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RESEARCH PAPER · Inorganic Chemistry · 2001

The Ordered [WO2F4]2- Anion

Margaret E. Welk, Alexander J. Norquist, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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The Ordered [WO2F4]2- AnionOriginalFrom Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds62Out-of-Center Distortions in d0 Transition Metal Oxide Fluoride Anions124Synthesis and molecular structure of the nitride (LOEt)Mo(N)Cl2 [LOEt=(η-C5H5)Co{P(O)(OEt)2}3]2Alignment of acentric MoO3F33− anions in a polar material: (Ag3MoO3F3)(Ag3MoO4)Cl439Probing helix formation in chains of vertex-linked octahedra44New trends in crystal engineering412Phase transitions in oxyfluoride (NH4)2WO2F416Cluster chemistry in the solid state: Structured diffuse scattering, oxide/fluoride ordering and polar behaviour in transition metal oxyfluorides35Dynamic disorder in ammonium oxofluorotungstates (NH4)2WO2F4 and (NH4)3WO3F319Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O18Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?0Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F429Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions46Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids34Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F416Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques8A3V5O14 (A = K+, Rb+, or Tl+), New Polar Oxides with a Tetragonal Tungsten Bronze Related Structural Topology: Synthesis, Structure, and Functional Properties76Synthesis, Characterization, and Structure–Property Relationships in Two New Polar Oxides: Zn2(MoO4)(SeO3) and Zn2(MoO4)(TeO3)80Anisotropic Thermal Properties of the Nonlinear Optical and Polar Oxide Material Na2TeW2O931BiO(IO3): A New Polar Iodate that Exhibits an Aurivillius-Type (Bi2O2)2+ Layer and a Large SHG Response503New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)50Synthesis, crystal and electronic structure, and theoretical investigations of charge-transfer, optical, and bonding properties of a [VF6]3− anion compound2Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)50The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)8Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)47Chemistry of Polar Transition-Metal Oxides1Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)16Investigation into phase diagrams of the fluorine-oxygen system: Ferroelastic-antiferroelectric (NH4)2WO2F4-(NH4)2MoO2F46Ba2YFeO5.5: A Ferromagnetic Pyroelectric Phase Prepared by Topochemical Oxidation.17Self-assembly, geometric and electronic structures, and structure-directing properties of organic–inorganic hybrid salt containing [WO2F4]2− anions and protonated 2-(2-hydroxyphenyl)benzimidazole cations0AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties22Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model16Synthesis and Magnetic Properties of β‐KVOF317On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units53Temperature-Independent, Large Dielectric Constant Induced by Vacancy and Partial Anion Order in the Oxyfluoride Pyrochlore Pb2Ti2O6−δF2δ42Cd3(MoO4)(TeO3)2: A Polar 3D Compound Containing d10–d0 SCALP-Effect Cations85A highly-distorted octahedron with a C 2v group symmetry inducing an ultra-intense zero phonon line in Mn 4+ -activated oxyfluoride Na 2 WO 2 F 4140Effect of Deuteration on the Thermodynamic Properties of Dioxotetrafluoromolybdate(VI), (NH4)2MoO2F41Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships16Assisting the Effective Design of Polar Iodates with Early Transition-Metal Oxide Fluoride Anions206A series of oxyfluoride chains containing asymmetric basic building units of both early- and late-transition metal cations5M 2 (SeO 3 )F 2 (M = Zn, Cd): understanding the structure directing effect of [SeO 3 ] 2− groups on constructing ordered oxyfluorides14Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands9Mixed Transition Metal (Oxy)fluoride Paramagnet Chains: Synthesis, Structure, and Characterization11Ba(B 2 OF 3 (OH) 2 ) 2 with well-ordered OH/F anions and a unique B 2 OF 3 (OH) 2 dimer30Crystal structure of an ordered [WOF5]− salt: (1,10-phen-H)[WOF5] (1,10-phen = 1,10-phenanthroline)4Chromium(VI) Oxyfluoride Dianions, [Cr2O4F6]2− and [CrO2F4]2−; Syntheses and Structures of [XeF5]2[Cr2O4F6], [XeF5]2[Cr2O4F6] ⋅ nX (X=HF, n=4; X=XeOF4, n=2), and [XeF5][Xe2F11][CrO2F4]1Studies on Three 3D Bimetallic Tellurates: Including a Second-Order NLO Material with d10-Zn2+ and SOJT-Effect Te4+/Mo6+ Cations2

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  1. From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds

    Inorganic Chemistry · 2002-07-24

    Paul A. Maggard, Amy L. Kopf, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier, Kang Min Ok, P. Shiv Halasyamani

    Read original paper ↗ ·

  2. Out-of-Center Distortions in d0 Transition Metal Oxide Fluoride Anions

    Inorganic Chemistry · 2002-09-07

    Margaret E. Welk, Alexander J. Norquist, Frederick P. Arnold, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  3. Synthesis and molecular structure of the nitride (LOEt)Mo(N)Cl2 [LOEt=(η-C5H5)Co{P(O)(OEt)2}3]

    Journal of Organometallic Chemistry · 2002-11-01

    Francisco Montilla, Agustı́n Galindo, Ángeles Monge, Enrique Gutiérrez‐Puebla

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  4. Alignment of acentric MoO3F33− anions in a polar material: (Ag3MoO3F3)(Ag3MoO4)Cl

    Journal of Solid State Chemistry · 2003-05-19

    Paul A. Maggard, Tiffany S Nault, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  5. Probing helix formation in chains of vertex-linked octahedra

    CrystEngComm · 2004-01-01

    Paul A. Maggard, Amy L. Kopf, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  6. New trends in crystal engineering

    CrystEngComm · 2005-01-01

    Dario Braga, Lee Brammer, Neil R. Champness

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  7. Phase transitions in oxyfluoride (NH4)2WO2F4

    Physics of the Solid State · 2006-01-01

    S. V. Mel’nikova, Valentina D. Fokina, N. M. Laptash

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  8. Cluster chemistry in the solid state: Structured diffuse scattering, oxide/fluoride ordering and polar behaviour in transition metal oxyfluorides

    Polyhedron · 2006-06-07

    Ray Leslie Withers, Frank Brink, Yun Liu, Lasse Norén

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  9. Dynamic disorder in ammonium oxofluorotungstates (NH4)2WO2F4 and (NH4)3WO3F3

    Journal of Structural Chemistry · 2006-07-01

    E. I. Voĭt, А. В. Войт, A. A. Mashkovskii, N. M. Laptash, V. Ya. Kavun

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  10. Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O

    Crystal Growth & Design · 2007-04-18

    Margaret E. Welk, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier, Alexander J. Norquist

    Read original paper ↗ ·

  11. Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?

    MRS Proceedings · 2008-01-01

    Rachelle Ann F. Pinlac, Michael R. Marvel, Julien Lesage, Kenneth Reinhard Poeppelmeier

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  12. Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F4

    Acta Crystallographica Section B Structural Science · 2008-11-13

    Anatoly A. Udovenko, N. M. Laptash

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  13. Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions

    Zeitschrift für anorganische und allgemeine Chemie · 2009-04-08

    Michael R. Marvel, Rachelle Ann F. Pinlac, Julien Lesage, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  14. Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids

    Crystal Growth & Design · 2010-01-08

    Haisheng Lin, Paul A. Maggard

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  15. Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F4

    Acta Crystallographica Section B Structural Science · 2010-01-22

    Anatoly A. Udovenko, Alexander D. Vasiliev, N. M. Laptash

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  16. Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques

    Unknown journal · 2010-06-11

    P. Shiv Halasyamani

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  17. A3V5O14 (A = K+, Rb+, or Tl+), New Polar Oxides with a Tetragonal Tungsten Bronze Related Structural Topology: Synthesis, Structure, and Functional Properties

    Inorganic Chemistry · 2010-07-07

    Jeongho Yeon, Sang‐Hwan Kim, P. Shiv Halasyamani

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  18. Synthesis, Characterization, and Structure–Property Relationships in Two New Polar Oxides: Zn2(MoO4)(SeO3) and Zn2(MoO4)(TeO3)

    Inorganic Chemistry · 2011-05-10

    Sau Doan Nguyen, Sang‐Hwan Kim, P. Shiv Halasyamani

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  19. Anisotropic Thermal Properties of the Nonlinear Optical and Polar Oxide Material Na2TeW2O9

    Crystal Growth & Design · 2011-06-13

    Weiguo Zhang, P. Shiv Halasyamani, Zeliang Gao, Shanpeng Wang, Jian Wang, Xutang Tao

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  20. BiO(IO3): A New Polar Iodate that Exhibits an Aurivillius-Type (Bi2O2)2+ Layer and a Large SHG Response

    Journal of the American Chemical Society · 2011-07-21

    Sau Doan Nguyen, Jeongho Yeon, Sang‐Hwan Kim, P. Shiv Halasyamani

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  21. New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)

    Inorganic Chemistry · 2011-12-06

    Jeongho Yeon, Sang‐Hwan Kim, Sau Doan Nguyen, Hana Lee, P. Shiv Halasyamani

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  22. Synthesis, crystal and electronic structure, and theoretical investigations of charge-transfer, optical, and bonding properties of a [VF6]3− anion compound

    Monatshefte für Chemie - Chemical Monthly · 2011-12-22

    Yi-Ping Tong, Hong Shu Liu, Zhen Jin, Yan‐Wen Lin

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  23. Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)

    Inorganic Chemistry · 2012-02-01

    Jeongho Yeon, Sang‐Hwan Kim, Sau Doan Nguyen, Hana Lee, P. Shiv Halasyamani

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  24. The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-27

    Martin D. Donakowski, Anastasiya I. Vinokur, Kenneth Reinhard Poeppelmeier

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  25. Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)

    Inorganic Chemistry · 2012-08-23

    Sau Doan Nguyen, P. Shiv Halasyamani

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  26. Chemistry of Polar Transition-Metal Oxides

    Elsevier eBooks · 2013-01-01

    P. Shiv Halasyamani

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  27. Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)

    Crystal Growth & Design · 2013-01-28

    Yi-Ping Tong, Guo‐Tian Luo, Zhen Jin, You Shen, Huiru Liu

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  28. Investigation into phase diagrams of the fluorine-oxygen system: Ferroelastic-antiferroelectric (NH4)2WO2F4-(NH4)2MoO2F4

    Physics of the Solid State · 2013-02-01

    Evgeniy V. Bogdanov, Evgeniy I. Pogoreltsev, S. V. Mel’nikova, М. В. Горев, Igor N. Flerov, Мaxim S. Моlokeev, A. V. Kartashev, A. G. Kocharova, N. M. Laptash

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  29. Ba2YFeO5.5: A Ferromagnetic Pyroelectric Phase Prepared by Topochemical Oxidation.

    Chemistry of Materials · 2013-04-09

    Kun Luo, Roger D. Johnson, T. Thao Tran, P. Shiv Halasyamani, Paolo G. Radaelli, Michael A. Hayward

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  30. Self-assembly, geometric and electronic structures, and structure-directing properties of organic–inorganic hybrid salt containing [WO2F4]2− anions and protonated 2-(2-hydroxyphenyl)benzimidazole cations

    Inorganic Chemistry Communications · 2013-05-14

    Zhen Jin, R.H.C. Tan, Yi-Ping Tong, Xiaodan Zheng, Yan‐Wen Lin

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  31. AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties

    Journal of the American Chemical Society · 2013-06-24

    Martin D. Donakowski, Arno L. Görne, John T. Vaughey, Kenneth Reinhard Poeppelmeier

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  32. Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model

    Crystal Growth & Design · 2013-07-31

    Romain Gautier, Kenneth Reinhard Poeppelmeier

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  33. Synthesis and Magnetic Properties of β‐KVOF3

    Zeitschrift für anorganische und allgemeine Chemie · 2014-01-23

    Martin D. Donakowski, Hongcheng Lu, Romain Gautier, Rana Saha, Athinarayanan Sundaresan, Kenneth Reinhard Poeppelmeier

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  34. On the Origin of the Differences in Structure Directing Properties of Polar Metal Oxyfluoride [MOxF6–x]2– (x = 1, 2) Building Units

    Inorganic Chemistry · 2015-01-22

    Romain Gautier, Régis Gautier, Kelvin B. Chang, Kenneth Reinhard Poeppelmeier

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  35. Temperature-Independent, Large Dielectric Constant Induced by Vacancy and Partial Anion Order in the Oxyfluoride Pyrochlore Pb2Ti2O6−δF2δ

    Chemistry of Materials · 2016-07-18

    Kengo Oka, Hajime Hojo, Masaki Azuma, Katsuyoshi Oh‐ishi

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  36. Cd3(MoO4)(TeO3)2: A Polar 3D Compound Containing d10–d0 SCALP-Effect Cations

    Inorganic Chemistry · 2016-11-09

    Yuquan Feng, Hui‐Tao Fan, Zhiguo Zhong, Hongwei Wang, Dongfang Qiu

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  37. A highly-distorted octahedron with a C 2v group symmetry inducing an ultra-intense zero phonon line in Mn 4+ -activated oxyfluoride Na 2 WO 2 F 4

    Journal of Materials Chemistry C · 2017-01-01

    Tao Hu, Hang Lin, Yao Cheng, Qingming Huang, Ju Xu, Yan Na Gao, Jiaomei Wang, Yuansheng Wang

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  38. Effect of Deuteration on the Thermodynamic Properties of Dioxotetrafluoromolybdate(VI), (NH4)2MoO2F4

    Inorganic Chemistry · 2017-05-11

    Evgeniy V. Bogdanov, Evgeniy I. Pogoreltsev, М. В. Горев, Igor N. Flerov

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  39. Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships

    Inorganic Chemistry · 2018-05-15

    Belal Ahmed, Hongil Jo, Seung‐Jin Oh, Kang Min Ok

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  40. Assisting the Effective Design of Polar Iodates with Early Transition-Metal Oxide Fluoride Anions

    Journal of the American Chemical Society · 2018-06-12

    Hongwei Yu, Matthew Lander Nisbet, Kenneth Reinhard Poeppelmeier

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  41. A series of oxyfluoride chains containing asymmetric basic building units of both early- and late-transition metal cations

    Journal of Solid State Chemistry · 2018-08-20

    Belal Ahmed, Hongil Jo, Sung Won Yoon, Kwang‐Yong Choi, Kang Min Ok

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  42. M 2 (SeO 3 )F 2 (M = Zn, Cd): understanding the structure directing effect of [SeO 3 ] 2− groups on constructing ordered oxyfluorides

    CrystEngComm · 2019-01-01

    Fengguang You, Pifu Gong, Fei Liang, Xingxing Jiang, Heng Tu, Ying Zhao, Zhanggui Hu, Zheshuai Lin

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  43. Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands

    Crystal Growth & Design · 2019-05-10

    Belal Ahmed, Hongil Jo, Kang Min Ok

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  44. Mixed Transition Metal (Oxy)fluoride Paramagnet Chains: Synthesis, Structure, and Characterization

    European Journal of Inorganic Chemistry · 2019-06-27

    Belal Ahmed, Hongil Jo, Sung Won Yoon, Kwang‐Yong Choi, Wei‐Tin Chen, F. C. Chou, Kang Min Ok

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  45. Ba(B 2 OF 3 (OH) 2 ) 2 with well-ordered OH/F anions and a unique B 2 OF 3 (OH) 2 dimer

    Chemical Communications · 2020-01-01

    Minqiang Gai, Ying Wang, Tinghao Tong, Liying Wang, Zhihua Yang, Xin Hua Zhou, Shilie Pan

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  46. Crystal structure of an ordered [WOF5]− salt: (1,10-phen-H)[WOF5] (1,10-phen = 1,10-phenanthroline)

    Acta Crystallographica Section E Crystallographic Communications · 2020-07-24

    Douglas Turnbull, Michael Gerken

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  47. Chromium(VI) Oxyfluoride Dianions, [Cr2O4F6]2− and [CrO2F4]2−; Syntheses and Structures of [XeF5]2[Cr2O4F6], [XeF5]2[Cr2O4F6] ⋅ nX (X=HF, n=4; X=XeOF4, n=2), and [XeF5][Xe2F11][CrO2F4]

    Chemistry - A European Journal · 2023-10-17

    Mark R. Bortolus, Hélène P. A. Mercier, Gary J. Schrobilgen

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  48. Studies on Three 3D Bimetallic Tellurates: Including a Second-Order NLO Material with d10-Zn2+ and SOJT-Effect Te4+/Mo6+ Cations

    Inorganic Chemistry · 2025-08-14

    Yuquan Feng, Zhiguo Zhong, Shuyang Chen, Sujuan Jin, Zhaohui Meng, Hongwei Wang

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