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RESEARCH PAPER · Physical Chemistry Chemical Physics · 2000

On the advantages of the use of the three-element detector system for measuring EDXRD patterns to follow the crystallisation of open-framework structures

Gavin Muncaster, Andrew T. Davies, Gopinathan Sankar, C. Richard A. Catlow, John Meurig Thomas, Sally L. Colston, Paul Barnes, Richard I. Walton, Dermot O’Hare

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On the advantages of the use of the three-element detector system for measuring EDXRD patterns to follow the crystallisation of open-framework structuresOriginalAdvances in the Determination of the Architecture of Active Sites in Solid Catalysts2ChemInform Abstract: On the Advantages of the Use of the Three‐Element Detector System for Measuring EDXRD Patterns to Follow the Crystallization of Open‐Framework Structures.0Nucleation and crystallization of solids from solution81Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffraction42In‐Situtime‐resolved X‐ray diffraction: The current state of the art11An Investigation of the Synthesis of the Layered Perovskite RbCa2Nb3O10 Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction19In Situ Study of the Formation of Crystalline Bismuth Molybdate Materials under Hydrothermal Conditions133Cation Exchange, Dehydration, and Calcination in Clinoptilolite: In Situ X-ray Diffraction and Computer Modeling42In situ characterization of iron phosphate and bismuth molybdate catalysts prepared by hydrothermal methods: An EDXRD and combined XRD/XAS study21On the Nature and Location of Organic Template Molecules and Their Effect on the Stability and Redox Properties of Microporous CoAlPO-34 Catalyst12The paste hydration of brownmillerite with and without gypsum: a time resolved synchrotron diffraction study at 30, 70, 100 and 150 °C105Probing Molten Salt Flux Reactions Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction: A New Synthesis Route to the Mixed-Valence NaTi2O445Unraveling the Crystallization Mechanism of CoAPO-5 Molecular Sieves under Hydrothermal Conditions136In-situ XRD as a tool to understanding zeolite crystallization105Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18New insights into the formation of microporous materials by in situ scattering techniques35A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation8Watching the crystallisation of complex oxides by in situ X-ray techniques28Solvent Influences on Metastable Polymorph Lifetimes: Real-Time Interconversions Using Energy Dispersive X-Ray Diffractometry**We dedicate this paper to Professor David Grant. Not only a talented scientist, he was a man who gave freely of his time and ideas to support and encourage others, including ourselves.30Phase-selective crystallization of cobalt-incorporated aluminophosphate molecular sieves with large pore by microwave irradiation37Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion76Structure Determination: Experimental Techniques1Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates24Hydrothermal/autoclave synthesis of AlPO-5: a prototype space/time study of crystallisation gradients8On the Structure of Cobalt-Substituted Aluminophosphate Catalysts and Their Catalytic Performance1Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study210Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study47Control of polymorphism in NaNbO 3 by hydrothermal synthesis71Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite11An iron molybdate catalyst for methanol to formaldehyde conversion prepared by a hydrothermal method and its characterization75Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method41In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐584In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐524In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating36UV Raman spectroscopic study on the synthesis mechanism and assembly of molecular sieves138In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques39Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction47Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Incorporation of Ti(III) into the AlPO4-5 framework by direct synthesis8Synchrotron radiation techniques in materials and environmental science8Location and orientation of the N,N-diisopropylethylamine template molecule in the AlPO4-18 framework by X-ray synchrotron diffraction and molecular modelling4Understanding Mechanism and Designing Strategies for Sustainable Synthesis of Zeolites: A Personal Story19Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Metal-Substituted Microporous Aluminophosphates7A kinetic and mechanistic study into the transformation of calcium sulfate hemihydrate to dihydrate40MOFs in the time domain66Case Studies: Crystallography as a Tool for Studying Methanol Conversion in Zeolites2

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  1. Advances in the Determination of the Architecture of Active Sites in Solid Catalysts

    Springer eBooks · 2001-01-01

    Gopinathan Sankar, Robert Raja, J. M. Thomas, David Gleeson

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  2. ChemInform Abstract: On the Advantages of the Use of the Three‐Element Detector System for Measuring EDXRD Patterns to Follow the Crystallization of Open‐Framework Structures.

    ChemInform · 2001-01-02

    Gavin Muncaster, Andrew T. Davies, Gopinathan Sankar, C. Richard A. Catlow, John Meurig Thomas, Sally L. Colston, Paul Barnes, Richard I. Walton, Dermot M. O'Hare

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  3. Nucleation and crystallization of solids from solution

    Current Opinion in Solid State and Materials Science · 2001-10-01

    Ferdi Schüth

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  4. Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffraction

    Microporous and Mesoporous Materials · 2001-11-01

    Richard I. Walton, Ronald I. Smith, Dermot M. O'Hare

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  5. In‐Situtime‐resolved X‐ray diffraction: The current state of the art

    Synchrotron Radiation News · 2002-07-01

    Ann E. Terry, G. Vaughan, Åke Kvick, Richard I. Walton, Alexander J. Norquist, Dermot M. O'Hare

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  6. An Investigation of the Synthesis of the Layered Perovskite RbCa2Nb3O10 Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction

    Chemistry of Materials · 2002-09-05

    Margret J. Geselbracht, Richard I. Walton, E. Sarah Cowell, Franck Millange, Dermot M. O'Hare

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  7. In Situ Study of the Formation of Crystalline Bismuth Molybdate Materials under Hydrothermal Conditions

    Chemistry of Materials · 2002-11-21

    Andrew Michael Beale, Gopinathan Sankar

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  8. Cation Exchange, Dehydration, and Calcination in Clinoptilolite: In Situ X-ray Diffraction and Computer Modeling

    The Journal of Physical Chemistry B · 2003-01-01

    Matthew N. R. Johnson, D. O'Connor, Paul Barnes, C. Richard A. Catlow, Scott L. Owens, Gopinathan Sankar, Robert G. Bell, Simon J. Teat, Richard A. Stephenson

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  9. In situ characterization of iron phosphate and bismuth molybdate catalysts prepared by hydrothermal methods: An EDXRD and combined XRD/XAS study

    Nuclear Instruments and Methods in Physics Research Section B Beam Interactions with Materials and Atoms · 2003-01-01

    Andrew Michael Beale, Gopinathan Sankar

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  10. On the Nature and Location of Organic Template Molecules and Their Effect on the Stability and Redox Properties of Microporous CoAlPO-34 Catalyst

    Topics in Catalysis · 2003-10-01

    Gopinathan Sankar, Joanna K. Wyles, C. Richard A. Catlow

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  11. The paste hydration of brownmillerite with and without gypsum: a time resolved synchrotron diffraction study at 30, 70, 100 and 150 °C

    Journal of Materials Chemistry · 2004-01-01

    Nicola Meller, Christopher Hall, Andrew C. Jupe, Sally L. Colston, Simon D. M. Jacques, Paul Barnes, Jonathan Phipps

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  12. Probing Molten Salt Flux Reactions Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction: A New Synthesis Route to the Mixed-Valence NaTi2O4

    Chemistry of Materials · 2004-02-27

    Margret J. Geselbracht, Liam D. Noailles, Lien T. Ngo, Jessica H. Pikul, Richard I. Walton, E. Sarah Cowell, Franck Millange, Dermot M. O'Hare

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  13. Unraveling the Crystallization Mechanism of CoAPO-5 Molecular Sieves under Hydrothermal Conditions

    Journal of the American Chemical Society · 2005-09-24

    Didier Grandjean, Andrew Michael Beale, Andrei V. Petukhov, Bert Marc Weckhuysen

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  14. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

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  15. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

    Chemistry of Materials · 2006-07-18

    Gareth R. Williams, Alexander J. Norquist, Dermot M. O'Hare

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  16. New insights into the formation of microporous materials by in situ scattering techniques

    Faraday Discussions · 2007-01-01

    Gopinathan Sankar, Tatsuya Okubo, Wei Fan, Florian Meneau

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  17. A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation

    The Journal of Physical Chemistry A · 2007-02-02

    Mei Dong, Guofu Wang, Zhangfeng Qin, Jianguo Wang, Tao Liu, Shuping Yuan, Haijun Jiao

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  18. Watching the crystallisation of complex oxides by in situ X-ray techniques

    Applied Catalysis A General · 2007-03-04

    Andrew Michael Beale, Lee M. Reilly, Gopinathan Sankar

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  19. Solvent Influences on Metastable Polymorph Lifetimes: Real-Time Interconversions Using Energy Dispersive X-Ray Diffractometry**We dedicate this paper to Professor David Grant. Not only a talented scientist, he was a man who gave freely of his time and ideas to support and encourage others, including ourselves.

    Journal of Pharmaceutical Sciences · 2007-04-24

    L. L. DEMATOS, Adrian C. Williams, Steven W. Booth, Catherine R. Petts, DAVID J. TAYLOR, N. Blagden

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  20. Phase-selective crystallization of cobalt-incorporated aluminophosphate molecular sieves with large pore by microwave irradiation

    Microporous and Mesoporous Materials · 2007-04-30

    Sung Hwa Jhung, Taihuan Jin, Young Ho Kim, Jong‐San Chang

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  21. Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion

    The Journal of Physical Chemistry C · 2007-10-01

    Banghao Chen, Yining Huang

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  22. Structure Determination: Experimental Techniques

    Royal Society of Chemistry eBooks · 2007-10-15

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  23. Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates

    The Journal of Physical Chemistry C · 2007-10-23

    Matthew G. O’Brien, Manuel Sánchez‐Sánchez, Andrew Michael Beale, Dewi W. Lewis, Gopinathan Sankar, C. Richard A. Catlow

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  24. Hydrothermal/autoclave synthesis of AlPO-5: a prototype space/time study of crystallisation gradients

    Journal of Materials Science · 2007-11-29

    Vesna Middelkoop, Simon D. M. Jacques, Matthew G. O’Brien, Andrew Michael Beale, Paul Barnes

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  25. On the Structure of Cobalt-Substituted Aluminophosphate Catalysts and Their Catalytic Performance

    Springer eBooks · 2008-04-05

    Gopinathan Sankar, Robert Raja

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  26. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

    Angewandte Chemie International Edition · 2008-04-18

    Franck Millange, Christian Serre, Nathalie Guillou, Gérard Férey, Richard I. Walton

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  27. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

    Angewandte Chemie · 2008-04-18

    Franck Millange, Christian Serre, Nathalie Guillou, Gérard Férey, Richard I. Walton

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  28. Control of polymorphism in NaNbO 3 by hydrothermal synthesis

    Chemical Communications · 2008-11-12

    Deena R. Modeshia, Richard J. Darton, Sharon Elizabeth Ashbrook, Richard I. Walton

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  29. Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite

    Dalton Transactions · 2009-01-01

    Robin D. Fisher, Richard I. Walton

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  30. An iron molybdate catalyst for methanol to formaldehyde conversion prepared by a hydrothermal method and its characterization

    Applied Catalysis A General · 2009-05-14

    Andrew Michael Beale, Simon D. M. Jacques, E. Sacaliuc, Matthew G. O’Brien, Paul Barnes, Bert Marc Weckhuysen

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  31. Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method

    The Journal of Physical Chemistry C · 2009-08-18

    Banghao Chen, Christopher W. Kirby, Yining Huang

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  32. In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐5

    Angewandte Chemie International Edition · 2009-10-13

    Fengtao Fan, Zhaochi Feng, Keju Sun, Meiling Guo, Qiang Guo, Yu Song, Wei‐Xue Li, Can Li

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  33. In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐5

    Angewandte Chemie · 2009-10-13

    Fengtao Fan, Zhaochi Feng, Keju Sun, Meiling Guo, Qiang Guo, Yu Song, Wei‐Xue Li, Can Li

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  34. In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating

    The Journal of Physical Chemistry C · 2009-11-02

    David Stephen Wragg, P.J. Byrne, G. Giriat, Benjamin Le Ouay, Róbert Gyepes, Andrew Harrison, A. Gavin Whittaker, Russell E. Morris

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  35. UV Raman spectroscopic study on the synthesis mechanism and assembly of molecular sieves

    Chemical Society Reviews · 2010-01-01

    Fengtao Fan, Zhaochi Feng, Can Li

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  36. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

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  37. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

    Angewandte Chemie · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

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  38. Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques

    The Journal of Physical Chemistry C · 2011-03-07

    Andrew Michael Beale, Matthew G. O’Brien, Marta Kasunič, Amalija Golobič, Manuel Sánchez‐Sánchez, Alan J. W. Lobo, Dewi W. Lewis, David Stephen Wragg, Sergey Nikitenko, Wim Bras, Bert Marc Weckhuysen

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  39. Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction

    Chemistry - A European Journal · 2011-05-09

    Richard I. Walton, Alexis S. Munn, Nathalie Guillou, Franck Millange

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  40. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

    Chemistry - A European Journal · 2012-10-10

    Е. А. Антонова, Beatrix Seidlhofer, Jing Wang, Michael Hinz, Wolfgang Bensch

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  41. Incorporation of Ti(III) into the AlPO4-5 framework by direct synthesis

    Microporous and Mesoporous Materials · 2014-02-28

    Almudena Alfayate, Manuel Sánchez‐Sánchez, Joaquín Pérez‐Pariente

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  42. Synchrotron radiation techniques in materials and environmental science

    Philosophical Transactions of the Royal Society A Mathematical Physical and Engineering Sciences · 2015-01-26

    C. Richard A. Catlow

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  43. Location and orientation of the N,N-diisopropylethylamine template molecule in the AlPO4-18 framework by X-ray synchrotron diffraction and molecular modelling

    CHINESE JOURNAL OF CATALYSIS (CHINESE VERSION) · 2015-06-01

    Christiana Zenonos, Dewi W. Lewis, Gopinathan Sankar

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  44. Understanding Mechanism and Designing Strategies for Sustainable Synthesis of Zeolites: A Personal Story

    The Chemical Record · 2016-03-24

    Yeqing Wang, Feng‐Shou Xiao

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  45. Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies

    European Journal of Inorganic Chemistry · 2016-09-19

    Michael Wendt, Lisa K. Mahnke, Niclas Heidenreich, Wolfgang Bensch

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  46. Metal-Substituted Microporous Aluminophosphates

    Structure and bonding · 2018-01-01

    Gopinathan Sankar, Manuel Sánchez‐Sánchez

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  47. A kinetic and mechanistic study into the transformation of calcium sulfate hemihydrate to dihydrate

    Journal of Synchrotron Radiation · 2019-04-04

    Sebastian J. Gurgul, Gabriel Seng, Gareth R. Williams

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  48. MOFs in the time domain

    Nature Reviews Chemistry · 2021-12-02

    Daniel J. Cerasale, Dominic C. Ward, Timothy L. Easun

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  49. Case Studies: Crystallography as a Tool for Studying Methanol Conversion in Zeolites

    Springer handbooks · 2023-01-01

    Pablo Beato, L. F. Lundegaard, Stian Svelle, David Stephen Wragg

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