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RESEARCH PAPER · Journal of the American Chemical Society · 2020

Periodic Tendril Perversion and Helices in the AMoO2F3 (A = K, Rb, NH4, Tl) Family

Justin C. Hancock, Matthew Lander Nisbet, Weiguo Zhang, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

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Periodic Tendril Perversion and Helices in the AMoO2F3 (A = K, Rb, NH4, Tl) FamilyOriginalSynthesis of NaMoO3F and Na5W3O9F5 with Morphological Controllability in Non-Aqueous Solvents15Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)8Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship24RbPb 8 O 4 Cl 9 : the first alkali metal lead oxyhalide with distorted [PbO 3 Cl 3 ] and [PbOCl 5 ] mixed-anion groups6Recent advances of oxyfluorides for nonlinear optical applications69Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph31Hydrogen‐Bond‐Driven Synergistically Enhanced Hyperpolarizability: Chiral Coordination Polymers with Nonpolar Structures Exhibiting Unusually Strong Second‐Harmonic Generation87Hydrogen‐Bond‐Driven Synergistically Enhanced Hyperpolarizability: Chiral Coordination Polymers with Nonpolar Structures Exhibiting Unusually Strong Second‐Harmonic Generation19Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component22Electrochemical Crystal Growth of Titanium Oxyfluorides—A Strategy for Development of Electron-Doped Materials2Synthesis of Hydrated Ternary Lanthanide-Containing Chlorides Exhibiting X-ray Scintillation and Luminescence8Centrosymmetric Rb[Te 2 O 4 (OH) 5 ] and noncentrosymmetric K 2 [Te 3 O 8 (OH) 4 ]: metal tellurates with corner and edge-sharing (Te 4 O 18 ) 12− anion groups8Metal oxyhalides: an emerging family of nonlinear optical materials125Modeling the mechanisms for formation of helices and perversions in elastic nanofilaments through molecular dynamics0Novel layered heterobimetallic fluorides with large optical band gaps3Luminescence and Scintillation of [Nb2O2F9]3–-Dimer-Containing Oxide–Fluorides: Cs10(Nb2O2F9)3F, Cs9.4K0.6(Nb2O2F9)3F, and Cs10(Nb2O2F9)3Cl5Ultrawide Bandgap and Outstanding Second‐Harmonic Generation Response by a Fluorine‐Enrichment Strategy at a Transition‐Metal Oxyfluoride Nonlinear Optical Material51Ultrawide Bandgap and Outstanding Second‐Harmonic Generation Response by a Fluorine‐Enrichment Strategy at a Transition‐Metal Oxyfluoride Nonlinear Optical Material12One-Side Capping in Two-Dimensional WO 3 -Type Materials Leading to Strong Second-Harmonic Response29[C(NH2)3]2MoO2F4·H2O: Unique Chinese-Knot Structure Revealing Superior Nonlinear-Optical Properties19Toward Large Second-Harmonic Generation and Deep-UV Transparency in Strongly Electropositive Transition Metal Sulfates112K2(H2O)WO3F2: A new nonlinear optical material with remarkable second-harmonic generation response and enhanced laser damage threshold9Discrete Mono-, Di-, and Trinuclear Anions [MoOF5]−, [MoVOF5]2–, [MoO2F4]2–, [Mo2O2F9]−, [Mo3O3F13]−, and the Infinite Chain Anion [MoO2F3]− Obtained from Reactions of MoOF4: Synthesis and Analysis of the Structure-Chemical Relations of the Compounds4Giant Mid‐Infrared Second‐Harmonic Generation Response in a Densely‐Stacked Van Der Waals Transition‐Metal Oxychloride39Giant Mid‐Infrared Second‐Harmonic Generation Response in a Densely‐Stacked Van Der Waals Transition‐Metal Oxychloride8Mixed Anionic Tetrahedra Guided Design of New Infrared Nonlinear Optical Material Cs 3 Ga 8 S 13 Cl with High Laser‐Induced Damage Threshold26Ultrashort Phase‐Matching Wavelength and Strong Second‐Harmonic Generation in Deep‐UV‐Transparent Oxyfluorides by Covalency Reduction33Ultrashort Phase‐Matching Wavelength and Strong Second‐Harmonic Generation in Deep‐UV‐Transparent Oxyfluorides by Covalency Reduction3Positive and Negative Contribution from Lead–Oxygen Groups and Halogen Atoms to Birefringence: A First Principles Investigation4Secondary‐Bond‐Driven Construction of a Polar Material Exhibiting Strong Broad‐Spectrum Second‐Harmonic Generation and Large Birefringence9Secondary‐Bond‐Driven Construction of a Polar Material Exhibiting Strong Broad‐Spectrum Second‐Harmonic Generation and Large Birefringence41Chemical perspectives on heteroanionic compounds: a potential playground for multiferroics7Computer-aided screening of bismuth molybdates nonlinear optical crystals γ -Bi 2 MoO 63Large second harmonic generation and birefringence from extended octupolar π-conjugated structures35Exploiting the Reactivity of Metal Trifluoroacetates to Access Alkali–Niobium(V) Oxyfluorides1Curly-Cue: Geometric Methods for Highly Coiled Hair10Reactions of Binary Nitrides in Liquid Hydrogen Fluoride and the First Calcium Oxidofluoridometallate of a Group Six Element Ca[Mo2O2F9]2 ⋅ HF1K4CuO2Cl2: A new alkali metal copper oxyhalide via aqueous solution processes0Enhanced Birefringence and Excellent Thermal Stability in Two Tellurium(IV) Vanadates: KTeOVO4 and Ca2TeV2O95Size effect of cations in the A2B3O4F3 family: Based on the new member Cs2B3O4F34Syntheses, crystal structures, and electronic structures of new barium fluoromolybdates1Syntheses and Crystal Structures of the Novel Salts Sr[MoVI2O2F9]2·HF, Ba[MoVI2O2F9]2·2HF, and of Ba[MoVOF5]0Recent achievements of d0 transition-metal-based oxyfluorides: Crystal chemistry and application in second-order NLO materials101D Cobalt‐Cytidine Monophosphate Coordination Polymer Exhibiting Efficient Ultraviolet Second‐Harmonic Generation7

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  1. Synthesis of NaMoO3F and Na5W3O9F5 with Morphological Controllability in Non-Aqueous Solvents

    Inorganic Chemistry · 2020-07-21

    Yusuke Asakura, Tomoyo Akahira, Makoto Kobayashi, Minoru Osada, Shu Yin

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  2. Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)

    Solid State Sciences · 2020-08-07

    Navindra Keerthisinghe, Vladislav V. Klepov, Eric Zhang, Mark D. Smith, Shani Egodawatte, Stephen H. Foulger, Hans‐Conrad zur Loye

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  3. Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship

    European Journal of Inorganic Chemistry · 2020-12-22

    Hongil Jo, Xinglong Chen, Hee‐Seung Lee, Kang Min Ok

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  4. RbPb 8 O 4 Cl 9 : the first alkali metal lead oxyhalide with distorted [PbO 3 Cl 3 ] and [PbOCl 5 ] mixed-anion groups

    Dalton Transactions · 2021-01-01

    Zhongxu Fan, Chen Bai, Hongsheng Shi, Min Zhang, Bei Zhang, Jun Zhang, Junjie Li

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  5. Recent advances of oxyfluorides for nonlinear optical applications

    Inorganic Chemistry Frontiers · 2021-01-01

    Shuo Bai, Dan Wang, Hongkun Liu, Ying Wang

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  6. Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph

    Chemistry of Materials · 2021-02-25

    Hongil Jo, Min Hyung Lee, Kang Min Ok

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  7. Hydrogen‐Bond‐Driven Synergistically Enhanced Hyperpolarizability: Chiral Coordination Polymers with Nonpolar Structures Exhibiting Unusually Strong Second‐Harmonic Generation

    Angewandte Chemie International Edition · 2021-06-07

    Joonhyuk Kee, Kang Min Ok

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  8. Hydrogen‐Bond‐Driven Synergistically Enhanced Hyperpolarizability: Chiral Coordination Polymers with Nonpolar Structures Exhibiting Unusually Strong Second‐Harmonic Generation

    Angewandte Chemie · 2021-06-07

    Joonhyuk Kee, Kang Min Ok

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  9. Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component

    Journal of the American Chemical Society · 2021-07-26

    Vladislav V. Klepov, Kristen A. Pace, Anna A. Berseneva, Justin B. Felder, Stuart Calder, Gregory W. Morrison, Qiang Zhang, Melanie Kirkham, David Parker, Hans‐Conrad zur Loye

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  10. Electrochemical Crystal Growth of Titanium Oxyfluorides—A Strategy for Development of Electron-Doped Materials

    Inorganic Chemistry · 2021-08-31

    Yusuke Chiba, Kengo Shibata, Hiroshi Takatsu, Kotaro Fujii, Miwa Saito, Hiroshi Kageyama, Kazuhiko Maeda, Masatomo Yashima, Teruki Motohashi

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  11. Synthesis of Hydrated Ternary Lanthanide-Containing Chlorides Exhibiting X-ray Scintillation and Luminescence

    Inorganic Chemistry · 2021-10-07

    Gyanendra B. Ayer, Mark D. Smith, Luiz Gustavo Jacobsohn, Gregory W. Morrison, Hunter B. Tisdale, Logan S. Breton, Weiguo Zhang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  12. Centrosymmetric Rb[Te 2 O 4 (OH) 5 ] and noncentrosymmetric K 2 [Te 3 O 8 (OH) 4 ]: metal tellurates with corner and edge-sharing (Te 4 O 18 ) 12− anion groups

    Inorganic Chemistry Frontiers · 2022-01-01

    Dandan Wang, Pifu Gong, Xinyuan Zhang, Zheshuai Lin, Zhanggui Hu, Yicheng Wu

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  13. Metal oxyhalides: an emerging family of nonlinear optical materials

    Chemical Science · 2022-01-01

    Xinglong Chen, Kang Min Ok

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  14. Modeling the mechanisms for formation of helices and perversions in elastic nanofilaments through molecular dynamics

    Polymer Bulletin · 2022-01-10

    J. P. T. Lopes, F. Vistulo de Abreu, Ricardo Simões

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  15. Novel layered heterobimetallic fluorides with large optical band gaps

    Journal of Solid State Chemistry · 2022-02-02

    Belal Ahmed, Kang Min Ok

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  16. Luminescence and Scintillation of [Nb2O2F9]3–-Dimer-Containing Oxide–Fluorides: Cs10(Nb2O2F9)3F, Cs9.4K0.6(Nb2O2F9)3F, and Cs10(Nb2O2F9)3Cl

    Inorganic Chemistry · 2022-02-09

    Gyanendra B. Ayer, Gregory W. Morrison, Mark D. Smith, Luiz Gustavo Jacobsohn, Hans‐Conrad zur Loye

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  17. Ultrawide Bandgap and Outstanding Second‐Harmonic Generation Response by a Fluorine‐Enrichment Strategy at a Transition‐Metal Oxyfluoride Nonlinear Optical Material

    Angewandte Chemie International Edition · 2022-03-17

    Tianhui Wu, Xingxing Jiang, Chao Wu, Yilei Hu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  18. Ultrawide Bandgap and Outstanding Second‐Harmonic Generation Response by a Fluorine‐Enrichment Strategy at a Transition‐Metal Oxyfluoride Nonlinear Optical Material

    Angewandte Chemie · 2022-03-17

    Tianhui Wu, Xingxing Jiang, Chao Wu, Yilei Hu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  19. One-Side Capping in Two-Dimensional WO 3 -Type Materials Leading to Strong Second-Harmonic Response

    Chemistry of Materials · 2022-03-29

    Haonan Liu, Hongping Wu, Zhanggui Hu, Jiyang Wang, Yicheng Wu, Hongwei Yu

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  20. [C(NH2)3]2MoO2F4·H2O: Unique Chinese-Knot Structure Revealing Superior Nonlinear-Optical Properties

    Inorganic Chemistry · 2022-09-07

    Wei Zeng, Yao Tian, Ling Huang, Hongmei Zeng, Zhien Lin, Guohong Zou

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  21. Toward Large Second-Harmonic Generation and Deep-UV Transparency in Strongly Electropositive Transition Metal Sulfates

    Journal of the American Chemical Society · 2023-01-12

    Chao Wu, Chunbo Jiang, Guangfeng Wei, Xingxing Jiang, Zujian Wang, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  22. K2(H2O)WO3F2: A new nonlinear optical material with remarkable second-harmonic generation response and enhanced laser damage threshold

    Journal of Alloys and Compounds · 2023-02-14

    Hong‐Xin Tang, Ruibiao Fu, Zuju Ma, Xintao Wu

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  23. Discrete Mono-, Di-, and Trinuclear Anions [MoOF5]−, [MoVOF5]2–, [MoO2F4]2–, [Mo2O2F9]−, [Mo3O3F13]−, and the Infinite Chain Anion [MoO2F3]− Obtained from Reactions of MoOF4: Synthesis and Analysis of the Structure-Chemical Relations of the Compounds

    Inorganic Chemistry · 2023-08-09

    Tobias Burghardt Wassermann, Riane E. Stene, Benjamin Scheibe, Antti J. Karttunen, Florian Kraus

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  24. Giant Mid‐Infrared Second‐Harmonic Generation Response in a Densely‐Stacked Van Der Waals Transition‐Metal Oxychloride

    Angewandte Chemie International Edition · 2023-08-23

    Congcong Jin, Xingxing Jiang, Chao Wu, Kaining Duanmu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  25. Giant Mid‐Infrared Second‐Harmonic Generation Response in a Densely‐Stacked Van Der Waals Transition‐Metal Oxychloride

    Angewandte Chemie · 2023-08-23

    Congcong Jin, Xingxing Jiang, Chao Wu, Kaining Duanmu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  26. Mixed Anionic Tetrahedra Guided Design of New Infrared Nonlinear Optical Material Cs 3 Ga 8 S 13 Cl with High Laser‐Induced Damage Threshold

    Advanced Optical Materials · 2023-09-10

    Linan Wang, Chenchen Tu, Jiazheng Zhou, Yu Chu, Zhihua Yang, Shilie Pan, Junjie Li

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  27. Ultrashort Phase‐Matching Wavelength and Strong Second‐Harmonic Generation in Deep‐UV‐Transparent Oxyfluorides by Covalency Reduction

    Angewandte Chemie International Edition · 2023-11-06

    Yilei Hu, Chao Wu, Xingxing Jiang, Kaining Duanmu, Zhipeng Huang, Zheshuai Lin, Mark Graeme Humphrey, Chi Zhang

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  28. Ultrashort Phase‐Matching Wavelength and Strong Second‐Harmonic Generation in Deep‐UV‐Transparent Oxyfluorides by Covalency Reduction

    Angewandte Chemie · 2023-11-06

    Yilei Hu, Chao Wu, Xingxing Jiang, Kaining Duanmu, Zhipeng Huang, Zheshuai Lin, Mark Graeme Humphrey, Chi Zhang

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  29. Positive and Negative Contribution from Lead–Oxygen Groups and Halogen Atoms to Birefringence: A First Principles Investigation

    Nanomaterials · 2023-11-28

    Can Deng, Jialong Wang, Mei Hu, Xiuhua Cui, Haiming Duan, Peng Li, Ming‐Hsien Lee

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  30. Secondary‐Bond‐Driven Construction of a Polar Material Exhibiting Strong Broad‐Spectrum Second‐Harmonic Generation and Large Birefringence

    Angewandte Chemie · 2023-12-20

    Tianhui Wu, Xingxing Jiang, Kaining Duanmu, Chao Wu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  31. Secondary‐Bond‐Driven Construction of a Polar Material Exhibiting Strong Broad‐Spectrum Second‐Harmonic Generation and Large Birefringence

    Angewandte Chemie International Edition · 2023-12-20

    Tianhui Wu, Xingxing Jiang, Kaining Duanmu, Chao Wu, Zheshuai Lin, Zhipeng Huang, Mark Graeme Humphrey, Chi Zhang

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  32. Chemical perspectives on heteroanionic compounds: a potential playground for multiferroics

    Materials Chemistry Frontiers · 2024-01-01

    Karishma Prasad, Vivian Nguyen, Bingheng Ji, Jasmine Quah, Danielle Goodwin, Jian Wang

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  33. Computer-aided screening of bismuth molybdates nonlinear optical crystals γ -Bi 2 MoO 6

    Inorganic Chemistry Frontiers · 2024-01-01

    Xuefan Wang, Yan Xiao, Wenjing Tan, Hongbo Huang, Daqing Yang, Ying Wang, Bingbing Zhang

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  34. Large second harmonic generation and birefringence from extended octupolar π-conjugated structures

    Chemical Science · 2024-01-01

    Danyang Dou, Bingbing Zhang, Daqing Yang, Ying Wang

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  35. Exploiting the Reactivity of Metal Trifluoroacetates to Access Alkali–Niobium(V) Oxyfluorides

    Inorganic Chemistry · 2024-06-10

    Marcos R. Imer, Regina G. Szlag, Benjamin D. E. Oreskovic, Esteban Urones‐Garrote, Susana García‐Martín, Federico A. Rabuffetti

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  36. Curly-Cue: Geometric Methods for Highly Coiled Hair

    SIGGRAPH Asia Conference Papers · 2024-12-03

    Haomiao Wu, Alvin Shi, A. M. Darke, Theodore Kim

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  37. Reactions of Binary Nitrides in Liquid Hydrogen Fluoride and the First Calcium Oxidofluoridometallate of a Group Six Element Ca[Mo2O2F9]2 ⋅ HF

    European Journal of Inorganic Chemistry · 2025-01-07

    Tobias Burghardt Wassermann, Lukas Link, Rainer Niewa, Antti J. Karttunen, Florian Kraus

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  38. K4CuO2Cl2: A new alkali metal copper oxyhalide via aqueous solution processes

    Solid State Sciences · 2025-02-22

    Li Zhang, Junliang Sun, Xianji Qiao

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  39. Enhanced Birefringence and Excellent Thermal Stability in Two Tellurium(IV) Vanadates: KTeOVO4 and Ca2TeV2O9

    Inorganic Chemistry · 2025-02-25

    Tingyu Wang, Han Luo, Shunke Zhang, Ling Huang, Liling Cao, Xuehua Dong, Guohong Zou

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  40. Size effect of cations in the A2B3O4F3 family: Based on the new member Cs2B3O4F3

    Materials Today Chemistry · 2025-03-06

    Bingliang Cheng, Wenjuan Ma, Abudukadi Tudi, Fangfang Zhang, Xifa Long, Shilie Pan, Yun Mo Yang

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  41. Syntheses, crystal structures, and electronic structures of new barium fluoromolybdates

    Journal of Solid State Chemistry · 2025-06-26

    Jie Ling, Chloe Jones, Oluwasegun Yusuf Raji, Mohammed Al‐Fahdi, Jackson Jones, Ming Hu

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  42. Syntheses and Crystal Structures of the Novel Salts Sr[MoVI2O2F9]2·HF, Ba[MoVI2O2F9]2·2HF, and of Ba[MoVOF5]

    European Journal of Inorganic Chemistry · 2025-08-07

    Tobias Burghardt Wassermann, Giuliana Hoß, Antti J. Karttunen, Florian Kraus

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  43. Recent achievements of d0 transition-metal-based oxyfluorides: Crystal chemistry and application in second-order NLO materials

    Coordination Chemistry Reviews · 2025-11-06

    Tianhui Wu, Jiahang Liu, Meiqi Liu, Xuan Li, Miao Zhang, Weiwei Cao, Jianmin Gu, Desong Wang

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  44. 1D Cobalt‐Cytidine Monophosphate Coordination Polymer Exhibiting Efficient Ultraviolet Second‐Harmonic Generation

    Chemistry - A European Journal · 2026-02-09

    Mubashar Ilyas, Lin Xiong, Li Zhang, Maida, Maroof Ahmad Khan, Muhammad Abbas, Nagesh Manurkar, Mudassar Ilyas, Niu Zhang, Hui Li

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