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RESEARCH PAPER · Journal of the American Chemical Society · 2004

Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates

Alexander J. Norquist, Dermot O’Hare

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Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc PhosphatesOriginalFive New Zinc Phosphite Structures: Tertiary Building Blocks in the Construction of Hybrid Materials75High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface68(C4H12N2)[Zn2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalatedN-methylpropane-1,3-diaminium cations2Formation of Zinc Phosphate Polymers and Networks through the Insertion of Metathiophosphates into Zinc Dialkyldithiophosphates10Novel Zinc Phosphate Topologies Defined by Organic Ligands95Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction57A Building‐Up Process in Open‐Framework Metal Carboxylates that Involves a Progressive Increase in Dimensionality116A Building‐Up Process in Open‐Framework Metal Carboxylates that Involves a Progressive Increase in Dimensionality10Structural diversity and chemical trends in hybrid inorganic–organic framework materials1082Towards understanding, control and application of layered double hydroxide chemistry582In-situ XRD as a tool to understanding zeolite crystallization105Synthesis and Characterization of a New Three‐dimensional Organically Templated Nickel‐Zinc Phosphate2Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction15Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18An ab Initio Molecular Dynamics and Density Functional Theory Study of the Formation of Phosphate Chains from Metathiophosphates16Memory Effect of Activated Mg–Al Hydrotalcite: In Situ XRD Studies during Decomposition and Gas‐Phase Reconstruction150Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane39(C5H14N2)[Zn3(HPO4)4], a New 3D Open‐framework Zincophosphate Synthesized by Hydrothermal Reversible Transformation of (C5H14N2)[Zn2(HPO4)3]·H2O3Synthesis of nanocrystals and morphology control of hydrothermally prepared LiFePO4320Crystal structures and spectroscopic properties of a new zinc phosphite cluster and an unexpected chainlike zinc phosphate obtained by hydrothermal reactions926-Ring-Channel Structure Constructed from Bimetal Phosphite Helical Chains130Assembly of a Homochiral, Body-Centered Cubic Network Composed of Vertex-Shared Mg12 Cages: Use of Electrospray Ionization Mass Spectrometry to Monitor Metal Carboxylate Nucleation127Synthesis, Structure, and Polymorphism Studies in Amine-Templated Open-Framework Zinc Phosphites47Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Transformation of a Layered Zinc Phosphite to a Three-Dimensional Open-Framework Structure with Intersecting 16- and 12-Ring Channels30New Variant of Highly Symmetric Layered Perovskite with Coordinated NO3− Ligand: Hydrothermal Synthesis, Structure, and Characterization of Cs2PbCl2(NO3)223Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium36Structural Transformation of Three‐Dimensional Bimetallic Phosphites Containing Corner‐Sharing 4‐Ring Chains8Kinetics and Thermodynamics of Zinc Phosphate Hydrate Synthesized by a Simple Route in Aqueous and Acetone Media42Nanoscale Chemistry of Uranyl Selenates1The application of statistical methodology to the analysis of time-resolved X-ray diffraction data12[Zn5(PO4)(HPO4)4(Hbpy)2(bpy)][H2PO4]·H2O: a novel inorganic–organic metal-phosphate framework showing an unprecedented (3,4)-connected (4·62)6(4·62·103)2(64·102)2 topology and the coexistence of various phosphates10Synthetic Methodologies0Steric-Induced Layer Flection in Templated Vanadium Tellurites11A new, facile method to prepare hybrid calcium poly(styrene-phenylvinylphosphonate)–phosphate materials for a superior performance catalyst support4Dimensionality changes in the solid phase at room temperature: 2D → 1D → 3D evolution induced by ammonia sorption–desorption on zinc phosphates7In Situ Studies of Solvothermal Synthesis of Energy Materials159PREPARATION AND ANTI-CORROSION PERFORMANCE OF ZINC PHOSPHATE NANOCRYSTALS BY ULTRASONIC–HYDROTHERMAL SYNERGISTIC ROUTE13“CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements76“CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements14Synthesis and characterization of a novel inorganic–organic hybrid open-framework zinc phosphate with 16-ring channels10An in situ EDXRD kinetic and mechanistic study of the hydrothermal crystallization of TiO 2 nanoparticles from nitric acid peptized sol–gel5The Lead Coordination Polymers Containing Pyrazine-2,3-Dicarboxylic Acid: Rapid Structural Transformations and Cation Exchange25Alkylzinc diorganophosphates: synthesis, structural diversity and unique ability to incorporate zincoxane units11Operando Techniques3Physicochemical characterization of nanomaterials: polymorph, composition, wettability, and thermal stability102An investigation of crystallization kinetics of the Na3MnCO3PO4 cathode material, synthesized by the hydrothermal method16Lead–Organic Frameworks Containing Trimesic Acid: Facile Dissolution–Crystallization and Near-White Light Emission15Naturally derived pyroxene nanomaterials: an ore for wide applications1Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph31Predicting inorganic dimensionality in templated metal oxides8In situ scattering studies of material formation during wet-chemical syntheses1Revealing the Mechanism and Kinetics of Fe5C2 Formation From Ferrous Oxalate under CO2 Fischer‐Tropsch Conditions Using Time‐Resolved In Situ X‐Ray Absorption Spectroscopy5Kinetics of Cu–Zn–Al Hydrotalcite Reconstruction Using a Modified Avrami–Erofeev Model: Preliminary Insights2

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  1. Five New Zinc Phosphite Structures: Tertiary Building Blocks in the Construction of Hybrid Materials

    Inorganic Chemistry · 2005-03-23

    Jian Fan, Carla Slebodnick, Diego Troya, Ross John Angel, Brian E. Hanson

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  2. High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface

    Review of Scientific Instruments · 2005-04-29

    Jan‐Dierk Grunwaldt, Michael Ramin, Markus Rohr, Alexej Michailovski, Greta Ricarda Patzke, Alfons Baiker

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  3. (C4H12N2)[Zn2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalatedN-methylpropane-1,3-diaminium cations

    Acta Crystallographica Section E Structure Reports Online · 2005-06-24

    Nataša Zabukovec Logar, Nevenka Z. Rajić, Djordje R. Stojakovic, Sanja Šajić, Amalija Golobič, Venčeslav Kaučič

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  4. Formation of Zinc Phosphate Polymers and Networks through the Insertion of Metathiophosphates into Zinc Dialkyldithiophosphates

    Inorganic Chemistry · 2005-09-10

    Nicholas J. Mosey, Tom K. Woo

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  5. Novel Zinc Phosphate Topologies Defined by Organic Ligands

    Inorganic Chemistry · 2005-09-10

    Jian Fan, Brian E. Hanson

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  6. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction

    Structure and bonding · 2005-11-08

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  7. A Building‐Up Process in Open‐Framework Metal Carboxylates that Involves a Progressive Increase in Dimensionality

    Angewandte Chemie International Edition · 2005-11-30

    Meenakshi Dan-Hardi, C. N. R. Rao

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  8. A Building‐Up Process in Open‐Framework Metal Carboxylates that Involves a Progressive Increase in Dimensionality

    Angewandte Chemie · 2005-11-30

    Meenakshi Dan-Hardi, C. N. R. Rao

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  9. Structural diversity and chemical trends in hybrid inorganic–organic framework materials

    Chemical Communications · 2006-01-01

    Anthony Kevin Cheetham, C. N. R. Rao, R.K. Feller

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  10. Towards understanding, control and application of layered double hydroxide chemistry

    Journal of Materials Chemistry · 2006-01-01

    Gareth R. Williams, Dermot O’Hare

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  11. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

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  12. Synthesis and Characterization of a New Three‐dimensional Organically Templated Nickel‐Zinc Phosphate

    Zeitschrift für anorganische und allgemeine Chemie · 2006-01-30

    Zhien Lin, Wei Fan, Naotaka Chino, Feifei Gao, Toshiyuki Yokoi, Tatsuya Okubo

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  13. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction

    ChemInform · 2006-05-23

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  14. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

    Chemistry of Materials · 2006-07-18

    Gareth R. Williams, Alexander J. Norquist, Dermot O’Hare

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  15. An ab Initio Molecular Dynamics and Density Functional Theory Study of the Formation of Phosphate Chains from Metathiophosphates

    Inorganic Chemistry · 2006-07-25

    Nicholas J. Mosey, Tom K. Woo

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  16. Memory Effect of Activated Mg–Al Hydrotalcite: In Situ XRD Studies during Decomposition and Gas‐Phase Reconstruction

    Chemistry - A European Journal · 2006-10-09

    Javier Pérez‐Ramírez, Sònia Abelló, Niek M. van der Pers

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  17. Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane

    New Journal of Chemistry · 2006-11-24

    R. Atencio, Alexander Briceño, Pedro J. Silva, José A. Rodríguez, Jonathan C. Hanson

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  18. (C5H14N2)[Zn3(HPO4)4], a New 3D Open‐framework Zincophosphate Synthesized by Hydrothermal Reversible Transformation of (C5H14N2)[Zn2(HPO4)3]·H2O

    Zeitschrift für anorganische und allgemeine Chemie · 2006-12-11

    Michael Wiebcke

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  19. Synthesis of nanocrystals and morphology control of hydrothermally prepared LiFePO4

    Journal of Materials Chemistry · 2007-01-01

    Brian L. Ellis, Wang Hay Kan, W. R. M. Makahnouk, Linda F. Nazar

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  20. Crystal structures and spectroscopic properties of a new zinc phosphite cluster and an unexpected chainlike zinc phosphate obtained by hydrothermal reactions

    Journal of Solid State Chemistry · 2007-01-10

    Zhien Lin, Wei Fan, Jinlou Gu, Tatsuya Okubo

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  21. 26-Ring-Channel Structure Constructed from Bimetal Phosphite Helical Chains

    Journal of the American Chemical Society · 2007-04-06

    Yu-Lun Lai, Kwang‐Hwa Lii, Sue‐Lein Wang

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  22. Assembly of a Homochiral, Body-Centered Cubic Network Composed of Vertex-Shared Mg12 Cages: Use of Electrospray Ionization Mass Spectrometry to Monitor Metal Carboxylate Nucleation

    Journal of the American Chemical Society · 2007-10-10

    J.A. Rood, Bill Boggess, Bruce C. Noll, Kenneth W. Henderson

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  23. Synthesis, Structure, and Polymorphism Studies in Amine-Templated Open-Framework Zinc Phosphites

    Inorganic Chemistry · 2008-05-07

    Sukhendu Bikas Mandal, Srinivasan Natarajan

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  24. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  25. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  26. Anion-topology approach

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    Sergey V. Krivovichev

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  27. Basic concepts

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  28. Copyright Page

    Unknown journal · 2009-01-22

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  29. Dedication

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  30. Dimensional reduction in inorganic oxysalts

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    Sergey V. Krivovichev

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  31. Graph theory applied to low-dimensional structural units in inorganic oxysalts

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  32. Preface

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  33. Structural Crystallography of Inorganic Oxysalts

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  34. Topology of framework structures in inorganic oxysalts

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  35. Transformation of a Layered Zinc Phosphite to a Three-Dimensional Open-Framework Structure with Intersecting 16- and 12-Ring Channels

    Inorganic Chemistry · 2009-03-23

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  36. New Variant of Highly Symmetric Layered Perovskite with Coordinated NO3− Ligand: Hydrothermal Synthesis, Structure, and Characterization of Cs2PbCl2(NO3)2

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  37. Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium

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  38. Structural Transformation of Three‐Dimensional Bimetallic Phosphites Containing Corner‐Sharing 4‐Ring Chains

    Zeitschrift für anorganische und allgemeine Chemie · 2009-12-01

    Zhien Lin, Hari Pada Nayek, Stefanie Dehnen

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  39. Kinetics and Thermodynamics of Zinc Phosphate Hydrate Synthesized by a Simple Route in Aqueous and Acetone Media

    Industrial & Engineering Chemistry Research · 2010-03-01

    Banjong Boonchom, Rattanai Baitahe, Samart Kongtaweelert, Naratip Vittayakorn

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  40. Nanoscale Chemistry of Uranyl Selenates

    Springer eBooks · 2011-01-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  41. The application of statistical methodology to the analysis of time-resolved X-ray diffraction data

    Analytical Methods · 2011-01-01

    J. Burley, Dermot O’Hare, Gareth R. Williams

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  42. [Zn5(PO4)(HPO4)4(Hbpy)2(bpy)][H2PO4]·H2O: a novel inorganic–organic metal-phosphate framework showing an unprecedented (3,4)-connected (4·62)6(4·62·103)2(64·102)2 topology and the coexistence of various phosphates

    CrystEngComm · 2012-01-01

    Wenyuan Xu, Xiao-Zhao Tian, Gong‐Ming Sun, Yu‐Mei Song, Hai-Xiao Huang, Yan Zhu, Zi-Zun Yuan, Xue-feng Feng, Mingbiao Luo, Shujuan Liu, Feng Luo

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  43. Synthetic Methodologies

    Elsevier eBooks · 2013-01-01

    S. A. Corr, Ram Seshadri

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  44. Steric-Induced Layer Flection in Templated Vanadium Tellurites

    Crystal Growth & Design · 2013-04-02

    Kelvin B. Chang, Matthew D. Smith, Samuel M. Blau, Ethan C. Glor, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  45. A new, facile method to prepare hybrid calcium poly(styrene-phenylvinylphosphonate)–phosphate materials for a superior performance catalyst support

    RSC Advances · 2014-01-01

    Jing Huang, Mei Tang, Chang Ming Li

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  46. Dimensionality changes in the solid phase at room temperature: 2D → 1D → 3D evolution induced by ammonia sorption–desorption on zinc phosphates

    Chemical Communications · 2014-01-01

    Zakariae Amghouz, Beatriz Ramajo, Sergei A. Khainakov, Iván da Silva, German Rafael Castro, José R. Garcı́a, Santiago García‐Granda

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  47. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  48. PREPARATION AND ANTI-CORROSION PERFORMANCE OF ZINC PHOSPHATE NANOCRYSTALS BY ULTRASONIC–HYDROTHERMAL SYNERGISTIC ROUTE

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  49. “CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements

    Angewandte Chemie International Edition · 2014-07-07

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  50. “CLASSIC NMR”: An In‐Situ NMR Strategy for Mapping the Time‐Evolution of Crystallization Processes by Combined Liquid‐State and Solid‐State Measurements

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