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RESEARCH PAPER · Inorganic Chemistry · 1999

The Polar [WO2F4]2- Anion in the Solid State

Kevin R. Heier, Alexander J. Norquist, P. Shiv Halasyamani, A. Duarte, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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The Polar [WO2F4]2- Anion in the Solid StateOriginalChemInform Abstract: The Polar [WO2F4]2‐ Anion in the Solid State.021 New compounds and structures in the solid state1Polar Compounds Constructed with the [Cr2O7]2- Anion32Understanding the Role of Helical Chains in the Formation of Noncentrosymmetric Solids275The Ordered [WO2F4]2- Anion48From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds62Synthesis and molecular structure of the nitride (LOEt)Mo(N)Cl2 [LOEt=(η-C5H5)Co{P(O)(OEt)2}3]2Tungsten5Evidence for Nonpolar Alignment of [NbOF5]2- Anions in Cd(pyridine)4NbOF5 Chains24Phase transitions in oxyfluoride (NH4)2WO2F416Two-Dimensional Heisenberg Antiferromagnets: Syntheses, X-ray Structures, and Magnetic Behavior of [Cu(pz)2](ClO4)2, [Cu(pz)2](BF4)2, and [Cu(pz)2(NO3)](PF6)81Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O18Cation−Anion Interactions and Polar Structures in the Solid State196Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?0Orientational disorder in crystals of (NH4)3MoO3F3 and (NH4)3WO3F324Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F429Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions21Supramolecular assemblies prepared from an iron(II) tripodal complex, tetrafluoroborate, and alkali metal cations. The effect of cation size on coordination number, anion disorder and hydrogen bonding19Strong H···F Hydrogen Bonds as Synthons in Polymeric Quantum Magnets: Structural, Magnetic, and Theoretical Characterization of [Cu(HF2)(pyrazine)2]SbF6, [Cu2F(HF)(HF2)(pyrazine)4](SbF6)2, and [CuAg(H3F4)(pyrazine)5](SbF6)276Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions46Specific features of the structure of tungsten(VI) mononuclear six-coordinate oxohalide complexes: A review3Calorimetric and dielectric studies of the (NH4)2MoO2F4 oxyfluoride11Investigation of thermal expansion, phase diagrams, and barocaloric effect in the (NH4)2WO2F4 and (NH4)2MoO2F4 oxyfluorides55Hydrolysis of ammonium oxofluorotungstates: A 19F, 17O and 183W NMR study4Low-temperature synthesis and structural properties of ferroelectric K3WO3F3 elpasolite12NMR and DFT study of chemical bonding of the titanyl ion in pentafluoro complexes (NH4)3TiOF5 and Rb2KTiOF57Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques8A3V5O14 (A = K+, Rb+, or Tl+), New Polar Oxides with a Tetragonal Tungsten Bronze Related Structural Topology: Synthesis, Structure, and Functional Properties76New Layered Oxide-Fluoride Perovskites: KNaNbOF5 and KNaMO2F4 (M = Mo6+, W6+)43Mixed metalII–metalIV hybrid fluorides11Synthesis, Characterization, and Structure–Property Relationships in Two New Polar Oxides: Zn2(MoO4)(SeO3) and Zn2(MoO4)(TeO3)80Anisotropic Thermal Properties of the Nonlinear Optical and Polar Oxide Material Na2TeW2O931BiO(IO3): A New Polar Iodate that Exhibits an Aurivillius-Type (Bi2O2)2+ Layer and a Large SHG Response507The role of structural and nonstructural water in oxyfluoride K2WO2F4 · H2O2New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)50Exploration on anion ordering, optical properties and electronic structure in K3WO3F3 elpasolite140Orientational order of [VOF5]2− and [NbOF5]2− polar units in chains40Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)7Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)47Chemistry of Polar Transition-Metal Oxides1Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)16Synthesis, Structure, and Characterization of Two New Polar Sodium Tungsten Selenites: Na2(WO3)3(SeO3)·2H2O and Na6(W6O19)(SeO3)247Ba2YFeO5.5: A Ferromagnetic Pyroelectric Phase Prepared by Topochemical Oxidation.17Self-assembly, geometric and electronic structures, and structure-directing properties of organic–inorganic hybrid salt containing [WO2F4]2− anions and protonated 2-(2-hydroxyphenyl)benzimidazole cations0AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties22Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model16Influence of the Molecular Groups Ordering on Structural Phase Transitions in (NH4)2WO2F4 Crystal10Polar Alignment of Λ-Shaped Basic Building Units within Transition Metal Oxide Fluoride Materials15On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units55Crystal structure and phase transition in (NH4)3WO2F5: from dynamic to static orientational disorder5Anion order in perovskites: a group-theoretical analysis38On the identification of oxygen and fluorine atoms in disordered inorganic oxyfluoride compounds8Temperature-Independent, Large Dielectric Constant Induced by Vacancy and Partial Anion Order in the Oxyfluoride Pyrochlore Pb2Ti2O6−δF2δ42The structure and phase transitions in oxyfluoride (ND4)2MoO2F44Directed Lifting of Inversion Symmetry in Ruddlesden–Popper Oxide–Fluorides: Toward Ferroelectric and Multiferroic Behavior57Cd3(MoO4)(TeO3)2: A Polar 3D Compound Containing d10–d0 SCALP-Effect Cations85Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships16A series of oxyfluoride chains containing asymmetric basic building units of both early- and late-transition metal cations5PbCdF(SeO 3 )(NO 3 ): A Nonlinear Optical Material Produced by Synergistic Effect of Four Functional Units52Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands9Polar Molecule-Based Material with Optic–Electric Switching Constructed by Polar Anions21Novel layered heterobimetallic fluorides with large optical band gaps3Enhanced CO 2 sorption properties in a polarizable [WO 2 F 4 ] 2− -pillared physisorbent under direct air capture conditions8Optimal Binding Affinity for Sieving Separation of Propylene from Propane in an Oxyfluoride Anion-Based Metal–Organic Framework131Synthesis, Anion Disordering and Electronic Structure of Rb2KWO3F3 Elpasolite0

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  1. ChemInform Abstract: The Polar [WO2F4]2‐ Anion in the Solid State.

    ChemInform · 1999-05-11

    Kevin R. Heier, Alexander J. Norquist, P. Shiv Halasyamani, A. Duarte, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  2. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2000-01-01

    William T. A. Harrison

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  3. Polar Compounds Constructed with the [Cr2O7]2- Anion

    Inorganic Chemistry · 2001-03-16

    Alexander J. Norquist, Kevin R. Heier, P. Shiv Halasyamani, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  4. Understanding the Role of Helical Chains in the Formation of Noncentrosymmetric Solids

    Journal of the American Chemical Society · 2001-07-11

    Paul A. Maggard, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  5. The Ordered [WO2F4]2- Anion

    Inorganic Chemistry · 2001-09-18

    Margaret E. Welk, Alexander J. Norquist, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  6. From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds

    Inorganic Chemistry · 2002-07-24

    Paul A. Maggard, Amy L. Kopf, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier, Kang Min Ok, P. Shiv Halasyamani

    Read original paper ↗ ·

  7. Synthesis and molecular structure of the nitride (LOEt)Mo(N)Cl2 [LOEt=(η-C5H5)Co{P(O)(OEt)2}3]

    Journal of Organometallic Chemistry · 2002-11-01

    Francisco Montilla, Agustı́n Galindo, Ángeles Monge, Enrique Gutiérrez‐Puebla

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  8. Tungsten

    Elsevier eBooks · 2003-01-01

    Taka‐aki Okamura, Norikazu Ueyama

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  9. Evidence for Nonpolar Alignment of [NbOF5]2- Anions in Cd(pyridine)4NbOF5 Chains

    Crystal Growth & Design · 2005-10-29

    P. Guillory, Janet E. Kirsch, Heather K. Izumi, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  10. Phase transitions in oxyfluoride (NH4)2WO2F4

    Physics of the Solid State · 2006-01-01

    S. V. Mel’nikova, Valentina D. Fokina, N. M. Laptash

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  11. Two-Dimensional Heisenberg Antiferromagnets: Syntheses, X-ray Structures, and Magnetic Behavior of [Cu(pz)2](ClO4)2, [Cu(pz)2](BF4)2, and [Cu(pz)2(NO3)](PF6)

    Inorganic Chemistry · 2007-04-14

    F. Matthew Woodward, P. J. Gibson, Geoffrey B. Jameson, Christopher P. Landee, Mark M. Turnbull, Roger DuWayne Willett

    Read original paper ↗ ·

  12. Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O

    Crystal Growth & Design · 2007-04-18

    Margaret E. Welk, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier, Alexander J. Norquist

    Read original paper ↗ ·

  13. Cation−Anion Interactions and Polar Structures in the Solid State

    Journal of the American Chemical Society · 2007-10-18

    Michael R. Marvel, Julien Lesage, Jaewook Baek, P. Shiv Halasyamani, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  14. Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?

    MRS Proceedings · 2008-01-01

    Rachelle Ann F. Pinlac, Michael R. Marvel, Julien Lesage, Kenneth Reinhard Poeppelmeier

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  15. Orientational disorder in crystals of (NH4)3MoO3F3 and (NH4)3WO3F3

    Acta Crystallographica Section B Structural Science · 2008-05-15

    Anatoly A. Udovenko, N. M. Laptash

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  16. Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F4

    Acta Crystallographica Section B Structural Science · 2008-11-13

    Anatoly A. Udovenko, N. M. Laptash

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  17. Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions

    Dalton Transactions · 2009-01-01

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

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  18. Supramolecular assemblies prepared from an iron(II) tripodal complex, tetrafluoroborate, and alkali metal cations. The effect of cation size on coordination number, anion disorder and hydrogen bonding

    CrystEngComm · 2009-01-01

    Luigi J. Alvarado, C. Brewer, Greg A. Brewer, Ray John Butcher, Alison Straka, Carol Viragh

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  19. Strong H···F Hydrogen Bonds as Synthons in Polymeric Quantum Magnets: Structural, Magnetic, and Theoretical Characterization of [Cu(HF2)(pyrazine)2]SbF6, [Cu2F(HF)(HF2)(pyrazine)4](SbF6)2, and [CuAg(H3F4)(pyrazine)5](SbF6)2

    Journal of the American Chemical Society · 2009-03-16

    Jamie L. Manson, John A. Schlueter, Kylee Funk, H.I. Southerland, Brendan Twamley, Tom Lancaster, Stephen J. Blundell, Peter J. Baker, Francis Laurence Pratt, John Singleton, R. McDonald, Paul Goddard, Pinaki Sengupta, Cristian D. Batista, Letian Ding, Changhoon Lee, Myung‐Hwan Whangbo, Isabel Franke, Susan Cox, Chris Baines, D. Trial

    Read original paper ↗ ·

  20. Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions

    Zeitschrift für anorganische und allgemeine Chemie · 2009-04-08

    Michael R. Marvel, Rachelle Ann F. Pinlac, Julien Lesage, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  21. Specific features of the structure of tungsten(VI) mononuclear six-coordinate oxohalide complexes: A review

    Crystallography Reports · 2009-09-01

    В.С. Сергиенко, В. Л. Абраменко, Andrei V. Churakov

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  22. Calorimetric and dielectric studies of the (NH4)2MoO2F4 oxyfluoride

    Physics of the Solid State · 2010-01-01

    Valentina D. Fokina, Evgeniy V. Bogdanov, Evgeniy I. Pogoreltsev, В. С. Бондарев, Igor N. Flerov, N. M. Laptash

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  23. Investigation of thermal expansion, phase diagrams, and barocaloric effect in the (NH4)2WO2F4 and (NH4)2MoO2F4 oxyfluorides

    Physics of the Solid State · 2010-01-01

    М. В. Горев, Evgeniy V. Bogdanov, Igor N. Flerov, A. G. Kocharova, N. M. Laptash

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  24. Hydrolysis of ammonium oxofluorotungstates: A 19F, 17O and 183W NMR study

    Journal of Fluorine Chemistry · 2010-02-12

    Martin A. Fedotov, V.V. Kon'shin, N. M. Laptash

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  25. Low-temperature synthesis and structural properties of ferroelectric K3WO3F3 elpasolite

    Chemical Physics Letters · 2010-05-13

    Victor V. Atuchin∥⊥, Tatiana A. Gavrilova, Valery G. Kesler, Мaxim S. Моlokeev, K. S. Aleksandrov

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  26. NMR and DFT study of chemical bonding of the titanyl ion in pentafluoro complexes (NH4)3TiOF5 and Rb2KTiOF5

    Journal of Structural Chemistry · 2010-06-01

    V. Ya. Kavun, S. G. Kozlova, И. А. Ткаченко, Svyatoslav Petrovich Gabuda

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  27. Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques

    Unknown journal · 2010-06-11

    P. Shiv Halasyamani

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  28. A3V5O14 (A = K+, Rb+, or Tl+), New Polar Oxides with a Tetragonal Tungsten Bronze Related Structural Topology: Synthesis, Structure, and Functional Properties

    Inorganic Chemistry · 2010-07-07

    Jeongho Yeon, Sang‐Hwan Kim, P. Shiv Halasyamani

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  29. New Layered Oxide-Fluoride Perovskites: KNaNbOF5 and KNaMO2F4 (M = Mo6+, W6+)

    Crystals · 2011-03-18

    Rachelle Ann F. Pinlac, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  30. Mixed metalII–metalIV hybrid fluorides

    Journal of Fluorine Chemistry · 2011-05-02

    Jérôme Lhoste, Karim Adil, Armel Le Bail, M. Leblanc, Annie Hémon‐Ribaud, V. Maisonneuve

    Read original paper ↗ ·

  31. Synthesis, Characterization, and Structure–Property Relationships in Two New Polar Oxides: Zn2(MoO4)(SeO3) and Zn2(MoO4)(TeO3)

    Inorganic Chemistry · 2011-05-10

    Sau Doan Nguyen, Sang‐Hwan Kim, P. Shiv Halasyamani

    Read original paper ↗ ·

  32. Anisotropic Thermal Properties of the Nonlinear Optical and Polar Oxide Material Na2TeW2O9

    Crystal Growth & Design · 2011-06-13

    Weiguo Zhang, P. Shiv Halasyamani, Zeliang Gao, Shanpeng Wang, Jian Wang, Xutang Tao

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  33. BiO(IO3): A New Polar Iodate that Exhibits an Aurivillius-Type (Bi2O2)2+ Layer and a Large SHG Response

    Journal of the American Chemical Society · 2011-07-21

    Sau Doan Nguyen, Jeongho Yeon, Sang‐Hwan Kim, P. Shiv Halasyamani

    Read original paper ↗ ·

  34. The role of structural and nonstructural water in oxyfluoride K2WO2F4 · H2O

    Physics of the Solid State · 2011-12-01

    S. V. Mel’nikova, Alexander D. Vasil'ev, A. G. Kocharova

    Read original paper ↗ ·

  35. New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)

    Inorganic Chemistry · 2011-12-06

    Jeongho Yeon, Sang‐Hwan Kim, Sau Doan Nguyen, Hana Lee, P. Shiv Halasyamani

    Read original paper ↗ ·

  36. Exploration on anion ordering, optical properties and electronic structure in K3WO3F3 elpasolite

    Journal of Solid State Chemistry · 2012-01-12

    Victor V. Atuchin∥⊥, L. I. Isaenko, Valery G. Kesler, Zheshuai Lin, Мaxim S. Моlokeev, Alexander Yèlisseyev, Sergey Alexandrovich Zhurkov

    Read original paper ↗ ·

  37. Orientational order of [VOF5]2− and [NbOF5]2− polar units in chains

    Journal of Solid State Chemistry · 2012-01-24

    Romain Gautier, Martin D. Donakowski, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  38. Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)

    Journal of Solid State Chemistry · 2012-02-24

    Maren Rasmussen, Christian Näther, Ulrich Bismayer, Wolfgang Bensch

    Read original paper ↗ ·

  39. Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)

    Inorganic Chemistry · 2012-08-23

    Sau Doan Nguyen, P. Shiv Halasyamani

    Read original paper ↗ ·

  40. Chemistry of Polar Transition-Metal Oxides

    Elsevier eBooks · 2013-01-01

    P. Shiv Halasyamani

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  41. Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)

    Crystal Growth & Design · 2013-01-28

    Yi-Ping Tong, Guo‐Tian Luo, Zhen Jin, You Shen, Huiru Liu

    Read original paper ↗ ·

  42. Synthesis, Structure, and Characterization of Two New Polar Sodium Tungsten Selenites: Na2(WO3)3(SeO3)·2H2O and Na6(W6O19)(SeO3)2

    Inorganic Chemistry · 2013-02-20

    Sau Doan Nguyen, P. Shiv Halasyamani

    Read original paper ↗ ·

  43. Ba2YFeO5.5: A Ferromagnetic Pyroelectric Phase Prepared by Topochemical Oxidation.

    Chemistry of Materials · 2013-04-09

    Kun Luo, Roger D. Johnson, T. Thao Tran, P. Shiv Halasyamani, Paolo G. Radaelli, Michael A. Hayward

    Read original paper ↗ ·

  44. Self-assembly, geometric and electronic structures, and structure-directing properties of organic–inorganic hybrid salt containing [WO2F4]2− anions and protonated 2-(2-hydroxyphenyl)benzimidazole cations

    Inorganic Chemistry Communications · 2013-05-14

    Zhen Jin, R.H.C. Tan, Yi-Ping Tong, Xiaodan Zheng, Yan‐Wen Lin

    Read original paper ↗ ·

  45. AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties

    Journal of the American Chemical Society · 2013-06-24

    Martin D. Donakowski, Arno L. Görne, John T. Vaughey, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  46. Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model

    Crystal Growth & Design · 2013-07-31

    Romain Gautier, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  47. Influence of the Molecular Groups Ordering on Structural Phase Transitions in (NH4)2WO2F4 Crystal

    Crystal Growth & Design · 2013-12-02

    А. С. Крылов, S. V. Goryaĭnov, N. M. Laptash, Alexander N. Vtyurin, S. V. Mel’nikova, S. N. Krylova

    Read original paper ↗ ·

  48. Polar Alignment of Λ-Shaped Basic Building Units within Transition Metal Oxide Fluoride Materials

    Inorganic Chemistry · 2013-12-12

    Michael A. Holland, Martin D. Donakowski, Eric A. Pozzi, Andrew M. Rasmussen, T. Thao Tran, Shannon E. Pease-Dodson, P. Shiv Halasyamani, Tamar Seideman, Richard P. Van Duyne, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  49. On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units

    Inorganic Chemistry · 2015-01-22

    Romain Gautier, Régis Gautier, Kelvin B. Chang, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  50. Crystal structure and phase transition in (NH4)3WO2F5: from dynamic to static orientational disorder

    Acta Crystallographica Section B Structural Science Crystal Engineering and Materials · 2015-07-23

    Anatoly A. Udovenko, N. M. Laptash

    Read original paper ↗ ·
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