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RESEARCH PAPER · Chemistry of Materials · 2001

In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions

Lars Engelke, M. Schaefer, Melissa J. Schur, Wolfgang Bensch

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In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal ConditionsOriginalIn situ X‐Ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions.0Nucleation and crystallization of solids from solution81In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions47[Cr(C6H18N4)(SbS3)], a chromium complex containing an unusual bidentate SbS33− ligand33Templated Synthesis of the Novel Layered Silver−Antimony Sulfides [H3NCH2CH2NH2][Ag2SbS3] and [H3NCH2CH2NH2]2[Ag5Sb3S8]71Reactive magnetron sputtering of molybdenum sulfide thin films: In situ synchrotron x-ray diffraction and transmission electron microscopy study20Four New Thioantimonates(III) with the General Formula [TM(tren)]Sb4S7 (TM = Mn, Fe, Co, Zn) with the Transition Metal as Part of a Thioantimonate(III) Network Synthesized under Solvothermal Conditions and Tuning of the Optical Band Gap by the Transition Metal Cation84In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions32Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24Directing the structures of silver-antimony sulphides: A new topological variant of the [Ag5Sb3S8]2− double layer26Combined In Situ EDXRD/EXAFS Investigation of the Crystal Growth of [Co(C6H18N4)][Sb2S4] under Solvothermal Conditions: Two Different Reaction Pathways Leading to the Same Product62From One-Dimensional Chains to Three-Dimensional Networks: Solvothermal Synthesis of Thiogallates in Ethylenediamine59The Reaction Mechanism of a Complex Intercalation System: In Situ X‐ray Diffraction Studies of the Chemical and Electrochemical Lithium Intercalation in Cr4TiSe819Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates7Morphological and Kinetic Studies on Hexagonal Tungstates55A study of Li intercalation into Cr3Ti2Se8 using electrochemistry, in-situ energy dispersive X-ray diffractometry and NMR spectroscopy11Tuning the Magnetic Properties of LixCrTi0.25Se2 (0.03≤x≤0.7) by Directed Deintercalation of Lithium8Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape64Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation45The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study38Solvothermal Syntheses of Two Novel Layered Quaternary Silver−Antimony(III) Sulfides with Different Strategies45Some Examples of Temperature and Time Resolved Studies of the Dehydration and Hydration Behavior of Zeolites and Clathrates6Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility26Syntheses and Characterization of a Series of Silver−Thioantimonates(III) and Thioarsenates(III) Containing Two Types of Silver−Sulfur Chains50In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies37Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation132A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Systematic and In Situ Energy Dispersive X-ray Diffraction Investigations on the Formation of Lanthanide Phosphonatobutanesulfonates: Ln(O3P-C4H8-SO3)(H2O) (Ln = La−Gd)53In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties43High‐Throughput and Time‐Resolved Energy‐Dispersive X‐Ray Diffraction (EDXRD) Study of the Formation of CAU‐1‐(OH) 2 : Microwave and Conventional Heating94From Zero- to Three-Dimensional Thioantimonates: [Ni(aepa)2]3Sb6S12 (aepa = C5H15N3 = N-(aminoethyl)-1,3-propandiamine), Containing the Unique [Sb6S12]6– Cyclic Anion, [Ni(aepa)2]6(Sb3S6)2(SO4)3·2H2O, with Isolated [Sb3S6]3– anions and [Ni(aepa)2]Sb4S7, Characterized by a Three-Dimensional Network Structure39High-Throughput and in Situ Energy Dispersive X-ray Diffraction Investigation on the Formation of the New Metal Organogermanate Cu(OOCC2H4Ge)2O319Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy368Synthesis of isoreticular CAU-1 compounds: effects of linker and heating methods on the kinetics of the synthesis45In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts57In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials32High-throughput and in situ EDXRD investigation on the formation of two new metal aminoethylphosphonates – Ca(O3PC2H4NH2) and Ca(OH)(O3PC2H4NH3)·2H2O21Systematic Investigation of Zinc Aminoalkylphosphonates: Influence of the Alkyl Chain Lengths on the Structure Formation16X‐Ray Diffraction and Small Angle X‐Ray Scattering23On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)16Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Copper Phosphonatoethanesulfonates: Temperature Dependent in Situ Energy Dispersive X-ray Diffraction Study and Influence of the pH on the Crystal Structures38Nanostructured Inorganic–Organic Hybrid Semiconductor Materials3One-step hydrothermal synthesis of hierarchical Ag/Bi2WO6 composites: In situ growth monitoring and photocatalytic activity studies66In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle Synthesis75Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies72Bismuth Tri‐ and Tetraarylcarboxylates: Crystal Structures, In Situ X‐ray Diffraction, Intermediates and Luminescence82High-throughput ultrasonic synthesis and in situ crystallisation investigation of metal phosphonocarboxylates25Insight into the mechanism of modulated syntheses: in situ synchrotron diffraction studies on the formation of Zr-fumarate MOF158In Situ Energy-Dispersive X-ray Diffraction for the Synthesis Optimization and Scale-up of the Porous Zirconium Terephthalate UiO-66219In situ 27Al NMR kinetic investigation of zeolite A crystallization24Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds33Acid-functionalized UiO-66(Zr) MOFs and their evolution after intra-framework cross-linking: structural features and sorption properties231Impact of the Nature of the Organic Spacer on the Crystallization Kinetics of UiO‐66(Zr)‐Type MOFs49Synthesis of heterometallic chalcogenides containing lanthanide and group 13–15 metal elements94Synthesis, Crystal Structure, and Physical Properties of Two Polymorphs of CsGaSe2, and High-Temperature X-ray Diffraction Study of the Phase Transition Kinetics23Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Divalent metal phosphonates – new aspects for syntheses, in situ characterization and structure solution11In Situ Studies on Phase Transitions of Tris(acetylacetonato)-Aluminum(III) Al(acac)321Polymorphism of CsGaS 2 – structural characterization of a new two-dimensional polymorph and study of the phase-transition kinetics27In situ luminescence analysis: a new light on monitoring calcium phosphate phase transitions26Monitoring the mechanism of formation of [Ce(1,10-phenanthroline) 2 (NO 3 ) 3 ] by in situ luminescence analysis of 5d–4f electronic transitions15Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles33Polymorphous Al-MOFs Based on V-Shaped Linker Molecules: Synthesis, Properties, and in Situ Investigation of Their Crystallization35Panoramic Synthesis as an Effective Materials Discovery Tool: The System Cs/Sn/P/Se as a Test Case46From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?20Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering Analyses51In situ Monitoring of the Formation of [Bis(acetylacetonato)manganese(II)] Complexes10In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11In situ scattering studies of material formation during wet-chemical syntheses1

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  1. In situ X‐Ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions.

    ChemInform · 2001-07-17

    Lars Engelke, M. Schaefer, Melissa J. Schur, Wolfgang Bensch

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  2. Nucleation and crystallization of solids from solution

    Current Opinion in Solid State and Materials Science · 2001-10-01

    Ferdi Schüth

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  3. In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions

    European Journal of Inorganic Chemistry · 2003-01-20

    Lars Engelke, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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  4. [Cr(C6H18N4)(SbS3)], a chromium complex containing an unusual bidentate SbS33− ligand

    Polyhedron · 2003-09-01

    Paz Vaqueiro, CHIPPINDALE Ann Mary, Anthony V. Powell

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  5. Templated Synthesis of the Novel Layered Silver−Antimony Sulfides [H3NCH2CH2NH2][Ag2SbS3] and [H3NCH2CH2NH2]2[Ag5Sb3S8]

    Inorganic Chemistry · 2003-10-29

    Paz Vaqueiro, CHIPPINDALE Ann Mary, Andrew R. Cowley, Anthony V. Powell

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  6. Reactive magnetron sputtering of molybdenum sulfide thin films: In situ synchrotron x-ray diffraction and transmission electron microscopy study

    Journal of Applied Physics · 2004-05-28

    V. Weiss, W. Bohne, J. Röhrich, Erik Strub, Ulrike Bloeck, I. Sieber, K. Ellmer, Rainald Mientus, Felix Porsch

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  7. Four New Thioantimonates(III) with the General Formula [TM(tren)]Sb4S7 (TM = Mn, Fe, Co, Zn) with the Transition Metal as Part of a Thioantimonate(III) Network Synthesized under Solvothermal Conditions and Tuning of the Optical Band Gap by the Transition Metal Cation

    Zeitschrift für anorganische und allgemeine Chemie · 2004-10-01

    Michael Schaefer, Ralph Stähler, Ragnar Kiebach, Christian Näther, Wolfgang Bensch

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  8. In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions

    Zeitschrift für anorganische und allgemeine Chemie · 2005-02-01

    Ragnar Kiebach, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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  9. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

    Angewandte Chemie International Edition · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  10. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

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    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  11. Directing the structures of silver-antimony sulphides: A new topological variant of the [Ag5Sb3S8]2− double layer

    Journal of Solid State Chemistry · 2005-10-03

    Anthony V. Powell, Jürgen Thun, CHIPPINDALE Ann Mary

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  12. Combined In Situ EDXRD/EXAFS Investigation of the Crystal Growth of [Co(C6H18N4)][Sb2S4] under Solvothermal Conditions: Two Different Reaction Pathways Leading to the Same Product

    Chemistry of Materials · 2006-02-08

    Ragnar Kiebach, Nicole Pienack, M.-E. Ordolff, Felix Studt, Wolfgang Bensch

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  13. From One-Dimensional Chains to Three-Dimensional Networks: Solvothermal Synthesis of Thiogallates in Ethylenediamine

    Inorganic Chemistry · 2006-04-19

    Paz Vaqueiro

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  14. The Reaction Mechanism of a Complex Intercalation System: In Situ X‐ray Diffraction Studies of the Chemical and Electrochemical Lithium Intercalation in Cr4TiSe8

    Chemistry - A European Journal · 2006-05-24

    Malte Behrens, Ragnar Kiebach, Jannes Ophey, Oliver Riemenschneider, Wolfgang Bensch

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  15. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

    Chemistry - A European Journal · 2006-11-17

    Alexej Michailovski, Greta Ricarda Patzke

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  16. Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates

    Zeitschrift für anorganische und allgemeine Chemie · 2006-12-11

    Alexej Michailovski, Greta Ricarda Patzke

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  17. Morphological and Kinetic Studies on Hexagonal Tungstates

    Chemistry of Materials · 2006-12-20

    Alexej Michailovski, Ragnar Kiebach, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alfons Baiker, Sridhar Komarneni, Greta Ricarda Patzke

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  18. A study of Li intercalation into Cr3Ti2Se8 using electrochemistry, in-situ energy dispersive X-ray diffractometry and NMR spectroscopy

    Solid State Ionics · 2007-03-29

    Joseph Wontcheu, Malte Behrens, Wolfgang Bensch, Sylvio Indris, Martin Wilkening, Paul Heitjans

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  19. Tuning the Magnetic Properties of LixCrTi0.25Se2 (0.03≤x≤0.7) by Directed Deintercalation of Lithium

    Chemistry - A European Journal · 2008-04-16

    Malte Behrens, Joseph Wontcheu, Ragnar Kiebach, Wolfgang Bensch

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  20. Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape

    Chemistry of Materials · 2008-04-17

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  21. Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation

    European Journal of Inorganic Chemistry · 2009-02-06

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  22. The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study

    Small · 2009-06-22

    Ying Zhou, Nicole Pienack, Wolfgang Bensch, Greta Ricarda Patzke

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  23. Solvothermal Syntheses of Two Novel Layered Quaternary Silver−Antimony(III) Sulfides with Different Strategies

    Crystal Growth & Design · 2009-07-09

    Hua–Gang Yao, Min Ji, Shou‐Hua Ji, Ren‐Chun Zhang, Yong‐Lin An, Guiling Ning

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  24. Some Examples of Temperature and Time Resolved Studies of the Dehydration and Hydration Behavior of Zeolites and Clathrates

    Particle & Particle Systems Characterization · 2009-09-01

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  25. Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility

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  26. Syntheses and Characterization of a Series of Silver−Thioantimonates(III) and Thioarsenates(III) Containing Two Types of Silver−Sulfur Chains

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  27. In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures

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  28. Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies

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  29. Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation

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  30. A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework

    CrystEngComm · 2010-10-01

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  31. Systematic and In Situ Energy Dispersive X-ray Diffraction Investigations on the Formation of Lanthanide Phosphonatobutanesulfonates: Ln(O3P-C4H8-SO3)(H2O) (Ln = La−Gd)

    Inorganic Chemistry · 2010-11-08

    Mark Feyand, Christian Näther, André Rothkirch, Norbert Stock

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  32. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

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  33. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

    Angewandte Chemie · 2011-02-15

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  34. A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties

    Inorganic Chemistry Communications · 2011-03-16

    Yi Liu, Yufeng Tian, Fengxia Wei, Michael Ser Chong Ping, Chuanwei Huang, Freddy Boey, Christian Kloc, Lang Chen, Tom Wu, Qichun Zhang

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  35. High‐Throughput and Time‐Resolved Energy‐Dispersive X‐Ray Diffraction (EDXRD) Study of the Formation of CAU‐1‐(OH) 2 : Microwave and Conventional Heating

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    Tim Ahnfeldt, J. Moellmer, Vincent Guillerm, R. Staudt, Christian Serre, Norbert Stock

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  36. From Zero- to Three-Dimensional Thioantimonates: [Ni(aepa)2]3Sb6S12 (aepa = C5H15N3 = N-(aminoethyl)-1,3-propandiamine), Containing the Unique [Sb6S12]6– Cyclic Anion, [Ni(aepa)2]6(Sb3S6)2(SO4)3·2H2O, with Isolated [Sb3S6]3– anions and [Ni(aepa)2]Sb4S7, Characterized by a Three-Dimensional Network Structure

    Crystal Growth & Design · 2011-10-10

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  37. High-Throughput and in Situ Energy Dispersive X-ray Diffraction Investigation on the Formation of the New Metal Organogermanate Cu(OOCC2H4Ge)2O3

    Crystal Growth & Design · 2011-10-25

    Corinna Schmidt, Norbert Stock

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  38. Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy

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  39. Synthesis of isoreticular CAU-1 compounds: effects of linker and heating methods on the kinetics of the synthesis

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  40. In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts

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    Stefan Zander, Beatrix Seidlhofer, Malte Behrens

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  41. In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials

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    Ying Zhou, Е. А. Антонова, Yuanhua Lin, Jan‐Dierk Grunwaldt, Wolfgang Bensch, Greta Ricarda Patzke

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  42. High-throughput and in situ EDXRD investigation on the formation of two new metal aminoethylphosphonates – Ca(O3PC2H4NH2) and Ca(OH)(O3PC2H4NH3)·2H2O

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  43. Systematic Investigation of Zinc Aminoalkylphosphonates: Influence of the Alkyl Chain Lengths on the Structure Formation

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  44. X‐Ray Diffraction and Small Angle X‐Ray Scattering

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  45. On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)

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  46. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

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  47. Copper Phosphonatoethanesulfonates: Temperature Dependent in Situ Energy Dispersive X-ray Diffraction Study and Influence of the pH on the Crystal Structures

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  48. Nanostructured Inorganic–Organic Hybrid Semiconductor Materials

    Elsevier eBooks · 2013-01-01

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  49. One-step hydrothermal synthesis of hierarchical Ag/Bi2WO6 composites: In situ growth monitoring and photocatalytic activity studies

    Science China Chemistry · 2013-02-21

    Ying Zhou, Qian Zhang, Yuanhua Lin, Е. А. Антонова, Wolfgang Bensch, Greta Ricarda Patzke

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  50. In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle Synthesis

    Particle & Particle Systems Characterization · 2013-03-20

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