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RESEARCH ARTICLE · Angewandte Chemie International Edition · 2005

Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD TechniquesOriginalThirteenth Bowditch lecture. The determinants of myocardial oxygen consumption.153In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure110One-Pot Redox Syntheses of Heteronanostructures of Ag Nanoparticles on MoO3 Nanofibers222D-Mapping of the Catalyst Structure Inside a Catalytic Microreactor at Work: Partial Oxidation of Methane over Rh/Al 2 O 3158Molybdenum trioxide nanostructures prepared by thermal oxidization of molybdenum91Molybdenum Trioxide Nanostructures: The Evolution from Helical Nanosheets to Crosslike Nanoflowers to Nanobelts80Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates7Morphological and Kinetic Studies on Hexagonal Tungstates55Hydrothermal synthesis of anisotropic alkali and alkaline earth vanadates15Targeted Synthesis of Nanostructured Oxide Materials2A New Facile Approach to the Synthesis of 3-Methylthio-Substituted Furans, Pyrroles, Thiophenes, and Related Derivatives155Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape64Hydrothermal synthesis of MoO3 nanobelts utilizing poly(ethylene glycol)119Surfactant‐Free Nonaqueous Synthesis of Metal Oxide Nanostructures478Tensidfreie nichtwässrige Synthese von Metalloxid‐Nanostrukturen36Hydrothermal Strategies Towards Polyoxofluoromolybdates(VI)18Single‐Crystalline Molybdenum Trioxide Nanoribbons: Photocatalytic, Photoconductive, and Electrochemical Properties126Kinetic and Thermodynamic Aspects in the Microwave-Assisted Synthesis of ZnO Nanoparticles in Benzyl Alcohol236Synthesis and Structural Characterization of a Novel Three-dimensional Molybdenum–Oxygen Framework Constructed from Mo3O9 Units10In Situ High‐Energy Synchrotron Radiation Study of Boehmite Formation, Growth, and Phase Transformation to Alumina in Sub‐ and Supercritical Water26Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility26In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42Modification of bone-like apatite nanoparticle size and growth kinetics by alizarin red S29Synthesis of molybdenum oxide hollow microspheres by ethanol and PEG assisting hydrothermal process26A novel additive-free oxides–hydrothermal approach for monazite-type LaPO4nanomaterials with controllable morphologies9In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts16Anisotropic Crystal Growth Kinetics of Anatase TiO2 Nanoparticles Synthesized in a Nonaqueous Medium80Synthesis and characterization of single-crystalline α-MoO3 nanofibers for enhanced Li-ion intercalation applications100Oxide Nanomaterials: Synthetic Developments, Mechanistic Studies, and Technological Innovations366Oxidische Nanomaterialien: Von der Synthese über den Mechanismus zur technologischen Innovation25Time Resolved in Situ XAFS Study of the Electrochemical Oxygen Intercalation in SrFeO2.5 Brownmillerite Structure: Comparison with the Homologous SrCoO2.5 System80Interplay Between Size and Crystal Structure of Molybdenum Dioxide Nanoparticles—Synthesis, Growth Mechanism, and Electrochemical Performance92MoO3 nanowires as electrochemical pseudocapacitor materials144Single-crystalline MoO3 nanoplates: topochemical synthesis and enhanced ethanol-sensing performance209The interplay of crystallization kinetics and morphology during the formation of SnO2 nanorods: snapshots of the crystallization from fast microwave reactions24In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Synthesis of α-MoO3 Microspheres Assembled by Nanorods in Room Temperature Ionic Liquids0In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts57Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique34Probing Liquid/Solid Interfaces at the Molecular Level458Optimizing the crystal environment through extended x-ray absorption fine structure to increase the luminescent lifetimes of Er3+ doped Y2O3 nanoparticles14A Modular and Scalable One‐Pot Synthesis of Polysubstituted Furans70A Modular and Scalable One‐Pot Synthesis of Polysubstituted Furans13Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions30Quantum Mechanics Insight into the Microwave Nucleation of SrTiO3Nanospheres80DFT+U Study of Properties of MoO3and Hydrogen Adsorption on MoO3(010)105A comprehensive study of the crystallization mechanism involved in the nonaqueous formation of tungstite33In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water16Template-mediated growth of microsphere, microbelt and nanorod α-MoO3 structures and their high pseudo-capacitances51A facile hydrothermal method for the fabrication of one-dimensional MoO3 nanobelts27Snapshots of the Formation of NaTi3O6(OH)·2H2O Nanowires: A Time‐Resolved XRD/HRTEM Study7High-throughput ultrasonic synthesis and in situ crystallisation investigation of metal phosphonocarboxylates25Alteration of architecture of MoO 3 nanostructures on arbitrary substrates: growth kinetics, spectroscopic and gas sensing properties108In Situ Studies of Solvothermal Synthesis of Energy Materials159Puzzling Mechanism behind a Simple Synthesis of Cobalt and Cobalt Oxide Nanoparticles: In Situ Synchrotron X-ray Absorption and Diffraction Studies70Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study41In Situ X‑ray Diffraction Study of the Formation, Growth, and Phase Transition of Colloidal Cu2– x S Nanocrystals61Hydrothermal synthesis and formation mechanism of photocatalytically active SrTiO 3 nanocrystals using anatase TiO 2 with different facets as a precursor19In situ microcalorimetry study of ZnFe 2 O 4 nanoparticle formation under solvothermal conditions20Matching the organic and inorganic counterparts during nucleation and growth of copper-based nanoparticles – in situ spectroscopic studies39One-dimensional manganese-cobalt oxide nanofibres as bi-functional cathode catalysts for rechargeable metal-air batteries109Systematic study on the influence of the morphology of α-MoO3 in the selective oxidation of propylene28MoV 2 O 8 nanostructures: controlled synthesis and lithium storage mechanism37High photocatalytic performance of a type-II α-MoO 3 @MoS 2 heterojunction: from theory to experiment64Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties29Mobile Polaronic States in α-MoO3: An ab Initio Investigation of the Role of Oxygen Vacancies and Alkali Ions55Single crystalline flowerlike α-MoO3 nanorods and their application as anode material for lithium-ion batteries52Mesoporous Spinel Nanofibers and Nitrogen‐doped Carbon Nanotubes as High‐Performance Electrocatalyst for Oxygen Reduction in Alkaline and Neutral Media10Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Development of hierarchical layered nanostructuredα-MoO3thin films using dc magnetron sputtering21Cell Designs for In Situ and Operando Studies22Self-template synthesis of ATiO 3 (A = Ba, Pb and Sr) perovskites for photocatalytic removal of NO18Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125Recent Advances in Selective Propylene Oxidation over Bismuth Molybdate Based Catalysts: Synthetic, Spectroscopic, and Theoretical Approaches84Synthesis, Characterization, and Application of One‐Dimensional ( 1D ) Nanostructures0Sheet-like orthorhombic MoO3 nanostructures prepared via hydrothermal approach for visible-light-driven photocatalytic application30Catalyst free single-step processes to grow crystalline MoO 3 nanowires by reactive sputtering method4α-MoO3- by plasma etching with improved capacity and stabilized structure for lithium storage167Tweaking the Electronic and Optical Properties of α-MoO3 by Sulphur and Selenium Doping – a Density Functional Theory Study42γ-Radiolysis as a highly efficient green approach to the synthesis of metal nanoclusters: A review of mechanisms and applications56Kinetics of the Topochemical Transformation of (PbSe)m(TiSe2)n(SnSe2)m(TiSe2)n to (Pb0.5Sn0.5Se)m(TiSe2)n4Effect of oxygen partial pressure on the growth of molybdenum trioxide thin films7Synthesis of porous MoV2O8 nanosheets as anode material for superior lithium storage34Moving Frontiers in Transition Metal Catalysis: Synthesis, Characterization and Modeling50Laser Synthesis and Spectroscopy of Molybdenum Oxide Nanorods6Optimized enhanced photodegradation activity of sintered molybdenum oxide: A morphological hierarchy in wastewater treatment5Rapid synthesis of vertically aligned α-MoO 3 nanostructures on substrates11Probing Liquid/Solid Interfaces at the Molecular Level1In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11A High‐Rate Aqueous Proton Battery Delivering Power Below −78 °C via an Unfrozen Phosphoric Acid257In-situ preparation of molybdenum trioxide-silver composites for the improved photothermal catalytic performance of cyclohexane oxidation51The Jahn-Teller Effect for Amorphization of Molybdenum Trioxide towards High-Performance Fiber Supercapacitor34Growth, characterization and performance of bulk and nanoengineered molybdenum oxides for electrochemical energy storage and conversion45Probing Active Sites in CuxPdy Cluster Catalysts by Machine-Learning-Assisted X-ray Absorption Spectroscopy37In situ scattering studies of material formation during wet-chemical syntheses1Electronic and Chemical Properties: X‐Ray Absorption and Photoemission1Enhanced Jahn–Teller distortion boosts molybdenum trioxide's superior lithium ion storage capability19Hydrothermally grown α-MoO3 microfibers for photocatalytic degradation of methylene blue dye33Solvothermal and hydrothermal methods for preparative solid-state chemistry5From DFT investigations of oxygen-implanted molybdenum disulfide to temperature-induced stabilization of MoS2/MoO3 heterostructure14Efficient syngas conversion via catalytic shunt100Tailoring the optoelectronic properties of MoOX nanoparticles: a novel microwave-assisted synthesis for near-infrared absorbing polyoxometallic clusters0Synthesis Strategies and Multifaceted Applications of Molybdenum‐Based Nanomaterials: A Comprehensive Review13

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  1. Thirteenth Bowditch lecture. The determinants of myocardial oxygen consumption.

    PubMed · 1969

    Eugene Braunwald M. D

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  2. In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure

    Physical Chemistry Chemical Physics · 2005

    Jan‐Dierk Grunwaldt, Alfons Baiker

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  3. One-Pot Redox Syntheses of Heteronanostructures of Ag Nanoparticles on MoO3 Nanofibers

    The Journal of Physical Chemistry B · 2006

    Wenjun Dong, Zhan Shi, Jingjing Ma, Changmin Hou, Qiang Wan, Shouhua Feng, Andrew Cogbill, Z. Ryan Tian

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  4. 2D-Mapping of the Catalyst Structure Inside a Catalytic Microreactor at Work: Partial Oxidation of Methane over Rh/Al 2 O 3

    The Journal of Physical Chemistry B · 2006

    Jan‐Dierk Grunwaldt, Stefan Hannemann, Christian G. Schroer, Alfons Baiker

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  5. Molybdenum trioxide nanostructures prepared by thermal oxidization of molybdenum

    Journal of Crystal Growth · 2006

    Qing-Ping Ding, Huandi Huang, Junhong Duan, Jiangfeng Gong, Shaoguang Yang, Xiaoning Zhao, Youwei Du

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  6. Molybdenum Trioxide Nanostructures: The Evolution from Helical Nanosheets to Crosslike Nanoflowers to Nanobelts

    The Journal of Physical Chemistry B · 2006

    Guicun Li, Li Jiang, Shuping Pang, Hongrui Peng, Zhikun Zhang

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  7. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

    Chemistry - A European Journal · 2006

    Alexej Michailovski, Greta Ricarda Patzke

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  8. Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates

    Zeitschrift für anorganische und allgemeine Chemie · 2006

    Alexej Michailovski, Greta Ricarda Patzke

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  9. Morphological and Kinetic Studies on Hexagonal Tungstates

    Chemistry of Materials · 2006

    Alexej Michailovski, Ragnar Kiebach, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alfons Baiker, Sridhar Komarneni, Greta Ricarda Patzke

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  10. Hydrothermal synthesis of anisotropic alkali and alkaline earth vanadates

    Journal of materials research/Pratt's guide to venture capital sources · 2007

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  11. Targeted Synthesis of Nanostructured Oxide Materials

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  12. A New Facile Approach to the Synthesis of 3-Methylthio-Substituted Furans, Pyrroles, Thiophenes, and Related Derivatives

    The Journal of Organic Chemistry · 2008

    Guodong Yin, Zihua Wang, Aihua Chen, Meng Gao, An‐Xin Wu, Yuanjiang Pan

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  13. Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape

    Chemistry of Materials · 2008

    Ragnar Kiebach, Nicole Pienack, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alexej Michailovski, Alfons Baiker, Thomas Fox, Ying Zhou, Greta Ricarda Patzke

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  14. Hydrothermal synthesis of MoO3 nanobelts utilizing poly(ethylene glycol)

    Journal of Power Sources · 2008

    Ch. Venkata Reddy, Edwin H. Walker, Wen Chen, Sun‐il Mho

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  15. Surfactant‐Free Nonaqueous Synthesis of Metal Oxide Nanostructures

    Angewandte Chemie International Edition · 2008

    Nicola Pinna, Markus Niederberger

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  16. Tensidfreie nichtwässrige Synthese von Metalloxid‐Nanostrukturen

    Angewandte Chemie · 2008

    Nicola Pinna, Markus Niederberger

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  17. Hydrothermal Strategies Towards Polyoxofluoromolybdates(VI)

    Crystal Growth & Design · 2008

    Alexej Michailovski, Firasat Hussain, Bernhard Spingler, Jörg Wagler, Greta Ricarda Patzke

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  18. Single‐Crystalline Molybdenum Trioxide Nanoribbons: Photocatalytic, Photoconductive, and Electrochemical Properties

    Chemistry - A European Journal · 2009

    Liang Cheng, Mingwang Shao, Xiuhua Wang, Haibo Hu

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  19. Kinetic and Thermodynamic Aspects in the Microwave-Assisted Synthesis of ZnO Nanoparticles in Benzyl Alcohol

    ACS Nano · 2009

    Idalia Bilecka, Pierre Elser, Markus Niederberger

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  20. Synthesis and Structural Characterization of a Novel Three-dimensional Molybdenum–Oxygen Framework Constructed from Mo3O9 Units

    Chemistry Letters · 2009

    Junwei Zhao, Pengtao Ma, Jingping Wang, Jingyang Niu

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  21. In Situ High‐Energy Synchrotron Radiation Study of Boehmite Formation, Growth, and Phase Transformation to Alumina in Sub‐ and Supercritical Water

    Chemistry - A European Journal · 2009

    Nina Lock, Martin Bremholm, Mogens Christensen, Jonathan Almer, Yu‐Sheng Chen, Bo B. Iversen

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  22. Li intercalation and anion/cation substitution of transition metal chalcogenides: Effects on crystal structure, microstructure, magnetic properties and Li+ ion mobility

    Progress in Solid State Chemistry · 2009

    Wolfgang Bensch, Thomas Bredow, H. Ebert, Paul Heitjans, Sylvio Indris, S. Mankovsky, Martin Wilkening

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  23. In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures

    Nanoscale · 2010

    Ying Zhou, Е. А. Антонова, Wolfgang Bensch, Greta Ricarda Patzke

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  24. Modification of bone-like apatite nanoparticle size and growth kinetics by alizarin red S

    Nanoscale · 2010

    Casper Jon Steenberg Ibsen, Henrik Birkedal

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  25. Synthesis of molybdenum oxide hollow microspheres by ethanol and PEG assisting hydrothermal process

    Materials Letters · 2010

    Zhiqi Wang, Hongfen Wang, Cheng Yang, Jinhu Wu

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  26. A novel additive-free oxides–hydrothermal approach for monazite-type LaPO4nanomaterials with controllable morphologies

    Journal of Applied Crystallography · 2010

    Jie Ma, Qingsheng Wu

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  27. In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts

    The Journal of Physical Chemistry C · 2010

    James A. Dorman, Yuanbing Mao, John Bargar, Jane P. Chang

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  28. Anisotropic Crystal Growth Kinetics of Anatase TiO2 Nanoparticles Synthesized in a Nonaqueous Medium

    Chemistry of Materials · 2010

    Grethe Vestergaard Jensen, Martin Bremholm, Nina Lock, Gulam Roshan Deen, Torben Rene Jensen, Bo B. Iversen, Markus Niederberger, Jan Skov Pedersen, Henrik Birkedal

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  29. Synthesis and characterization of single-crystalline α-MoO3 nanofibers for enhanced Li-ion intercalation applications

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  30. Oxide Nanomaterials: Synthetic Developments, Mechanistic Studies, and Technological Innovations

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  31. Oxidische Nanomaterialien: Von der Synthese über den Mechanismus zur technologischen Innovation

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  32. Time Resolved in Situ XAFS Study of the Electrochemical Oxygen Intercalation in SrFeO2.5 Brownmillerite Structure: Comparison with the Homologous SrCoO2.5 System

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  33. Interplay Between Size and Crystal Structure of Molybdenum Dioxide Nanoparticles—Synthesis, Growth Mechanism, and Electrochemical Performance

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  34. MoO3 nanowires as electrochemical pseudocapacitor materials

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  35. Single-crystalline MoO3 nanoplates: topochemical synthesis and enhanced ethanol-sensing performance

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  36. The interplay of crystallization kinetics and morphology during the formation of SnO2 nanorods: snapshots of the crystallization from fast microwave reactions

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  37. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011

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  38. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

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  39. Synthesis of α-MoO3 Microspheres Assembled by Nanorods in Room Temperature Ionic Liquids

    Advanced materials research · 2011

    Liu Zhi, Yan Song, Li Ping Deng, Xing Hai Liu

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  40. In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts

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  41. Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique

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  42. Probing Liquid/Solid Interfaces at the Molecular Level

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  43. Optimizing the crystal environment through extended x-ray absorption fine structure to increase the luminescent lifetimes of Er3+ doped Y2O3 nanoparticles

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  44. A Modular and Scalable One‐Pot Synthesis of Polysubstituted Furans

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  45. A Modular and Scalable One‐Pot Synthesis of Polysubstituted Furans

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  46. Controlling Nucleation and Crystal Growth of a Distinct Polyoxovanadate Cluster: An In Situ Energy Dispersive X‐ray Diffraction Study under Solvothermal Conditions

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  47. Quantum Mechanics Insight into the Microwave Nucleation of SrTiO3Nanospheres

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  48. DFT+U Study of Properties of MoO3and Hydrogen Adsorption on MoO3(010)

    The Journal of Physical Chemistry C · 2012

    Yanhua Lei, Zhao‐Xu Chen

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  49. A comprehensive study of the crystallization mechanism involved in the nonaqueous formation of tungstite

    Nanoscale · 2013

    Inga Olliges‐Stadler, Marta D. Rossell, Martin Süess, Bettina Ludi, Oliver Bunk, Jan Skov Pedersen, Henrik Birkedal, Markus Niederberger

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  50. In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water

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