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RESEARCH PAPER · ACS Sustainable Chemistry & Engineering · 2021

Tandem Heterogeneous Catalysis for Polyethylene Depolymerization via an Olefin-Intermediate Process

Lucas D. Ellis, Sara V. Orski, Grace A. Kenlaw, Andrew G. Norman, Kathryn L. Beers, Yuriy Román‐Leshkov, Gregg T. Beckham

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Tandem Heterogeneous Catalysis for Polyethylene Depolymerization via an Olefin-Intermediate ProcessOriginalNanocatalyzed Upcycling of the Plastic Wastes for a Circular Economy123Breaking C–C Bonds via Electrochemically Mediated Hydrogen Atom Transfer Reactions1Waste to Wealth: Chemical Recycling and Chemical Upcycling of Waste Plastics for a Great Future320Recent Progress in the Chemical Upcycling of Plastic Wastes298Hydrogenolysis of Polypropylene and Mixed Polyolefin Plastic Waste over Ru/C to Produce Liquid Alkanes288Recent Advancements in Plastic Packaging Recycling: A Mini-Review151Polyethylene Hydrogenolysis at Mild Conditions over Ruthenium on Tungstated Zirconia292Polyolefin plastic waste hydroconversion to fuels, lubricants, and waxes: a comparative study145Scalable Synthesis of Pt/SrTiO3 Hydrogenolysis Catalysts in Pursuit of Manufacturing-Relevant Waste Plastic Solutions44Electrochemical Activation of C−C Bonds through Mediated Hydrogen Atom Transfer Reactions63Polymer waste surgical masks decorated by superhydrophobic metal-organic frameworks towards oil spills clean-up37Catalytic conversion of SPW and products upgrading9Population balance models for polymer upcycling: signatures of the mechanism in the molecular weight evolution22Methodological development for the structural elucidation of natural and synthetic insoluble polymers by chemical depolymerization and ultra-high-resolution mass spectrometry0A High‐Throughput Approach to Repurposing Olefin Polymerization Catalysts for Polymer Upcycling32A High‐Throughput Approach to Repurposing Olefin Polymerization Catalysts for Polymer Upcycling0Critical advances and future opportunities in upcycling commodity polymers1324Sustainable chemical upcycling of waste polyolefins by heterogeneous catalysis127Upgrading of polyethylene to hydrocarbon fuels over the Fe-modified Pt/Al2O3 catalysts at a mild condition without external H245Upcycling Plastic Wastes into Value‐Added Products by Heterogeneous Catalysis112Reactive Molecular Dynamics Simulations of the Depolymerization of Polyethylene Using Graphene-Oxide-Supported Platinum Nanoparticles12Biodegradation of polyethylene and polystyrene: From microbial deterioration to enzyme discovery369Multiscale modeling of hydrogenolysis of ethane and propane on Ru(0001): Implications for plastics recycling32Chemical Upcycling of Poly(3-hydroxybutyrate) into Bicyclic Ether–Ester Monomers toward Value-Added, Degradable, and Recyclable Poly(ether ester)45Catalytic Upcycling of Plastic Waste into High Value-added Chemicals0Unleashing the Power of Knowledge Extraction from Scientific Literature in Catalysis27Polyolefin Innovations toward Circularity and Sustainable Alternatives96A unified view on catalytic conversion of biomass and waste plastics584Metathesis, molecular redistribution of alkanes, and the chemical upgrading of low-density polyethylene44Catalytic hydrogenolysis of plastic to liquid hydrocarbons over a nickel-based catalyst78Enabling resource circularity through thermo-catalytic and solvent-based conversion of waste plastics49Catalytic deconstruction of waste polyethylene with ethylene to form propylene419Competing Time Scales in Surface-Driven Solution Depolymerization2Upcycling disposable face masks into fuel range iso-alkanes through hydropyrolysis coupled with vapor-phase hydrocracking13Ni/SiO2 catalysts for polyolefin deconstruction via the divergent hydrogenolysis mechanism121Rapid atom-efficient polyolefin plastics hydrogenolysis mediated by a well-defined single-site electrophilic/cationic organo-zirconium catalyst82Towards a Cradle‐to‐Cradle Polyolefin Lifecycle11Towards a Cradle‐to‐Cradle Polyolefin Lifecycle1Enhanced Production of Liquid Alkanes from Waste Polyethylene via the Electronic Effect‐Favored Csecondary−Csecondary Bond Cleavage42Functionalization of polyethylene with hydrolytically-stable ester groups6Heterogeneous Pt-catalyzed transfer dehydrogenation of long-chain alkanes with ethylene7Turning Polyethylene Waste to Hydrocarbons Using a Sustainable Acidic Carbocatalyst5Polyethylene Valorization by Combined Chemical Catalysis with Bioconversion by Plastic-Enriched Microbial Consortia26Strategic use of thermo-chemical processes for plastic waste valorization23Machine Learning and Informatics Based Elucidation of Reaction Pathways for Upcycling Model Polyolefin to Aromatics11Recent Advances in Catalytic Chemical Recycling of Polyolefins104Enhanced degradation of polyethylene terephthalate plastics by CdS/CeO2 heterojunction photocatalyst activated peroxymonosulfate143Up-cycling plastic waste into swellable super-sorbents34Sustainable catalytic strategies for the transformation of plastic wastes into valued products53Preparation of monocyclic aromatic hydrocarbons from chlorine-containing mixed waste plastics via tandem catalysis coupled with hydrothermal pretreatment27Degradation of Polyvinyl Chloride by Sequential Dehydrochlorination and Olefin Metathesis26Mass transfer in catalytic depolymerization: External effectiveness factors and serendipitous processivity in stagnant and stirred melts31Ab Initio Thermochemistry of Highly Flexible Molecules for Thermal Decomposition Analysis22Upcycling of polyvinyl chloride to hydrocarbon waxes via dechlorination and catalytic hydrogenation50Hydrogen-free catalytic depolymerization of waste polyolefins at mild temperatures43Structure–Property Relationships for Nickel Aluminate Catalysts in Polyethylene Hydrogenolysis with Low Methane Selectivity61Upcycling of polyethylenes by catalysis0Chemical recycling of polyolefins: a closed-loop cycle of waste to olefins126Treasuring trash: Pt/SrTiO3 catalysts process plastic waste into high-value materials25Heterogenous electromediated depolymerization of highly crystalline polyoxymethylene43Enhanced production and control of liquid alkanes in the hydrogenolysis of polypropylene over shaped Ru/CeO2 catalysts23Mechanistic study of heterogeneous propene metathesis on WOx/SiO2 catalysts13Transition Metal Catalysts for Depolymerization0Entropy Confinement Promotes Hydrogenolysis Activity for Polyethylene Upcycling72Entropy Confinement Promotes Hydrogenolysis Activity for Polyethylene Upcycling8Progress toward Sustainable Methods for Polymer Synthesis and Editing1Proteomes reveal metabolic capabilities of Yarrowia lipolytica for biological upcycling of polyethylene into high-value chemicals16Nickel and cobalt complexes with ferrocenyl Schiff bases: preparation, characterization, and application in ethylene oligomerization6Effect of chloride salts and microwaves on polyethylene terephthalate (PET) hydrolysis by iron chloride/acetic acid Lewis/Brønsted acidic deep eutectic solvent15Closed-loop recycling of semi-aromatic polyesters upcycled from poly(ethylene terephthalate)10Electrochemical C−H/C−C Bond Oxygenation: A Potential Technology for Plastic Depolymerization13Boosting strong metal-support interactions between Ru and sodium titanate nanowire for hydrogenolysis of polyolefins under mild conditions44Thiol-ene click chemistry incorporates carboxylic acid-terminated alkane pendants on polycyclooctene to tune properties14Characterization of polymer properties and identification of additives in commercially available research plastics112Computational Insights into Catalysis: Evaluating Alternative Metal Potentials in Mgcl2-Supported Ziegler-Natta Catalysts0Valorization of mixed plastics waste for the synthesis of flexible superhydrophobic films25Review on Catalytic Depolymerization of Polyolefin Waste by Hydrogenolysis: State-of-the-Art and Outlook57Significantly Tunable Foaming Behavior of Blowing Agent for the Polyethylene Foam Resin with a Unique Designed Blowing Agent System6Catalytic conversion of mixed polyolefins under mild atmospheric pressure48Visible light-induced PET degradation using red CdxZn1−xSeyS1−y quantum dots capped with two different ligands under varying pH conditions2Mechanistic Pathways for the Dehydrogenation of Alkanes on Pt(111) and Ru(0001) Surfaces7Upcycling Waste Plastics with a C–C Backbone by Heterogeneous Catalysis45A state-of-the-art review of multilayer packaging recycling: Challenges, alternatives, and outlook150The Overlooked Potential of Sulfated Zirconia: Reexamining Solid Superacidity Toward the Controlled Depolymerization of Polyolefins11Catalysis at the intersection of sustainable chemistry and a circular economy23Selective Upcycling of Polyethylene over Ru/H‐ZSM‐5 Bifunctional Catalyst into High‐Quality Liquid Fuel at Mild Conditions31Deconstruction of Polymers through Olefin Metathesis101Recent advances in polyolefin plastic waste upcycling via mild heterogeneous catalysis route from catalyst development to process design25Mild Catalytic Degradation of Crystalline Polyethylene Units in a Solid State Assisted by Carboxylic Acid Groups23Recycling the polyethylene into fuels via an olefin-intermediate tandem catalysis over Fe2O3/USY catalysts3Copolymerization of Olefins and Conjugated Dienes: A Promising Approach to Produce Recyclable Polyolefins14Advances in Nonreactive Polymer Compatibilizers for Commodity Polyolefin Blends102Enhanced activation of peroxymonosulfate by ZIF-67/g-C3N4 S-scheme photocatalyst under visible light assistance for degradation of polyethylene terephthalate22Catalytic Upcycling of Polyolefins316Tracking Chain Populations and Branching Structure during Polyethylene Deconstruction Processes12Polyolefin waste to light olefins with ethylene and base-metal heterogeneous catalysts151N2O deconstruction of polycyclooctene to generate carbonyl-functionalized macromonomers3Selective Upcycling of Polyolefins into High-Value Nitrogenated Chemicals80Installing a Trigger to Upcycle High-Density Polyethylene42Homogeneously catalyzed oxidations to produce chemical intermediates (pharmaceuticals, agrochemicals, and plastics)0Close-loop chemical recycling unlocked via waste polyolefins-ethylene co-metathesis2Hydroesterification of Polycyclooctene to Access Linear Ethylene Ethyl Acrylate Copolymers as a Step Toward Polyolefin Functionalization6Plastic Degradation and Conversion by Photocatalysis10Plastic Degradation and Conversion by Photocatalysis (Volume 2): From Waste to Wealth3Catalytic materials based on metals (ions) used in the upcycling of plastics and polymers into fuels and valuable chemicals as part of sustainable development23Kinetic Models for Polymer Upcycling by Tag-and-Cut Strategies6Heterogeneous catalysis strategies for polyolefin plastic upcycling: co-reactant-assisted and direct transformation under mild conditions15Depolymerization by transition metal complexes: strategic approaches to convert polymeric waste into feedstocks3Circular plastic economy for sustainable development: current advances and future perspectives49Recent developments in recycling of post-consumer polyethylene waste33Selective hydrocracking of polyolefin waste into branched liquid fuels over a non-noble metal bifunctional Ni–W/ZrO 2 catalyst4Ruthenium‐Catalyzed Deconstruction of Polyolefins: A Strategy to Up‐cycle Waste Polyethylene to Value‐Added Alkene1Ruthenium‐Catalyzed Deconstruction of Polyolefins: A Strategy to Up‐cycle Waste Polyethylene to Value‐Added Alkene20Effects of Pretreatment Conditions and Branched Alkanes on Mo/MCM-41 Catalysts in Tandem Alkane Cross-metathesis for Non-hydrogen Polyolefin Recycling3Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis25Advances and Challenges in Low‐Temperature Upcycling of Waste Polyolefins via Tandem Catalysis2Versatile C─H Alkylation and Alkylidenation via Catalytic Alkylidene Transfer of Enones2Versatile C─H Alkylation and Alkylidenation via Catalytic Alkylidene Transfer of Enones0The role of the Pt-group dehydrogenation catalyst in alkane metathesis for polyolefin deconstruction9Optimization of low-temperature catalytic cracking of polyolefin waste in open-batch reactors using zeolite beta with controlled intrinsic properties20Upcycling of Waste Plastics into Value-Added Chemicals6Zeolites in the epoch of catalytic recycling plastic waste: Toward circular economy and sustainability20Advances in reaction coupling technologies for efficient conversion of low-carbon molecules1Co-recycling of plastics and other waste materials70Synergistic Catalysis for Recycling and Upcycling of Plastics35Advancements in the production methods and recycling of multilayer plastics with sustainable applications: A comprehensive review19Coordinating cracking and hydrogenation of polyethylene waste via acid-metal site isolation for selective hydrocarbon production10The role of H2 donation in heterogeneous Mo-based olefin metathesis site creation0Catalysis for the Energy Transition8Ternary-Active NiO–NiAl2O4–Al2O3 Nanocomposite for Selective Upcycling of Polypropylene into Liquid Branched Olefins8Catalytic Depolymerization of Plastics to Valuable Products7Functionalizations of C─H and C═C Bonds in Polyolefins Catalyzed by Transition‐Metal Complexes14Nature-Inspired Ag/TiO₂ Nanoparticles: Fighting Drug Pollution and Infections Sustainably1Hydrogen-Free Catalytic Strategies for the Upcycling of Polyolefin Plastics3Standardizing Depolymerization: Strategies and Performance Metrics5Advances in sustainable polyolefins: synthesis, chemical transformation and recycling23Plasma Catalysis for Plastic Waste Conversion into Value‐Added Products: Advancements and Perspectives11Valorization of mixed plastics via catalytic hydrogenolysis over layered multifunctional Ru/Nb-MMT catalyst0Sustainable Valorization of Polyethylene into Liquid Fuels via Fe 0 /USY-Catalyzed Hydropyrolysis: Insights into Catalyst Design and Hydrogenation Mechanisms1Supported Organoiridium-Pincer Catalysts for the Nonoxidative Dehydrogenation of High-Density Polyethylene1Regulating the Short-Chain Branching Structures of Polyethylene by Liquid Propane Flash in a Bimetallic Catalytic System0A self-regenerative Sn–W/γ-Al 2 O 3 catalyst for low-carbon and scalable polyolefin upcycling via tandem dehydrogenation–metathesis2In Situ Catalytic Pyrolysis of Spent Mulching Film over Fe/Ni/Co-Doped α-Al 2 O 3 for Light Oil and High-Value Aromatics1Carbon–carbon bond cleavage for lignin and plastics deconstruction0Interfacial electronic coupling engineering in Pt/WO x –Al 2 O 3 for hydrogen-free polyolefin upcycling0Recent Advances in Earth-Abundant Metal-Catalyzed Oxidative Degradation of Polyolefins0Sustainable Solutions for Microplastic/Microfiber Pollution Management0Circularity in polyethylene waste management through multidimensional integration3Heterogeneous olefin metathesis promotion using molecular hydrogen0A single catalyst solution: unraveling propane-to-propene conversion over WOx/SiO2 catalysts combining DFT and microkinetic modeling study0

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