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RESEARCH PAPER · Chemistry - A European Journal · 2012

Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

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Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal ConditionsOriginalHydrothermal syntheses, crystal structures and characterization of new vanadoborates: The novel decorated cage cluster [V6B22O44(OH)10]31(C6H6)4[H4GeMo12O40]·1.5H2O: A New Polyoxomolybdate Obtained from In Situ Reaction2Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies72High-throughput ultrasonic synthesis and in situ crystallisation investigation of metal phosphonocarboxylates25In Situ Studies of Solvothermal Synthesis of Energy Materials159Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds33Semimetal-functionalised polyoxovanadates290Catalysis of “outer-phase” oxygen atom exchange reactions by encapsulated “inner-phase” water in {V 15 Sb 6 }-type polyoxovanadates37High Nuclearity Antimonato‐Polyoxovanadate Cluster {V15Sb6O42} as a Synthon for the Solvothermal in situ Generation of α‐ and β‐{V14Sb8O42} Isomers18The ZIF system zinc(II) 4,5-dichoroimidazolate: theoretical and experimental investigations of the polymorphism and crystallization mechanisms7Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Combined in- and ex situ studies of pyrazine adsorption into the aliphatic MOF Al-CAU-13: structures, dynamics and correlations23In situ luminescence analysis: a new light on monitoring calcium phosphate phase transitions26Polymorphous Al-MOFs Based on V-Shaped Linker Molecules: Synthesis, Properties, and in Situ Investigation of Their Crystallization35Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks38In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes41From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?20Configurational Isomerism in Polyoxovanadates52Konfigurationsisomerie in Polyoxovanadaten8New Water‐Soluble Cluster Compound {Zn(en)3}3[V15Sb6O42(H2O)]⋅ (Ethylenediamine)3⋅10 H2O as a Synthon for the Generation of Two New Antimonato Polyoxovanadates17Rational Syntheses of Three New {V14Sb8} Clusters Applying a Water-Soluble High-Nuclearity Cluster as Synthon8Mixing SbIIIand GeIVoccupancy in the polyoxovanadate {V14E8} archetype2Investigation of the Kinetic Stabilization of a Ce4+‐based MOF by in‐situ Powder X‐ray Diffraction26New pronounced progress in the synthesis of group 5 polyoxometalates29A Lacunary Polyoxovanadate Precursor and Transition‐Metal‐Sandwiched Derivatives for Catalytic Oxidation of Sulfides32In situ scattering studies of material formation during wet-chemical syntheses1The crystal structure of tetra(1-ethylimidazole-κ 1 N)-[μ 4-imidazole-4,5-dicarboxylato-κ 4 O, N, O′, N′]-trioxido-divanadium, C25H33N10O7V24Two extended structures constructed by borate- or germanate-substituted octadecavanadate clusters3

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  1. Hydrothermal syntheses, crystal structures and characterization of new vanadoborates: The novel decorated cage cluster [V6B22O44(OH)10]

    Journal of Solid State Chemistry · 2013-02-28

    Xing Liu, Jian Zhou, Litao An, Rong Chen, Fei-Long Hu, Qiuling Tang

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  2. (C6H6)4[H4GeMo12O40]·1.5H2O: A New Polyoxomolybdate Obtained from In Situ Reaction

    Journal of Cluster Science · 2013-04-11

    Gao-Juan Cao, Cheng Rong

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  3. Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies

    Inorganic Chemistry · 2013-07-17

    Felicitas Niekiel, Maximilian Ackermann, Paul Guerrier, André Rothkirch, Norbert Stock

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  4. High-throughput ultrasonic synthesis and in situ crystallisation investigation of metal phosphonocarboxylates

    Dalton Transactions · 2013-10-31

    Lars‐Hendrik Schilling, Norbert Stock

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  5. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  6. Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds

    Inorganic Chemistry · 2014-05-20

    Jessica Hilbert, Christian Näther, Wolfgang Bensch

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  7. Semimetal-functionalised polyoxovanadates

    Chemical Society Reviews · 2015-01-01

    Kirill Yu. Monakhov, Wolfgang Bensch, Paul Kögerler

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  8. Catalysis of “outer-phase” oxygen atom exchange reactions by encapsulated “inner-phase” water in {V 15 Sb 6 }-type polyoxovanadates

    Chemical Science · 2016-01-01

    Michael Wendt, Ulrike Warzok, Christian Näther, Jan van Leusen, Paul Kögerler, Christoph A. Schalley, Wolfgang Bensch

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  9. High Nuclearity Antimonato‐Polyoxovanadate Cluster {V15Sb6O42} as a Synthon for the Solvothermal in situ Generation of α‐ and β‐{V14Sb8O42} Isomers

    Chemistry - A European Journal · 2016-04-10

    Michael Wendt, Christian Näther, Wolfgang Bensch

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  10. The ZIF system zinc(II) 4,5-dichoroimidazolate: theoretical and experimental investigations of the polymorphism and crystallization mechanisms

    Zeitschrift für Kristallographie - Crystalline Materials · 2016-09-17

    Sergej Springer, Niclas Heidenreich, Norbert Stock, Leo van Wüllen, Klaus P. Huber, Stefano Leoni, Michael Wiebcke

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  11. Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies

    European Journal of Inorganic Chemistry · 2016-09-19

    Michael Wendt, Lisa K. Mahnke, Niclas Heidenreich, Wolfgang Bensch

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  12. Combined in- and ex situ studies of pyrazine adsorption into the aliphatic MOF Al-CAU-13: structures, dynamics and correlations

    Dalton Transactions · 2017-01-01

    Helge Reinsch, Jannik Benecke, Martin Etter, Niclas Heidenreich, Norbert Stock

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  13. In situ luminescence analysis: a new light on monitoring calcium phosphate phase transitions

    Inorganic Chemistry Frontiers · 2017-01-01

    Huayna Terraschke, Merrit Rothe, A.-M. Tsirigoni, Patric Lindenberg, Laura Ruiz Arana, Niclas Heidenreich, F. Bertram, Martin Etter

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  14. Polymorphous Al-MOFs Based on V-Shaped Linker Molecules: Synthesis, Properties, and in Situ Investigation of Their Crystallization

    Inorganic Chemistry · 2017-04-28

    Martin Krüger, A. Ken Inge, Helge Reinsch, Yuan-Han Li, Mohammad Wahiduzzaman, Chia‐Her Lin, Sue‐Lein Wang, Guillaume Maurin, Norbert Stock

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  15. Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks

    Crystal Growth & Design · 2017-05-08

    Timo Rhauderwiek, Niclas Heidenreich, Helge Reinsch, Sigurd Øien‐Ødegaard, Kirill A. Lomachenko, Uta Ruett, Alexander V. Soldatov, Karl Petter Lillerud, Norbert Stock

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  16. In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review

    Reviews in Analytical Chemistry · 2017-08-19

    Huayna Terraschke, Merrit Rothe, Patric Lindenberg

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  17. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

    Review of Scientific Instruments · 2017-10-01

    Niclas Heidenreich, U. Rütt, Milan Köppen, A. Ken Inge, S. Beier, Ann‐Christin Dippel, Ralf Suren, Norbert Stock

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  18. Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes

    Chemistry - A European Journal · 2017-12-11

    Helge Reinsch, Thomas Homburg, Niclas Heidenreich, Dominik Fröhlich, Stefan K. Henninger, Michael Wark, Norbert Stock

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  19. From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?

    Physical Chemistry Chemical Physics · 2017-12-20

    Philipp Müscher‐Polzin, Irma Vania Eliani, Jonas Ströh, M. Braun, Niklas Ruser, Niclas Heidenreich, Pia Rönfeldt, Florian Bertram, Christian Näther, Stephan Wöhlbrandt, Markus Suta, Huayna Terraschke

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  20. Configurational Isomerism in Polyoxovanadates

    Angewandte Chemie International Edition · 2018-01-12

    Lisa K. Mahnke, Aleksandar Kondinski, Ulrike Warzok, Christian Näther, Jan van Leusen, Christoph A. Schalley, Kirill Yu. Monakhov, Paul Kögerler, Wolfgang Bensch

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  21. Konfigurationsisomerie in Polyoxovanadaten

    Angewandte Chemie · 2018-01-12

    Lisa K. Mahnke, Aleksandar Kondinski, Ulrike Warzok, Christian Näther, Jan van Leusen, Christoph A. Schalley, Kirill Yu. Monakhov, Paul Kögerler, Wolfgang Bensch

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  22. New Water‐Soluble Cluster Compound {Zn(en)3}3[V15Sb6O42(H2O)]⋅ (Ethylenediamine)3⋅10 H2O as a Synthon for the Generation of Two New Antimonato Polyoxovanadates

    Chemistry - A European Journal · 2018-02-21

    Lisa K. Mahnke, Ulrike Warzok, Mengxi Lin, Christian Näther, Christoph A. Schalley, Wolfgang Bensch

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  23. Rational Syntheses of Three New {V14Sb8} Clusters Applying a Water-Soluble High-Nuclearity Cluster as Synthon

    Crystal Growth & Design · 2018-08-20

    Lisa K. Mahnke, Michael Wendt, Christian Näther, Wolfgang Bensch

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  24. Mixing SbIIIand GeIVoccupancy in the polyoxovanadate {V14E8} archetype

    Zeitschrift für Naturforschung B · 2018-09-11

    Michael Wendt, Christian Näther, Jan van Leusen, Paul Kögerler, Wolfgang Bensch

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  25. Investigation of the Kinetic Stabilization of a Ce4+‐based MOF by in‐situ Powder X‐ray Diffraction

    Zeitschrift für anorganische und allgemeine Chemie · 2018-10-31

    Niclas Heidenreich, Steve Waitschat, Helge Reinsch

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  26. New pronounced progress in the synthesis of group 5 polyoxometalates

    CrystEngComm · 2020-01-01

    Joanna Dopta, Lisa K. Mahnke, Wolfgang Bensch

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  27. A Lacunary Polyoxovanadate Precursor and Transition‐Metal‐Sandwiched Derivatives for Catalytic Oxidation of Sulfides

    Chemistry - A European Journal · 2020-01-27

    Rong Wan, Peipei He, Zhen Liu, Xinyi Ma, Pengtao Ma, Vikram Singh, Chao Zhang, Jingyang Niu, Jingping Wang

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  28. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  29. The crystal structure of tetra(1-ethylimidazole-κ 1 N)-[μ 4-imidazole-4,5-dicarboxylato-κ 4 O, N, O′, N′]-trioxido-divanadium, C25H33N10O7V2

    Zeitschrift für Kristallographie - New Crystal Structures · 2023-04-13

    Na Li, Xiaojie Wang, Yucai Qin, Jingyun Wang

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  30. Two extended structures constructed by borate- or germanate-substituted octadecavanadate clusters

    Inorganic Chemistry Communications · 2023-06-05

    Kai‐Yao Wang, Xin Hao, Zi-Zhao Wang, Lin Cheng

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