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RESEARCH PAPER · Chemistry of Materials · 1999

An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallizations of Open-Framework Gallium Oxyfluorophosphates with the ULM-3 and ULM-4 Structures

Richard I. Walton, Thierry Loiseau, Dermot O’Hare, Gérard Férey

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An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallizations of Open-Framework Gallium Oxyfluorophosphates with the ULM-3 and ULM-4 StructuresOriginalDynamic neutron and synchrotron X-ray powder diffraction methods in the study of chemical processes19On the advantages of the use of the three-element detector system for measuring EDXRD patterns to follow the crystallisation of open-framework structures49Synthesis, Structures, and Reactivity of Two Compounds Containing the Tancoite-like [Ga(HPO4)2F]2-∞ Chain58Crystallization of a Large-Pore Three-Dimensional Gallium Fluorophosphate under Mild Conditions37Crystallization of a Large-Pore Three-Dimensional Gallium Fluorophosphate under Mild Conditions7In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions75Crystallogenesis of microporous metallophosphates38New evidences for the fluoride contribution in synthesis of gallium phosphates2Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphateElectronic supplementary information (ESI) available: crystal data, atomic coordinates and metrical data for 1 and 2. See http://www.rsc.org/suppdata/cc/b2/b201178f/31In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions47Comparison of one-, two-, and three-dimensional iron phosphates containing ethylenediamine20Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates64Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42Solvothermal Pathways to Transition Metal Oxides0In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions32Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction57Towards understanding, control and application of layered double hydroxide chemistry582In-situ XRD as a tool to understanding zeolite crystallization105Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction15Hybrid Porous Solids34Metal-organic frameworks: the young child of the porous solids family62Hybrid porous solids: past, present, future5822Control of framework stoichiometry in MeGaPO laumontites using 1-methylimidazole as structure-directing agent5Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study210Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study47Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370The Long Story and the Brilliant Future of Crystallized Porous Solids5Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite11Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation45Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates26In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating36Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks220Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks51Characterization of the gel phases formed in the synthesis of microporous gallophosphate, cloverite3In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42Selective Sorption of Organic Molecules by the Flexible Porous Hybrid Metal−Organic Framework MIL-53(Fe) Controlled by Various Host−Guest Interactions122A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche43Surface Chemistry of Metal–Organic Frameworks at the Liquid–Solid Interface318High-surface thermally stable mesoporous gallium phosphates constituted by nanoparticles as primary building blocks4In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction47Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy368NMR and SAXS Analysis of Connectivity of Aluminum and Silicon Atoms in the Clear Sol Precursor of SSZ-13 Zeolite53Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate39Watching nanoparticle kinetics in liquid37Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Diffraction and Spectroscopy of Porous Solids1Crystallisation Kinetics of Metal Organic Frameworks From in situ Time-Resolved X-ray Diffraction59In situ 27Al NMR kinetic investigation of zeolite A crystallization24Theoretical Calculation about the High Energy Density Molecules of Nitrate Ester Substitution Derivatives of Prismane2In Situ Studies on Phase Transitions of Tris(acetylacetonato)-Aluminum(III) Al(acac)321A gel aging effect in the synthesis of open-framework gallium phosphates: structure solution and solid-state NMR of a large-pore, open-framework material7In Situ Neutron Diffraction Studies of the Flux Crystal Growth of the Reduced Molybdates La 4 Mo 2 O 11 and Ce 4 Mo 2 O 11 : Revealing Unexpected Mixed-Valent Transient Intermediates and Determining the Sequence of Events during Crystal Growth19In situ Monitoring of the Formation of [Bis(acetylacetonato)manganese(II)] Complexes10Anatomy of a complex mineral replacement reaction: Role of aqueous redox, mineral nucleation, and ion transport properties revealed by an in-situ study of the replacement of chalcopyrite by copper sulfides31Solvothermal synthesis of zirconia nanomaterials: Latest developments and future45Advanced In Situ and Operando Characterization Techniques for Zinc‐Ion Batteries18

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  1. Dynamic neutron and synchrotron X-ray powder diffraction methods in the study of chemical processes

    Journal of Materials Chemistry · 2000-01-01

    María Carmen Morón

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  2. On the advantages of the use of the three-element detector system for measuring EDXRD patterns to follow the crystallisation of open-framework structures

    Physical Chemistry Chemical Physics · 2000-01-01

    Gavin Muncaster, Andrew T. Davies, Gopinathan Sankar, C. Richard A. Catlow, John Meurig Thomas, Sally L. Colston, Paul Barnes, Richard I. Walton, Dermot M. O'Hare

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  3. Synthesis, Structures, and Reactivity of Two Compounds Containing the Tancoite-like [Ga(HPO4)2F]2-∞ Chain

    Chemistry of Materials · 2000-06-23

    Richard I. Walton, Franck Millange, Dermot M. O'Hare, Capucine Paulet, Thierry Loiseau, Gérard Férey

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  4. Crystallization of a Large-Pore Three-Dimensional Gallium Fluorophosphate under Mild Conditions

    Angewandte Chemie International Edition · 2000-12-15

    Richard I. Walton, Franck Millange, Thierry Loiseau, Dermot M. O'Hare, Gérard Férey

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  5. Crystallization of a Large-Pore Three-Dimensional Gallium Fluorophosphate under Mild Conditions

    Angewandte Chemie · 2000-12-15

    Richard I. Walton, Franck Millange, Thierry Loiseau, Dermot M. O'Hare, Gérard Férey

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  6. In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions

    Chemistry of Materials · 2001-03-20

    Lars Engelke, M. Schaefer, Melissa J. Schur, Wolfgang Bensch

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  7. Crystallogenesis of microporous metallophosphates

    Current Opinion in Solid State and Materials Science · 2001-10-01

    Françis Taulelle

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  8. New evidences for the fluoride contribution in synthesis of gallium phosphates

    Studies in surface science and catalysis · 2002-01-01

    Vasile Ion Parvulescu, C.M. Visniescu, M. Hassan Zahedi-Niaki, Serge Kaliaguine

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  9. Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphateElectronic supplementary information (ESI) available: crystal data, atomic coordinates and metrical data for 1 and 2. See http://www.rsc.org/suppdata/cc/b2/b201178f/

    Chemical Communications · 2002-03-18

    Franck Millange, Richard I. Walton, Nathalie Guillou, Thierry Loiseau, Dermot M. O'Hare, Gérard Férey

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  10. In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions

    European Journal of Inorganic Chemistry · 2003-01-20

    Lars Engelke, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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  11. Comparison of one-, two-, and three-dimensional iron phosphates containing ethylenediamine

    Journal of Solid State Chemistry · 2003-06-30

    Yanning Song, Peter Y. Zavalij, Natasha A. Chernova, Masatsugu Suzuki, M. Stanley Whittingham

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  12. Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates

    Journal of the American Chemical Society · 2004-05-08

    Alexander J. Norquist, Dermot M. O'Hare

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  13. Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)

    The Journal of Physical Chemistry B · 2004-11-24

    Thierry Loiseau, L. Beitone, Franck Millange, Françis Taulelle, Dermot M. O'Hare, Gérard Férey

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  14. Solvothermal Pathways to Transition Metal Oxides

    MRS Proceedings · 2005-01-01

    Alexej Michailovski, Greta Ricarda Patzke

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  15. In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions

    Zeitschrift für anorganische und allgemeine Chemie · 2005-02-01

    Ragnar Kiebach, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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  16. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

    Angewandte Chemie International Edition · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  17. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

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    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  18. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction

    Structure and bonding · 2005-11-08

    Gareth R. Williams, Aamir I. Khan, Dermot M. O'Hare

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  19. Towards understanding, control and application of layered double hydroxide chemistry

    Journal of Materials Chemistry · 2006-01-01

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  20. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

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  21. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction

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  22. Hybrid Porous Solids

    Studies in surface science and catalysis · 2007-01-01

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  23. Metal-organic frameworks: the young child of the porous solids family

    Studies in surface science and catalysis · 2007-01-01

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  24. Hybrid porous solids: past, present, future

    Chemical Society Reviews · 2007-09-19

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  25. Control of framework stoichiometry in MeGaPO laumontites using 1-methylimidazole as structure-directing agent

    Microporous and Mesoporous Materials · 2007-11-09

    Fabrice O. M. Gaslain, Katherine E. White, Andrew R. Cowley, CHIPPINDALE Ann Mary

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  26. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

    Angewandte Chemie International Edition · 2008-04-18

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  27. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

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  28. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

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  29. The Long Story and the Brilliant Future of Crystallized Porous Solids

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  30. Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite

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  31. Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation

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  32. Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates

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  33. In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating

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  34. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

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  35. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

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  36. Characterization of the gel phases formed in the synthesis of microporous gallophosphate, cloverite

    Journal of Materials Chemistry · 2010-01-01

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  37. In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures

    Nanoscale · 2010-01-01

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  38. Selective Sorption of Organic Molecules by the Flexible Porous Hybrid Metal−Organic Framework MIL-53(Fe) Controlled by Various Host−Guest Interactions

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  39. A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework

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  40. Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche

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  42. High-surface thermally stable mesoporous gallium phosphates constituted by nanoparticles as primary building blocks

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  43. In‐Situ Monitoring of the Formation of Crystalline Solids

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  44. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

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  45. Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction

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  46. Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy

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  47. NMR and SAXS Analysis of Connectivity of Aluminum and Silicon Atoms in the Clear Sol Precursor of SSZ-13 Zeolite

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  48. Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate

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  49. Watching nanoparticle kinetics in liquid

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  50. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

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