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REVIEW · Current Opinion in Colloid & Interface Science · 2006

In-situ XRD as a tool to understanding zeolite crystallization

Poul Norby

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In-situ XRD as a tool to understanding zeolite crystallizationOriginalHydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques0Stability of AlPO and SAPO molecular sieves during adsorption-desorption cycles of water vapor investigated by in-situ XRD measurements13Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion76Reactor design for in situ X-ray scattering studies of nanoparticle formation in supercritical water syntheses55Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates24Hydrothermal/autoclave synthesis of AlPO-5: a prototype space/time study of crystallisation gradients8Functionalisation and Structure Characterisation of Porous Silicates and Aluminophosphates4Structural and morphological evolution of β-MnO2nanorods during hydrothermal synthesis84High‐Pressure, High‐Temperature Formation of Phase‐Pure Monoclinic Zirconia Nanocrystals Studied by Time‐Resolved in situ Synchrotron X‐Ray Diffraction57Time‐Resolved In Situ Synchrotron X‐ray Study and Large‐Scale Production of Magnetite Nanoparticles in Supercritical Water83Time‐Resolved In Situ Synchrotron X‐ray Study and Large‐Scale Production of Magnetite Nanoparticles in Supercritical Water20Hydrothermal formation of tobermorite studied byin situX-ray diffraction under autoclave condition19Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method41In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating36Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques30Formation Process of Autoclaved Lightweight Concrete Studied by in situ X-ray Diffraction under Hydrothermal Condition4In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42In-Situ X-ray Diffraction under Hydrothermal Condition Using Synchrotron Radiation and Its Application to Tobermorite Formation Reaction2Methods for in situ spectroscopic probing of the synthesis of a zeolite112Modification of bone-like apatite nanoparticle size and growth kinetics by alizarin red S29The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids47In Situ Time‐Resolved X‐Ray Diffraction of Tobermorite Formation Process Under Autoclave Condition37Versatile in situ powder X-ray diffraction cells for solid–gas investigations163Anisotropic Crystal Growth Kinetics of Anatase TiO2 Nanoparticles Synthesized in a Nonaqueous Medium80Development of an in situ X-ray Diffraction System for Hydrothermal Reaction0The application of statistical methodology to the analysis of time-resolved X-ray diffraction data12In situ time-resolved X-ray diffraction of tobermorite formation in autoclaved aerated concrete: Influence of silica source reactivity and Al addition173Development of capabilities for "in situ" analysis of nanoparticles at the MCX powder diffraction beamline0Development of an in situ X-ray diffraction system for hydrothermal reactions and its application to autoclaved aerated concrete formation1Effects of quartz particle size and water-to-solid ratio on hydrothermal synthesis of tobermorite studied by in-situ time-resolved X-ray diffraction51Enhanced ammonia nitrogen removal using consistent ammonium exchange of modified zeolite and biological regeneration in a sequencing batch reactor process32Kinetic Control of Metal–Organic Framework Crystallization Investigated by Time‐Resolved In Situ X‐Ray Scattering214Kinetic Control of Metal–Organic Framework Crystallization Investigated by Time‐Resolved In Situ X‐Ray Scattering41Watching Nanoparticles Form: An In Situ (Small‐/Wide‐Angle X‐ray Scattering/Total Scattering) Study of the Growth of Yttria‐Stabilised Zirconia in Supercritical Fluids40Colloidal wettability probed with X-ray microscopy21Influence of poly(acrylic acid) on apatite formation studied byin situX-ray diffraction using an X-ray scattering reaction cell with high-precision temperature control14Applications of in situ synchrotron XRD in hydrometallurgy: Literature review and investigation of chalcopyrite dissolution45Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study45Diffraction and Spectroscopy of Porous Solids1In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water16In situ/operando studies for the production of hydrogen through the water-gas shift on metal oxide catalysts91The fast Z-scan method for studying working catalytic reactors with high energy X-ray diffraction: ZSM-5 in the methanol to gasoline process13In‐situPowder X‐ray Diffraction in Heterogeneous Catalysis8Recent Trends in Operando and In Situ Characterization: Techniques for Rational Design of Catalysts6Energy-dispersive X-ray diffraction mapping on a benchtop X-ray fluorescence system5In Situ Studies of Solvothermal Synthesis of Energy Materials159Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study41In Situ X‑ray Diffraction Study of the Formation, Growth, and Phase Transition of Colloidal Cu2– x S Nanocrystals61Understanding Solvothermal Crystallization of Mesoporous Anatase Beads by In Situ Synchrotron PXRD and SAXS40In situ powder X-ray diffraction study of the hydro-thermal formation of LiMn 2 O 4 nanocrystallites10Characterization of Gas‐Solid Reactions using In Situ Powder X‐ray Diffraction38Synthesis variables and behavior of VPI-5: A review2Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 1936Accelerated Thermal Decomposition of Graphene Oxide Films in Air via in Situ X-ray Diffraction Analysis65In Situ Time-Resolved Observation of the Development of Intracrystalline Mesoporosity in USY Zeolite41Systematic study of the crystallization process of CrAPO-5 using in situ high resolution X-ray diffraction7Insights into the aminothermal crystallization process of SAPO-34 and its comparison with hydrothermal system18In-Situ XRD Investigation of Bauxite Dehydroxylation5Physicochemical characterization of nanomaterials: polymorph, composition, wettability, and thermal stability102Formation Mechanisms of Nanocrystalline MnO 2 Polymorphs under Hydrothermal Conditions78In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth610Interface Engineering of Graphene/Polymer Conductive Composites and Their Application in Energy Storage.0The Contribution of Synchrotron X-Ray Powder Diffraction to Modern Zeolite Applications: A Mini-review and Prospects65Low-cost disposable high-pressure setup for in situ X-ray experiments5Real-time inline monitoring of zeolite synthesis by Photon Density Wave spectroscopy18Reaction/crystallization kinetics studied via in situ XRD: experimental conditions versus methods of kinetic analysis7In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11In situ monitoring of hydrothermal reactions by X-ray diffraction with Bragg–Brentano geometry2Molecular Intermediate in the Directed Formation of a Zeolitic Metal–Organic Framework21A Flow-Through Reaction Cell for Studying Minerals Leaching by In-Situ Synchrotron Powder X-ray Diffraction5Experimental studies on hydrothermal mineral replacement of bornite by copper sulphides0Structures and Role of the Intermediate Phases on the Crystallization of BaTiO3 from an Aqueous Synthesis Route19In situ scattering studies of material formation during wet-chemical syntheses1Investigation into the crystallization of molecular sieve DNL-60A review of recent developments for the in situ / operando characterization of nanoporous materials46Prospects and challenges for autonomous catalyst discovery viewed from an experimental perspective46In Situ Characterization Techniques Applied in Photocatalysis: A Review148Understanding formation thermodynamics of structurally diverse zeolite oligomers with first principles calculations14Study of the ABW-Structured LiZnPO4 crystallization using X-ray diffraction and CrystalGrower simulation1In Situ Multinuclear Magic-Angle Spinning NMR: Monitoring Crystallization of Molecular Sieve AlPO4-11 in Real Time11An in situ study to shed light on the formation of goethite spindles by pseudomorphic transformation of intermediate phases5Perspective on the Use of Ultrasonic Monitoring for In Situ Diagnostics of Zeolite and MOF Crystallization6Novel Application of an In Situ Raman Technique for a Co-Crystal Ternary Phase Diagram Determination2In Situ X-ray Diffraction as a Basic Tool to Study Oxide and Metal Oxide Catalysts34Experimental Methods for Membrane Applications in Desalination and Water Treatment12Membrane Distillation9Evaluation of Agricultural Soil-Improving Zeolite for Improving Irrigation Water Quality16Do we achieve “1 + 1 > 2” in dual-atom or dual-single-atom catalysts?87Fly ash-based zeolites: from waste to value – A comprehensive overview of synthesis, properties, and applications24Investigation of biomass valorization processes through catalysis and functional materials0Hydrated silicate ionic liquids: Ionic liquids for silicate material synthesis7A simple and robust high-pressure cell for transmission X-ray investigation1Reliability of pair distribution function analysis in in situ experiments1In Situ SXRD Study of Phase Transformations and Reduction Kinetics in Iron Ore During Hydrogen-Based High-Temperature Reduction3Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40Crystallization pathways as design tools for titanosilicate catalysts0Operando X‐Ray Diffraction and Total Scattering Characterization of Battery Materials: Not Just a Pretty Picture6A Review on In Situ Microscopic Understandings of Dendritic Zinc Growth in Aqueous Zinc Ion Batteries0Quantifying the Kinetics of UiO-66 Metal−Organic Framework Crystallization from X-ray Attenuation in the Zr K-Edge Region0In Situ Ultrasound Monitoring of Fast ZIF-8 Nanoparticle Synthesis0Mineralogical and Geochemical Characterization of Calcium-Rich Natural Zeolites from the Deccan Traps, Maharashtra, India0A “Precise” Future for Chemistry: Engineering Electron Quantum States for Precision Catalysis0A kinetic study of the crystallization of LTA-type zeolite from colloidal solutions by in-situ ultrasonic attenuation measurements0

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  1. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

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  2. In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques

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  3. Stability of AlPO and SAPO molecular sieves during adsorption-desorption cycles of water vapor investigated by in-situ XRD measurements

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  4. Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion

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  5. Reactor design for in situ X-ray scattering studies of nanoparticle formation in supercritical water syntheses

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  6. Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates

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  9. Structural and morphological evolution of β-MnO2nanorods during hydrothermal synthesis

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  14. Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method

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  16. Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques

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  20. Methods for in situ spectroscopic probing of the synthesis of a zeolite

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