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RESEARCH PAPER · European Journal of Inorganic Chemistry · 2003

In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions

Lars Engelke, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal ConditionsOriginalFour New Thioantimonates(III) with the General Formula [TM(tren)]Sb4S7 (TM = Mn, Fe, Co, Zn) with the Transition Metal as Part of a Thioantimonate(III) Network Synthesized under Solvothermal Conditions and Tuning of the Optical Band Gap by the Transition Metal Cation84In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure110In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions32Thermal disproportionation of SnO under high pressure18Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24In-situ XRD as a tool to understanding zeolite crystallization105Combined In Situ EDXRD/EXAFS Investigation of the Crystal Growth of [Co(C6H18N4)][Sb2S4] under Solvothermal Conditions: Two Different Reaction Pathways Leading to the Same Product62The Reaction Mechanism of a Complex Intercalation System: In Situ X‐ray Diffraction Studies of the Chemical and Electrochemical Lithium Intercalation in Cr4TiSe819Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62Morphological and Kinetic Studies on Hexagonal Tungstates55Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation45The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study38Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility26In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42A thermosyphon-driven hydrothermal flow-through cell forin situand time-resolved neutron diffraction studies14Five dimeric thiogermanates with transition metal complexes of multidentate chelating amines: Syntheses, structures, magnetism and photoluminescence41Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation132In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts16A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Systematic and In Situ Energy Dispersive X-ray Diffraction Investigations on the Formation of Lanthanide Phosphonatobutanesulfonates: Ln(O3P-C4H8-SO3)(H2O) (Ln = La−Gd)53In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties43From Zero- to Three-Dimensional Thioantimonates: [Ni(aepa)2]3Sb6S12 (aepa = C5H15N3 = N-(aminoethyl)-1,3-propandiamine), Containing the Unique [Sb6S12]6– Cyclic Anion, [Ni(aepa)2]6(Sb3S6)2(SO4)3·2H2O, with Isolated [Sb3S6]3– anions and [Ni(aepa)2]Sb4S7, Characterized by a Three-Dimensional Network Structure39In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts57In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials32Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique34Investigations of the crystallization mechanism of CrSb and CrSb2 multilayered films using in-situ X-ray diffraction and in-situ X-ray reflectometry12On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)16Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Kinetics of Phase Transformations and of Other Time‐Dependent Processes in Solids Analyzed by Powder Diffraction4Nanostructured Inorganic–Organic Hybrid Semiconductor Materials3Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies72In Situ Studies of Solvothermal Synthesis of Energy Materials159Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds33Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28In Situ Studies on Phase Transitions of Tris(acetylacetonato)-Aluminum(III) Al(acac)321In situ luminescence analysis: a new light on monitoring calcium phosphate phase transitions26Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles33Panoramic Synthesis as an Effective Materials Discovery Tool: The System Cs/Sn/P/Se as a Test Case46In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?20In situ scattering studies of material formation during wet-chemical syntheses1Crystallisation of phosphates revisited: a multi-step formation process for SrHPO44A kinetic study of the crystallization of LTA-type zeolite from colloidal solutions by in-situ ultrasonic attenuation measurements0

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  1. Four New Thioantimonates(III) with the General Formula [TM(tren)]Sb4S7 (TM = Mn, Fe, Co, Zn) with the Transition Metal as Part of a Thioantimonate(III) Network Synthesized under Solvothermal Conditions and Tuning of the Optical Band Gap by the Transition Metal Cation

    Zeitschrift für anorganische und allgemeine Chemie · 2004-10-01

    Michael Schaefer, Ralph Stähler, Ragnar Kiebach, Christian Näther, Wolfgang Bensch

    Read original paper ↗ ·

  2. In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure

    Physical Chemistry Chemical Physics · 2005-01-01

    Jan‐Dierk Grunwaldt, Alfons Baiker

    Read original paper ↗ ·

  3. In‐situ Energy Dispersive X‐ray Diffraction Studies of the Crystallization of (1, 2‐DAPH2)2Ge9(OH)4O18 · 2 H2O under Solvothermal Conditions

    Zeitschrift für anorganische und allgemeine Chemie · 2005-02-01

    Ragnar Kiebach, Michael Schaefer, Felix Porsch, Wolfgang Bensch

    Read original paper ↗ ·

  4. Thermal disproportionation of SnO under high pressure

    Solid State Ionics · 2005-04-13

    Hubertus Giefers, Felix Porsch, Gerhard Wortmann

    Read original paper ↗ ·

  5. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

    Angewandte Chemie International Edition · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  6. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

    Angewandte Chemie · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  7. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

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  8. Combined In Situ EDXRD/EXAFS Investigation of the Crystal Growth of [Co(C6H18N4)][Sb2S4] under Solvothermal Conditions: Two Different Reaction Pathways Leading to the Same Product

    Chemistry of Materials · 2006-02-08

    Ragnar Kiebach, Nicole Pienack, M.-E. Ordolff, Felix Studt, Wolfgang Bensch

    Read original paper ↗ ·

  9. The Reaction Mechanism of a Complex Intercalation System: In Situ X‐ray Diffraction Studies of the Chemical and Electrochemical Lithium Intercalation in Cr4TiSe8

    Chemistry - A European Journal · 2006-05-24

    Malte Behrens, Ragnar Kiebach, Jannes Ophey, Oliver Riemenschneider, Wolfgang Bensch

    Read original paper ↗ ·

  10. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

    Chemistry - A European Journal · 2006-11-17

    Alexej Michailovski, Greta Ricarda Patzke

    Read original paper ↗ ·

  11. Morphological and Kinetic Studies on Hexagonal Tungstates

    Chemistry of Materials · 2006-12-20

    Alexej Michailovski, Ragnar Kiebach, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alfons Baiker, Sridhar Komarneni, Greta Ricarda Patzke

    Read original paper ↗ ·

  12. Solvothermal Syntheses of Two New Thiostannates and an In‐Situ Energy Dispersive X‐ray Scattering Study of Their Formation

    European Journal of Inorganic Chemistry · 2009-02-06

    Nicole Pienack, Christian Näther, Wolfgang Bensch

    Read original paper ↗ ·

  13. The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study

    Small · 2009-06-22

    Ying Zhou, Nicole Pienack, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  14. Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility

    Progress in Solid State Chemistry · 2009-11-07

    Wolfgang Bensch, Thomas Bredow, H. Ebert, Paul Heitjans, Sylvio Indris, S. Mankovsky, Martin Wilkening

    Read original paper ↗ ·

  15. In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures

    Nanoscale · 2010-01-01

    Ying Zhou, Е. А. Антонова, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  16. A thermosyphon-driven hydrothermal flow-through cell forin situand time-resolved neutron diffraction studies

    Journal of Applied Crystallography · 2010-03-25

    Fang Xia, Brian O’Neill, Yung Ngothai, Jason Peak, Christophe Tenailleau, Barbara E. Etschmann, Gujie Qian, Joël Brugger, Andrew J. Studer, Scott R. Olsen, Allan Pring

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  17. Five dimeric thiogermanates with transition metal complexes of multidentate chelating amines: Syntheses, structures, magnetism and photoluminescence

    Journal of Molecular Structure · 2010-08-27

    Guang‐Ning Liu, Guo‐Cong Guo, Ming‐Sheng Wang, Li‐Zhen Cai, Jin‐Shun Huang

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  18. Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation

    Journal of Solid State Chemistry · 2010-09-18

    Yi Liu, Pushkar D. Kanhere, Chui Ling Wong, Yuefeng Tian, Yuhua Feng, Freddy Boey, Tom Wu, Hongyu Chen, Timothy John White, Zhong Chen, Qichun Zhang

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  19. In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts

    The Journal of Physical Chemistry C · 2010-09-20

    James A. Dorman, Yuanbing Mao, John Bargar, Jane P. Chang

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  20. A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework

    CrystEngComm · 2010-10-01

    Franck Millange, Racha El Osta, Manuela E. Medina, Richard I. Walton

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  21. Systematic and In Situ Energy Dispersive X-ray Diffraction Investigations on the Formation of Lanthanide Phosphonatobutanesulfonates: Ln(O3P-C4H8-SO3)(H2O) (Ln = La−Gd)

    Inorganic Chemistry · 2010-11-08

    Mark Feyand, Christian Näther, André Rothkirch, Norbert Stock

    Read original paper ↗ ·

  22. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

    Read original paper ↗ ·

  23. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

    Angewandte Chemie · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

    Read original paper ↗ ·

  24. A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties

    Inorganic Chemistry Communications · 2011-03-16

    Yi Liu, Yufeng Tian, Fengxia Wei, Michael Ser Chong Ping, Chuanwei Huang, Freddy Boey, Christian Kloc, Lang Chen, Tom Wu, Qichun Zhang

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  25. From Zero- to Three-Dimensional Thioantimonates: [Ni(aepa)2]3Sb6S12 (aepa = C5H15N3 = N-(aminoethyl)-1,3-propandiamine), Containing the Unique [Sb6S12]6– Cyclic Anion, [Ni(aepa)2]6(Sb3S6)2(SO4)3·2H2O, with Isolated [Sb3S6]3– anions and [Ni(aepa)2]Sb4S7, Characterized by a Three-Dimensional Network Structure

    Crystal Growth & Design · 2011-10-10

    Beatrix Seidlhofer, John Djamil, Christian Näther, Wolfgang Bensch

    Read original paper ↗ ·

  26. In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts

    Dalton Transactions · 2012-01-01

    Stefan Zander, Beatrix Seidlhofer, Malte Behrens

    Read original paper ↗ ·

  27. In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials

    European Journal of Inorganic Chemistry · 2012-01-03

    Ying Zhou, Е. А. Антонова, Yuanhua Lin, Jan‐Dierk Grunwaldt, Wolfgang Bensch, Greta Ricarda Patzke

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  28. Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique

    Chemistry - A European Journal · 2012-01-16

    Inga Olliges‐Stadler, Jan Stötzel, Dorota Koziej, Marta D. Rossell, Jan‐Dierk Grunwaldt, Maarten Nachtegaal, R. Frahm, Markus Niederberger

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  29. Investigations of the crystallization mechanism of CrSb and CrSb2 multilayered films using in-situ X-ray diffraction and in-situ X-ray reflectometry

    Journal of Solid State Chemistry · 2012-07-27

    Matthias Regus, Gerhard Kuhn, Sergej Mankovsky, H. Ebert, Wolfgang Bensch

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  30. On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-09-26

    Beatrix Seidlhofer, Е. А. Антонова, Jing Wang, Diana Schinkel, Wolfgang Bensch

    Read original paper ↗ ·

  31. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

    Chemistry - A European Journal · 2012-10-10

    Е. А. Антонова, Beatrix Seidlhofer, Jing Wang, Michael Hinz, Wolfgang Bensch

    Read original paper ↗ ·

  32. Kinetics of Phase Transformations and of Other Time‐Dependent Processes in Solids Analyzed by Powder Diffraction

    Unknown journal · 2012-10-15

    Andreas Leineweber, E. J. Mittemeijer

    Read original paper ↗ ·

  33. Nanostructured Inorganic–Organic Hybrid Semiconductor Materials

    Elsevier eBooks · 2013-01-01

    Jing Li, R. Zhang

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  34. Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies

    Inorganic Chemistry · 2013-07-17

    Felicitas Niekiel, Maximilian Ackermann, Paul Guerrier, André Rothkirch, Norbert Stock

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  35. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  36. Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds

    Inorganic Chemistry · 2014-05-20

    Jessica Hilbert, Christian Näther, Wolfgang Bensch

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  37. Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies

    European Journal of Inorganic Chemistry · 2016-09-19

    Michael Wendt, Lisa K. Mahnke, Niclas Heidenreich, Wolfgang Bensch

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  38. In Situ Studies on Phase Transitions of Tris(acetylacetonato)-Aluminum(III) Al(acac)3

    Crystals · 2016-11-28

    Nicole Pienack, Laura Ruiz Arana, Wolfgang Bensch, Huayna Terraschke

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  39. In situ luminescence analysis: a new light on monitoring calcium phosphate phase transitions

    Inorganic Chemistry Frontiers · 2017-01-01

    Huayna Terraschke, Merrit Rothe, A.-M. Tsirigoni, Patric Lindenberg, Laura Ruiz Arana, Niclas Heidenreich, F. Bertram, Martin Etter

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  40. Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles

    The Journal of Physical Chemistry C · 2017-02-13

    Siyu Yao, Ce Yang, Huabo Zhao, Siwei Li, Lili Lin, Wen Wen, Jinxun Liu, Gang Hu, Wei‐Xue Li, Yanglong Hou, Ding Ma

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  41. Panoramic Synthesis as an Effective Materials Discovery Tool: The System Cs/Sn/P/Se as a Test Case

    Journal of the American Chemical Society · 2017-06-30

    Alyssa S. Haynes, Constantinos C. Stoumpos, Haijie Chen, Daniel G. Chica, Mercouri G. Kanatzidis

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  42. In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review

    Reviews in Analytical Chemistry · 2017-08-19

    Huayna Terraschke, Merrit Rothe, Patric Lindenberg

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  43. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

    Review of Scientific Instruments · 2017-10-01

    Niclas Heidenreich, U. Rütt, Milan Köppen, A. Ken Inge, S. Beier, Ann‐Christin Dippel, Ralf Suren, Norbert Stock

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  44. From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?

    Physical Chemistry Chemical Physics · 2017-12-20

    Philipp Müscher‐Polzin, Irma Vania Eliani, Jonas Ströh, M. Braun, Niklas Ruser, Niclas Heidenreich, Pia Rönfeldt, Florian Bertram, Christian Näther, Stephan Wöhlbrandt, Markus Suta, Huayna Terraschke

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  45. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  46. Crystallisation of phosphates revisited: a multi-step formation process for SrHPO4

    Zeitschrift für Naturforschung B · 2022-03-03

    Laura Ruiz Arana, Jonas Ströh, Jasper Amtsfeld, Giscard Doungmo, Dmitri Novikov, Azat Khadiev, Martin Etter, Michael T. Wharmby, Markus Suta, Huayna Terraschke

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  47. A kinetic study of the crystallization of LTA-type zeolite from colloidal solutions by in-situ ultrasonic attenuation measurements

    Microporous and Mesoporous Materials · 2026-09-28

    Hasan Baser, Martin Hartmann, Wilhelm Schwieger

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