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RESEARCH PAPER · Angewandte Chemie · 2011

In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

Nicole Pienack, Wolfgang Bensch

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In‐situ‐Verfolgung der Bildung kristalliner FeststoffeOriginalFast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering263Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering57Assembly of [V15Sb6O42(H2O)]6− cluster shells into higher dimensional aggregates via weak Sb⋯N/Sb⋯O intercluster interactions and a new polyoxovanadate with a discrete [V16Sb4O42(H2O)]8− cluster shell27Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique34Materials Discovery by Flux Crystal Growth: Quaternary and Higher Order Oxides386Auf der Suche nach neuen Materialien: Kristallzucht von quaternären und höherwertigen Oxiden in Flussmitteln18Synthese und Identifizierung metastabiler Verbindungen: schwarzes Arsen – Fiktion oder Wirklichkeit?26Synthesis and Identification of Metastable Compounds: Black Arsenic—Science or Fiction?123Investigations of the crystallization mechanism of CrSb and CrSb2 multilayered films using in-situ X-ray diffraction and in-situ X-ray reflectometry12Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions97Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions15On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)16Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study45Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates31Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates3Keimbildung organischer Kristalle aus molekularer Sichtweise37Nucleation of Organic Crystals—A Molecular Perspective567The Molecular Pathway to ZIF‐7 Microrods Revealed by In Situ Time‐Resolved Small‐ and Wide‐Angle X‐Ray Scattering, Quick‐Scanning Extended X‐Ray Absorption Spectroscopy, and DFT Calculations48On the Entangled Growth of NaTaO3 Cubes and Na2Ti3O7 Wires in Sodium Hydroxide Solution5Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies72Bismuth Tri‐ and Tetraarylcarboxylates: Crystal Structures, In Situ X‐ray Diffraction, Intermediates and Luminescence82Synthesis and Phase Relations of Single‐Phase Fibrous Phosphorus73Formation and Decomposition of Metastable α′′‐Fe16N2 from in situ Powder Neutron Diffraction and Thermal Analysis37In Situ Studies of Solvothermal Synthesis of Energy Materials159Computer‐Assisted Synthesis Optimisation of Inorganic–Organic Hybrid Compounds Using the Local Optimisation Algorithm BOBYQA6“CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements77“CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements14Access and in situ growth of phosphorene-precursor black phosphorus371Die erweiterte Stabilitätsreihe der Phosphorallotrope32The Extended Stability Range of Phosphorus Allotropes171Chemical Speciation and Bond Lengths of Organic Solutes by Core‐Level Spectroscopy: pH and Solvent Influence on p‐Aminobenzoic Acid16Thermodynamics and Kinetics of Prenucleation Clusters, Classical and Non‐Classical Nucleation126Pb2PdO2(OH)2 and Pb2PdO(OH)4(H2O): Synthesis and Crystal Growth at Ambient Conditions3Conversion Reactions of Solids: From a Surprising Three‐Step Mechanism towards Directed Product Formation6Hydrogenation Reaction Pathways in the Systems Li3N–H2, Li3N–Mg–H2, and Li3N–MgH2–H2 by in Situ X-ray Diffraction, in Situ Neutron Diffraction, and in Situ Thermal Analysis10Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation38Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation10Christian‐Albrechts‐Universität Kiel29Precursor‐Directed Nucleation and Self‐Assembly Growth: From Hollow Microprisms to Nanoplatelets4Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33A sapphire single-crystal cell for in situ neutron powder diffraction of solid-gas reactions15100 yearsin situdiffraction5Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes41Kinetics during hydrothermal synthesis of nanosized K x Na 1−x NbO 316Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20Synthesis, Transformation, Catalysis, and Gas Sorption Investigations on the Bismuth Metal–Organic Framework CAU‐17106Multiparameter High-Throughput and in Situ X-ray Diffraction Study of Six New Bismuth Sulfonatocarboxylates: Discovery, Phase Transformation, and Reaction Trends25Anisotropic Assembly during Heat‐Up: The Early Stage Hydrothermal Synthesis of TiO2 from a Complexed Precursor1Establishing the Transitory Existence of Amorphous Phases in Crystallization Pathways by the CLASSIC NMR Technique17In situ Monitoring of the Formation of [Bis(acetylacetonato)manganese(II)] Complexes10Activation of Co−Mo−S Hydrodesulfurization Catalysts Under Refinery Conditions‐A Combined SAXS/XAS Study15Looking into the Black Box of Solid‐State Synthesis74Characterization of Metal‐zeolite Composite Catalysts: Determining the Environment of the Active Phase39Solid–gas reactions in synthetic chemistry: what can we learn from reaction pathways?3Perovskite Oxides Prepared by Hydrothermal and Solvothermal Synthesis: A Review of Crystallisation, Chemistry, and Compositions152Impact of Organic Templates on the Selective Formation of Zeolite Oligomers16Impact of Organic Templates on the Selective Formation of Zeolite Oligomers10In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**23Design and use of a sapphire single-crystal gas-pressure cell forin situneutron powder diffraction14Simultaneous neutron powder diffraction and Raman spectroscopy – an approach of combining two complementary techniques1A double-walled sapphire single-crystal gas-pressure cell (type III) for in situ neutron diffraction1Hydrogenation Reaction Pathways and Crystal Structures of La2H2Se, La2H3Se and La2H4Se5In situ X‐ray Scattering of the Crystallisation of Basic Magnesium Chlorides using a Laboratory Instrument1In Situ X‐ray Diffraction Studies on the Reduction of V2O5 and WO3 by Using Hydrogen8Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40A kinetic study of the crystallization of LTA-type zeolite from colloidal solutions by in-situ ultrasonic attenuation measurements0

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  1. Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering

    Angewandte Chemie International Edition · 2011-07-11

    Janosch Cravillon, Christian A. Schröder, Roman Nayuk, Jérémie Gummel, Klaus P. Huber, Michael Wiebcke

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  2. Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering

    Angewandte Chemie · 2011-07-11

    Janosch Cravillon, Christian A. Schröder, Roman Nayuk, Jérémie Gummel, Klaus P. Huber, Michael Wiebcke

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  3. Assembly of [V15Sb6O42(H2O)]6− cluster shells into higher dimensional aggregates via weak Sb⋯N/Sb⋯O intercluster interactions and a new polyoxovanadate with a discrete [V16Sb4O42(H2O)]8− cluster shell

    CrystEngComm · 2012-01-01

    Е. А. Антонова, Christian Näther, Wolfgang Bensch

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  4. Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique

    Chemistry - A European Journal · 2012-01-16

    Inga Olliges‐Stadler, Jan Stötzel, Dorota Koziej, Marta D. Rossell, Jan‐Dierk Grunwaldt, Maarten Nachtegaal, R. Frahm, Markus Niederberger

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  5. Materials Discovery by Flux Crystal Growth: Quaternary and Higher Order Oxides

    Angewandte Chemie International Edition · 2012-01-27

    Daniel E. Bugaris, Hans‐Conrad zur Loye

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  6. Auf der Suche nach neuen Materialien: Kristallzucht von quaternären und höherwertigen Oxiden in Flussmitteln

    Angewandte Chemie · 2012-01-30

    Daniel E. Bugaris, Hans‐Conrad zur Loye

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  7. Synthese und Identifizierung metastabiler Verbindungen: schwarzes Arsen – Fiktion oder Wirklichkeit?

    Angewandte Chemie · 2012-02-09

    Oliver Osters, Tom Nilges, Frederik Bachhuber, Florian Pielnhofer, Richard Weihrich, Michael Schöneich, Peer Schmidt

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  8. Synthesis and Identification of Metastable Compounds: Black Arsenic—Science or Fiction?

    Angewandte Chemie International Edition · 2012-02-09

    Oliver Osters, Tom Nilges, Frederik Bachhuber, Florian Pielnhofer, Richard Weihrich, Michael Schöneich, Peer Schmidt

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  9. Investigations of the crystallization mechanism of CrSb and CrSb2 multilayered films using in-situ X-ray diffraction and in-situ X-ray reflectometry

    Journal of Solid State Chemistry · 2012-07-27

    Matthias Regus, Gerhard Kuhn, Sergej Mankovsky, H. Ebert, Wolfgang Bensch

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  10. Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions

    Angewandte Chemie International Edition · 2012-08-15

    Christoffer Tyrsted, Kirsten M. Ø. Jensen, Espen Drath Bøjesen, Nina Lock, Mogens Christensen, Simon J. L. Billinge, Bo B. Iversen

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  11. Understanding the Formation and Evolution of Ceria Nanoparticles Under Hydrothermal Conditions

    Angewandte Chemie · 2012-08-15

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  12. On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-09-26

    Beatrix Seidlhofer, Е. А. Антонова, Jing Wang, Diana Schinkel, Wolfgang Bensch

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  13. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

    Chemistry - A European Journal · 2012-10-10

    Е. А. Антонова, Beatrix Seidlhofer, Jing Wang, Michael Hinz, Wolfgang Bensch

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  14. Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study

    Crystal Growth & Design · 2012-10-24

    Jianli Mi, Casper Clausen, Martin Bremholm, Nina Lock, Kirsten M. Ø. Jensen, Mogens Christensen, Bo B. Iversen

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  15. Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates

    Angewandte Chemie International Edition · 2012-11-13

    Tadeja Birsa Čelič, Мojca Rangus, Károly Lázár, Venčeslav Kaučič, Nataša Zabukovec Logar

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  16. Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates

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  17. Keimbildung organischer Kristalle aus molekularer Sichtweise

    Angewandte Chemie · 2013-01-10

    Roger J. Davey, Sven L. M. Schroeder, Joop H. ter Horst

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  18. Nucleation of Organic Crystals—A Molecular Perspective

    Angewandte Chemie International Edition · 2013-01-10

    Roger J. Davey, Sven L. M. Schroeder, Joop H. ter Horst

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  19. The Molecular Pathway to ZIF‐7 Microrods Revealed by In Situ Time‐Resolved Small‐ and Wide‐Angle X‐Ray Scattering, Quick‐Scanning Extended X‐Ray Absorption Spectroscopy, and DFT Calculations

    Chemistry - A European Journal · 2013-04-15

    Maarten G. Goesten, Eli Stavitski, Evgeny A. Pidko, Canan Gücüyener, Bart Boshuizen, Steven N. Ehrlich, Emiel J. M. Hensen, Freek Kapteijn, Jorge Gascón

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  20. On the Entangled Growth of NaTaO3 Cubes and Na2Ti3O7 Wires in Sodium Hydroxide Solution

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    Stefan Baumann, Chang Long Liu, Michael J. Elser, Andreas Sternig, Nicolas Siedl, Thomas Berger, Oliver Diwald

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  21. Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies

    Inorganic Chemistry · 2013-07-17

    Felicitas Niekiel, Maximilian Ackermann, Paul Guerrier, André Rothkirch, Norbert Stock

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  22. Bismuth Tri‐ and Tetraarylcarboxylates: Crystal Structures, In Situ X‐ray Diffraction, Intermediates and Luminescence

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  23. Synthesis and Phase Relations of Single‐Phase Fibrous Phosphorus

    Zeitschrift für anorganische und allgemeine Chemie · 2013-08-16

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  24. Formation and Decomposition of Metastable α′′‐Fe16N2 from in situ Powder Neutron Diffraction and Thermal Analysis

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  25. In Situ Studies of Solvothermal Synthesis of Energy Materials

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  26. Computer‐Assisted Synthesis Optimisation of Inorganic–Organic Hybrid Compounds Using the Local Optimisation Algorithm BOBYQA

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  27. “CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements

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  28. “CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements

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  29. Access and in situ growth of phosphorene-precursor black phosphorus

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    Marianne Köpf, Nadine Eckstein, Daniela Pfister, Carolin Grotz, Ilona Krüger, Magnus Greiwe, Thomas C. Hansen, Holger Kohlmann, Tom Nilges

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  30. Die erweiterte Stabilitätsreihe der Phosphorallotrope

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    Frederik Bachhuber, Jörg von Appen, Richard Dronskowski, Peer Schmidt, Tom Nilges, Arno Pfitzner, Richard Weihrich

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  31. The Extended Stability Range of Phosphorus Allotropes

    Angewandte Chemie International Edition · 2014-09-05

    Frederik Bachhuber, Jörg von Appen, Richard Dronskowski, Peer Schmidt, Tom Nilges, Arno Pfitzner, Richard Weihrich

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  32. Chemical Speciation and Bond Lengths of Organic Solutes by Core‐Level Spectroscopy: pH and Solvent Influence on p‐Aminobenzoic Acid

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    Joanna S. Stevens, Adrian Gainar, Edlira Suljoti, Jie Xiao, Ronny Golnak, Emad Flear Aziz, Sven L. M. Schroeder

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  33. Thermodynamics and Kinetics of Prenucleation Clusters, Classical and Non‐Classical Nucleation

    ChemPhysChem · 2015-04-27

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  34. Pb2PdO2(OH)2 and Pb2PdO(OH)4(H2O): Synthesis and Crystal Growth at Ambient Conditions

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  35. Conversion Reactions of Solids: From a Surprising Three‐Step Mechanism towards Directed Product Formation

    Chemistry - A European Journal · 2016-03-21

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  36. Hydrogenation Reaction Pathways in the Systems Li3N–H2, Li3N–Mg–H2, and Li3N–MgH2–H2 by in Situ X-ray Diffraction, in Situ Neutron Diffraction, and in Situ Thermal Analysis

    The Journal of Physical Chemistry C · 2016-06-07

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  37. Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies

    European Journal of Inorganic Chemistry · 2016-09-19

    Michael Wendt, Lisa K. Mahnke, Niclas Heidenreich, Wolfgang Bensch

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  38. Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation

    Angewandte Chemie International Edition · 2016-10-11

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  39. Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation

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  40. Christian‐Albrechts‐Universität Kiel

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  41. Precursor‐Directed Nucleation and Self‐Assembly Growth: From Hollow Microprisms to Nanoplatelets

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  42. Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents

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  43. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

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  44. A sapphire single-crystal cell for in situ neutron powder diffraction of solid-gas reactions

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  45. 100 yearsin situdiffraction

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  46. Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes

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  47. Kinetics during hydrothermal synthesis of nanosized K x Na 1−x NbO 3

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  48. Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity

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  49. Synthesis, Transformation, Catalysis, and Gas Sorption Investigations on the Bismuth Metal–Organic Framework CAU‐17

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  50. Multiparameter High-Throughput and in Situ X-ray Diffraction Study of Six New Bismuth Sulfonatocarboxylates: Discovery, Phase Transformation, and Reaction Trends

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