear complexes with single M-F-M bridge (M: Fe, Mn, and Cu): A critical analysis of the impact of fluoride for isoelectronic hydroxide substitution7Salt Metathesis: Tetrafluoroborate Anion Rapidly Fluoridates Organoboronic Acids to give Organotrifluoroborates22Salt Metathesis: Tetrafluoroborate Anion Rapidly Fluoridates Organoboronic Acids to give Organotrifluoroborates1Coordination of ε-Caprolactone to a Cationic Niobium(V) Alkoxide Complex: Fundamental Insight into Ring-Opening Polymerization via Coordination–Insertion11Structural variations in Co(II), Co(III) and Zn(II) complexes of a chiral triphenolic macrocycle0

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  1. Metallomacrocycles from ditopic chiral scorpionate ligands

    Dalton Transactions · 2007-01-01

    Fan Zhang, T. Morawitz, S. Bieller, Michael Bolte, Hans-Wolfram Lerner, Matthias Wagner

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  2. Zinc, cadmium and mercury

    Annual Reports Section A (Inorganic Chemistry) · 2007-01-01

    Andrew J. West

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  3. Synthesis of an anthracene-based bis(pyrazolyl)methane ligand and the structural characterization of its dinuclear tricarbonylrhenium(I) complex

    Journal of Organometallic Chemistry · 2007-03-19

    Daniel L. Reger, Russell P. Watson, Mark D. Smith

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  4. Metallacyclic Zinc Complexes of Alkylidene-Linked Bitopic Bis(pyrazolyl)methane Ligands: Unusual Exocyclic Bridging Fluoride Ligands

    Crystal Growth & Design · 2007-04-20

    Daniel L. Reger, Russell P. Watson, Mark D. Smith, Perry J. Pellechia

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  5. Binuclear Fluoro-Bridged Zinc and Cadmium Complexes of a Schiff Base Expanded Porphyrin: Fluoride Abstraction from the Tetrafluoroborate Anion

    Inorganic Chemistry · 2007-07-14

    Elisa Tomat, Luciano Cuesta, Vincent M. Lynch, Jonathan L. Sessler

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  6. Silver(I) Double and Multiple Salts Containing the 1,3‐Butadiynediide Dianion: Coordination Diversity and Assembly with the Supramolecular Synthon Ag4⊂CCCC⊃Ag4

    Chemistry - An Asian Journal · 2007-09-04

    Liang Zhao, Miao Du, Thomas C. W. Mak

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  7. Solid-State Characterization of the Nuclear and Electronic Environments in a Boron−Fluoride Co-doped TiO2Visible-Light Photocatalyst

    The Journal of Physical Chemistry C · 2007-10-18

    Enrique A. Reyes-García, Yanping Sun, Daniel Raftery

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  8. An Organoplatinum(II) Complex of a Bitopic, Propylene-linked Bis(pyrazolyl)methane Ligand

    Journal of Chemical Crystallography · 2007-10-23

    Daniel L. Reger, Russell P. Watson, Mark D. Smith

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  9. Zinc, cadmium and mercury

    Annual Reports Section A (Inorganic Chemistry) · 2008-01-01

    Andrew J. West

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  10. First-Row Transition-Metal Complexes of a New Pentadentate Ligand, α,α,α′,α′-Tetra(pyrazolyl)lutidine

    Inorganic Chemistry · 2008-08-06

    T.J. Morin, Brian Bennett, Sergey V. Lindeman, J.R. Gardinier

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  11. Di- and Tritopic Poly(pyrazol-1-yl)borate Ligands: Synthesis, Characterization, and Reactivity toward [Mn(CO) 5 Br]

    Organometallics · 2008-09-10

    T. Morawitz, Fan Zhang, Michael Bolte, Jan W. Bats, Hans-Wolfram Lerner, Matthias Wagner

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  12. Chemical etching with tetrafluoroborate: a facile method for resizing of CdTe nanocrystals under mild conditions

    Chemical Communications · 2009-01-01

    Jianbo Liu, Xiaohai Yang, Kemin Wang, Dong Wang, Pengfei Zhang

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  13. SiF6 2 − anionic hydrogen-bonds in [Co(im)6] · (SiF6) · (im)2 and cis-[Cd2(bipy)2(H2O)4(μ-F)2] · SiF6 complexes

    Journal of Coordination Chemistry · 2009-05-18

    Jing Wang, Fang‐Fang Jian, Xian Wang

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  14. Halido‐Bridged Dinuclear Nickel and Zinc Complexes with a Bis(tripodal) Octaamine Ligand – Unusual Coordination Mode of an ortho‐Phenylenediamine

    European Journal of Inorganic Chemistry · 2009-09-02

    F. Ekkehardt Hahn, H. Schröder, Tania Pape

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  15. Unusual Reactivity of the Bis(pyrazolyl)borate Chelate: B−H for B−X (X = F, Cl, OH) Substitution in Complexes of Ruthenium

    Organometallics · 2009-10-12

    Michael J. Page, Barbara Ann Messerle, Jörg Wagler

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  16. Monofluoride Bridged, Binuclear Metallacycles of First Row Transition Metals Supported by Third Generation Bis(1-pyrazolyl)methane Ligands: Unusual Magnetic Properties

    Inorganic Chemistry · 2009-10-14

    Daniel L. Reger, Elizabeth A. Foley, Russell P. Watson, Perry J. Pellechia, Mark D. Smith, Fernande Grandjean, Gary J. Long

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  17. Anion-directed genuine meso-helical supramolecular isomers of two 1D Ag(i) complexes based on arene-linked bis(pyrazolyl)methane ligands

    CrystEngComm · 2010-01-01

    Shuang Wang, Hong‐Ying Zang, Chunyi Sun, Guang‐Juan Xu, Xinlong Wang, Kui‐Zhan Shao, Ya‐Qian Lan, Zhong‐Min Su

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  18. Spectroscopic and functional models for Hmd hydrogenase

    Illinois Digital Environment for Access to Learning and Scholarship (University of Illinois at Urbana-Champaign) · 2010-01-01

    Aaron M. Royer

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  19. Synthesis and Coordination Chemistry of a New N4-Polydentate Class of Pyridyl-Functionalized Scorpionate Ligands: Complexes of FeII, ZnII, NiII, VIV, PdII and Use for Heterobimetallic Systems

    Inorganic Chemistry · 2010-07-28

    Riccardo D. Wanke, Maria Fátima C. Guedes da Silva, Stefano Lancianesi, Telma F. S. Silva, Luísa M. D. R. S. Martins, Claudio Pettinari, Armando J. L. Pombeiro

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  20. Synthesis and Coordination Chemistry of Two N2-Donor Chelating Di(indazolyl)methane Ligands: Structural Characterization and Comparison of Their Metal Chelation Aptitudes

    Inorganic Chemistry · 2010-10-22

    Claudio Pettinari, Alessandro Marinelli, F. Marchetti, Jean Ngouné, Agustı́n Galindo, Eleuterio Álvarez, Margarita Gómez

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  21. Synthesis, structure and properties of one 2-D Ag(I) complex based on trinuclear silver(I) cluster and arene-linked bis(pyrazolyl)methane ligand

    Inorganic Chemistry Communications · 2010-11-26

    Shuang Wang, Gang Yuan, Chunyi Sun, Guang‐Sheng Yang, Kui‐Zhan Shao, Xinlong Wang, Ya‐Qian Lan, Zhong‐Min Su

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  22. Ditopic tris(2-mercaptoimidazol-1-yl)borate ligands and their coordination behavior toward [Ru(p-cymene)]2+

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  23. Solvent control: dinuclear versus tetranuclear complexes of a bis-tetradentate pyrimidine-based ligand

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  24. The multifunctional roles of the ionic liquid [Bmim][BF4] in the creation of cadmium metal–organic frameworks

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  25. Structural Variations in Copper(II) Complexes of a Bitopic Bis(pyrazolyl)methane Ligand

    European Journal of Inorganic Chemistry · 2012-05-25

    Daniel L. Reger, Andrea Eva Pascui, Mark D. Smith

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  26. Halide and Hydroxide Linearly Bridged Bimetallic Copper(II) Complexes: Trends in Strong Antiferromagnetic Superexchange Interactions

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  27. Synthesis, structural, and biological evaluation of the arene-linked pyrazolyl methane ligands and their d9/d10 metal complexes

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  28. Dinuclear Complexes Containing Linear M–F–M [M = Mn(II), Fe(II), Co(II), Ni(II), Cu(II), Zn(II), Cd(II)] Bridges: Trends in Structures, Antiferromagnetic Superexchange Interactions, and Spectroscopic Properties

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  29. Self-assembly of transition metal ion complexes of a hybrid pyrazine–terpyridine ligand

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  30. Group 11 complexes with the bidentate di(1H-indazol-1-yl)methane and di(2H-indazol-2-yl)methane) ligands

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  31. Rhodium and Iridium Complexes with a New Scorpionate Phosphane Ligand

    Inorganic Chemistry · 2013-06-13

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  32. Di‐ and Tetranuclear Complexes of Bis‐Tetradentate Pyrimidine‐Based Ligands with All‐Methylene‐ Versus Mixed Methylene/Ethylene‐Linked Arms

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  33. Zinc(II) and Cadmium(II) Monohydroxide Bridged, Dinuclear Metallacycles: A Unique Case of Concerted Double Berry Pseudorotation

    Inorganic Chemistry · 2013-09-09

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  34. Synthesis, Structure, and Reactivity of a Terminal Organozinc Fluoride Compound: Hydrogen Bonding, Halogen Bonding, and Donor–Acceptor Interactions

    Journal of the American Chemical Society · 2013-12-10

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  35. Structure, Stability, and Catalytic Activity of Fluorine-Bridged Complexes IPr·GaCl2(μ-F)EFn–1 (EFn– = SbF6–, PF6–, or BF4–)

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  36. Dinuclear Metallacycles with Single M–O(H)–M Bridges [M = Fe(II), Co(II), Ni(II), Cu(II)]: Effects of Large Bridging Angles on Structure and Antiferromagnetic Superexchange Interactions

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  37. Beyond the Balz–Schiemann Reaction: The Utility of Tetrafluoroborates and Boron Trifluoride as Nucleophilic Fluoride Sources

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  38. Conversion of a Monodentate Amidinate–Germylene Ligand into Chelating Imine–Germanate Ligands (on Mononuclear Manganese Complexes)

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  39. Base‐Free Non‐Noble‐Metal‐Catalyzed Hydrogen Generation from Formic Acid: Scope and Mechanistic Insights

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  40. A trigonal prismatic Cu 6 -pyrazolato complex containing a μ 6 -F ligand

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  41. Fluoride-coordination chemistry in molecular and low-dimensional magnetism

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  42. How Innocent are Potentially Redox Non-Innocent Ligands? Electronic Structure and Metal Oxidation States in Iron-PNN Complexes as a Representative Case Study

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  43. The transition-metal chemistry of amidinatosilylenes, -germylenes and -stannylenes

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  44. Intramolecularly Stabilized Heavier Tetrylenes: From Monodentate to Bidentate Ligands

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  45. A Boron‐Fluorinated Tris(pyrazolyl)borate Ligand (FTp*) and Its Mono‐ and Dinuclear Copper Complexes [Cu(FTp*)2] and [Cu2(FTp*)2]: Synthesis, Structures, and DFT Calculations

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  46. Diiron(III)–μ‐Fluoro Bisporphyrins: Effect of Bridging Ligand on the Metal Spin State

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  47. A Hydrophobic Metal–Organic Framework Based on Cubane‐Type [Co 4 (μ 3 ‐F) 3 (μ 3 ‐SO 4 )] 3+ Clusters for Gas Storage and Adsorption Selectivity of Benzene over Cyclohexane

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  48. Spontaneous Si–C bond cleavage in (Triphos Si )-nickel complexes

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  49. Multiple coordination modes of a new ditopic bis(pyrazolyl)methane-based ligand

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  50. A tetranuclear fluorido-bridged iron compound: Fluoride abstraction from the tetrafluoridoborate anion

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