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RESEARCH PAPER · Inorganic Chemistry · 2008

Further Examples of the Failure of Surrogates to Properly Model the Structural and Hydrothermal Chemistry of Transuranium Elements: Insights Provided by Uranium and Neptunium Diphosphonates

Anna‐Gay D. Nelson, Travis H. Bray, Wei Zhan, Richard Geoffrey Haire, T.S. Sayler, Thomas E. Albrecht‐Schmitt

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Further Examples of the Failure of Surrogates to Properly Model the Structural and Hydrothermal Chemistry of Transuranium Elements: Insights Provided by Uranium and Neptunium DiphosphonatesOriginalCapitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate40Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate7The actinides1Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems47Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines691D and 3D arrays of isomeric cadmium(II) diphosphonates constructed from N,N-dimethylaminomethane-1,1-diphosphonate ligand5Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds45Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]52Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions29Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Novel double-chained or double-layered metal diphosphonates: synergic coordination effect of two closely linked phosphonate moieties promoted by large metal ionic radius10Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates66USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES24Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium48Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction23Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates54Advances in actinide solid-state and coordination chemistry37Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy109Two new layer structures of zinc(II) or strontium(II) diphosphonates based on N,N-dimethylaminomethane-1,1-diphosphonate ligand4Deviation Between the Chemistry of Ce(IV) and Pu(IV) and Routes to Ordered and Disordered Heterobimetallic 4f/5f and 5f/5f Phosphonates50Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates23Diphosphates and diphosphonates in polyoxometalate chemistry173Mixed-Valent Uranium(IV,VI) Diphosphonate: Synthesis, Structure, and Spectroscopy26Barium uranyl diphosphonates16Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates43From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Uranium diphosphonates templated by interlayer organic amines22From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates28From Yellow to Black: Dramatic Changes between Cerium(IV) and Plutonium(IV) Molybdates37Three New Silver Uranyl Diphosphonates: Structures and Properties23Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Structural chemistry of uranium phosphonates143Structural Variations of the First Family of Heterometallic Uranyl Carboxyphosphinate Assemblies by Synergy between Carboxyphosphinate and Imidazole Ligands21Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions23Electronic Structure and Properties of Berkelium Iodates38Porous Uranium Diphosphonate Frameworks with Trinuclear Units Templated by Organic Ammonium Hydrolyzed from Amine Solvents23Electrochemical, spectroscopic and theoretical studies on redox speciation of neptunium with phenylphosphonic acid7New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid1Actinides12The presence of mixed-valent silver in the uranyl phenylenediphosphonate framework5Uranyl Phosphonates with Multiple Uranyl Coordination Geometries and Low Temperature Phase Transition14Synthesis, Characterization, and Solid-State Structural Chemistry of Uranium(IV) Aliphatic Dicarboxylates7The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds41An updated status and trends in actinide metal-organic frameworks (An-MOFs): From synthesis to application145Understanding The Structural Chemistry of Actinide Phosphonates0Actinium chelation and crystallization in a macromolecular scaffold12Layered metal phosphonates: Structures and properties7Syntheses and characterization of non-molecular phenyl- and methyl-phosphonates and ethylenediphosphonates of thorium and cerium1

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  1. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie International Edition · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

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  2. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

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  3. The actinides

    Annual Reports Section A (Inorganic Chemistry) · 2009-01-01

    S. A. Cotton

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  4. Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems

    Inorganic Chemistry · 2009-04-06

    Anna‐Gay D. Nelson, Travis H. Bray, Forrest A. Stanley, Thomas E. Albrecht‐Schmitt

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  5. Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines

    Inorganic Chemistry · 2009-06-22

    Karah E. Knope, Christopher L. Cahill

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  6. 1D and 3D arrays of isomeric cadmium(II) diphosphonates constructed from N,N-dimethylaminomethane-1,1-diphosphonate ligand

    Inorganic Chemistry Communications · 2009-10-31

    Zi‐Yi Du, Yu-Hui Sun, Yong‐Rong Xie, Jing Lin, He‐Rui Wen

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  7. Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds

    Inorganic Chemistry · 2009-11-02

    A.N. Alsobrook, Thomas E. Albrecht‐Schmitt

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  8. Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]

    Chemical Communications · 2010-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  9. Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions

    Dalton Transactions · 2010-01-01

    Karah E. Knope, Christopher L. Cahill

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  10. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

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  11. Novel double-chained or double-layered metal diphosphonates: synergic coordination effect of two closely linked phosphonate moieties promoted by large metal ionic radius

    CrystEngComm · 2010-01-01

    Zi‐Yi Du, Yu-Hui Sun, Xiuzhi Zhang, Shu-Fen Luo, Yong‐Rong Xie, Dong‐Bei Wan

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  12. Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates

    European Journal of Inorganic Chemistry · 2010-01-29

    Karah E. Knope, Christopher L. Cahill

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  13. USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES

    Comments on Inorganic Chemistry · 2010-03-30

    Juan Diwu, Anna‐Gay D. Nelson, Thomas E. Albrecht‐Schmitt

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  14. Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium

    Inorganic Chemistry · 2010-07-27

    Padmini Ramaswamy, Ramanath Prabhu, Srinivasan Natarajan

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  15. Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction

    CrystEngComm · 2010-09-06

    Karah E. Knope, Christopher L. Cahill

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  16. Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates

    Inorganic Chemistry · 2010-10-04

    Juan Diwu, Shuao Wang, Zuolei Liao, Peter Carman Burns, Thomas E. Albrecht‐Schmitt

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  17. Advances in actinide solid-state and coordination chemistry

    MRS Bulletin · 2010-11-01

    Peter Carman Burns, Yasuhisa Ikeda, Ken Czerwinski

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  18. Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy

    Dalton Transactions · 2011-01-01

    Michael P. Redmond, S.M. Cornet, Sean D. Woodall, Daniel M. Whittaker, David Collison, M. Helliwell, Louise S. Natrajan

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  19. Two new layer structures of zinc(II) or strontium(II) diphosphonates based on N,N-dimethylaminomethane-1,1-diphosphonate ligand

    Journal of Molecular Structure · 2011-03-13

    Yu-Hui Sun, Zi‐Yi Du, Zhonggao Zhou, Shi‐Yong Zhang, Guohai Xu, Yong‐Rong Xie

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  20. Deviation Between the Chemistry of Ce(IV) and Pu(IV) and Routes to Ordered and Disordered Heterobimetallic 4f/5f and 5f/5f Phosphonates

    Inorganic Chemistry · 2011-04-25

    Juan Diwu, Shuao Wang, Justin J. Good, V.H. DiStefano, Thomas E. Albrecht‐Schmitt

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  21. Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates

    European Journal of Inorganic Chemistry · 2011-08-05

    Eric M. Villa, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  22. Diphosphates and diphosphonates in polyoxometalate chemistry

    Chemical Society Reviews · 2012-01-01

    Abhishek Banerjee, Bassem S. Bassil, Gerd‐Volker Röschenthaler, Ulrich Kortz

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  23. Mixed-Valent Uranium(IV,VI) Diphosphonate: Synthesis, Structure, and Spectroscopy

    Inorganic Chemistry · 2012-03-29

    Juan Diwu, Thomas E. Albrecht‐Schmitt

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  24. Barium uranyl diphosphonates

    Journal of Solid State Chemistry · 2012-04-06

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Rodney Charles Ewing, Thomas E. Albrecht‐Schmitt

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  25. Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates

    Inorganic Chemistry · 2012-05-30

    Eric M. Villa, Connor J. Marr, Laurent J. Jouffret, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  26. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

    Inorganic Chemistry · 2012-10-24

    Weiting Yang, Hongyue Wu, Run-Xue Wang, Qing‐Jiang Pan, Zhong‐Ming Sun, Hongjie Zhang

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  27. Uranium diphosphonates templated by interlayer organic amines

    Journal of Solid State Chemistry · 2012-10-24

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Thomas E. Albrecht‐Schmitt, Rodney Charles Ewing

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  28. From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates

    Inorganic Chemistry · 2013-01-09

    Eric M. Villa, Connor J. Marr, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  29. From Yellow to Black: Dramatic Changes between Cerium(IV) and Plutonium(IV) Molybdates

    Journal of the American Chemical Society · 2013-01-29

    Justin N. Cross, Patrick M. Duncan, Eric M. Villa, Matthew J. Polinski, Jean‐Marie Babo, Evgeny V. Alekseev, Corwin H. Booth, Thomas E. Albrecht‐Schmitt

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  30. Three New Silver Uranyl Diphosphonates: Structures and Properties

    Inorganic Chemistry · 2014-02-13

    Anna‐Gay D. Nelson, Zsolt Rak, Thomas E. Albrecht‐Schmitt, Udo Becker, Rodney Charles Ewing

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  31. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

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  32. Hybrid Materials of the f-Elements Part I

    Elsevier eBooks · 2015-01-01

    Korey Prescott Carter, Christopher L. Cahill

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  33. Hybrid Materials of the f-Elements Part II

    Elsevier eBooks · 2015-01-01

    Robert G. Surbella, Christopher L. Cahill

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  34. Structural chemistry of uranium phosphonates

    Coordination Chemistry Reviews · 2015-05-30

    Weiting Yang, T. Gannon Parker, Zhong‐Ming Sun

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  35. Structural Variations of the First Family of Heterometallic Uranyl Carboxyphosphinate Assemblies by Synergy between Carboxyphosphinate and Imidazole Ligands

    Crystal Growth & Design · 2016-03-03

    Weiting Yang, Dai Wu, Chao Liu, Qing‐Jiang Pan, Zhong‐Ming Sun

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  36. Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions

    Inorganic Chemistry · 2017-05-26

    Lanhua Chen, Juan Diwu, Daxiang Gui, Yaxing Wang, Zhehui Weng, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  37. Electronic Structure and Properties of Berkelium Iodates

    Journal of the American Chemical Society · 2017-08-17

    Mark A. Silver, Samantha K. Cary, Alejandro J. Garza, Ryan Baumbach, Alexandra A. Arico, Gregory A. Galmin, Kuan-Wen Chen, Jason A. Johnson, Jamie C. Wang, Ronald Jene Clark, Alexander T. Chemey, Teresa M. Eaton, Matthew L. Marsh, Kevin Seidler, Shane S. Galley, Lambertus J. van de Burgt, Ashley L. Gray, David E. Hobart, Kenneth Hanson, Shelley M. Van Cleve, Frédéric Gendron, Jochen Autschbach, Gustavo E. Scuseria, Laurent Maron, Manfred Speldrich, Paul Kögerler, Cristian Celis‐Barros, Dayán Páez‐Hernández, Ramiro Arratia‐Pérez, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  38. Porous Uranium Diphosphonate Frameworks with Trinuclear Units Templated by Organic Ammonium Hydrolyzed from Amine Solvents

    Inorganic Chemistry · 2017-10-17

    Zhi‐Hui Zhang, Ganna A. Senchyk, Yi Liu, Tyler L. Spano, Jennifer E. S. Szymanowski, Peter Carman Burns

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  39. Electrochemical, spectroscopic and theoretical studies on redox speciation of neptunium with phenylphosphonic acid

    Inorganica Chimica Acta · 2018-06-20

    Ashutosh Srivastava, Rama Mohana Rao Dumpala, Neetika Rawat, Bhupendra Singh Tomar

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  40. New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid

    Minerals · 2018-11-01

    Eric M. Villa, Justin N. Cross, Thomas E. Albrecht‐Schmitt

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  41. Actinides

    Elsevier eBooks · 2019-12-02

    Sascha T. Löffler, Karsten Meyer

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  42. The presence of mixed-valent silver in the uranyl phenylenediphosphonate framework

    New Journal of Chemistry · 2020-01-01

    Ru Bai, Lanhua Chen, Yugang Zhang, Long Chen, Juan Diwu, Xiao‐Feng Wang

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  43. Uranyl Phosphonates with Multiple Uranyl Coordination Geometries and Low Temperature Phase Transition

    Chinese Journal of Chemistry · 2020-10-16

    Lanhua Chen, Yugang Zhang, Zhehui Weng, Zhiyong Liu, Jiarong Zhang, Yaxing Wang, Shuao Wang

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  44. Synthesis, Characterization, and Solid-State Structural Chemistry of Uranium(IV) Aliphatic Dicarboxylates

    Crystal Growth & Design · 2021-03-15

    Aphra V. Murray, Jennifer N. Wacker, Jeffery A. Bertke, Karah E. Knope

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  45. The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds

    Coordination Chemistry Reviews · 2021-06-05

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  46. An updated status and trends in actinide metal-organic frameworks (An-MOFs): From synthesis to application

    Coordination Chemistry Reviews · 2021-07-07

    Kai Lv, Sebastian Fichter, Mei Gu, Juliane März, Moritz Schmidt

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  47. Understanding The Structural Chemistry of Actinide Phosphonates

    Figshare · 2022-09-15

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  48. Actinium chelation and crystallization in a macromolecular scaffold

    Nature Communications · 2024-07-15

    Jennifer N. Wacker, Joshua J. Woods, Peter B. Rupert, Appie A. Peterson, Marc Allaire, Wayne W. Lukens, Alyssa Gaiser, Stefan G. Minasian, Roland K. Strong, Rebecca J. Abergel

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  49. Layered metal phosphonates: Structures and properties

    Coordination Chemistry Reviews · 2025-03-15

    Jia‐Ge Jia, Song‐Song Bao, George K. H. Shimizu, Li‐Min Zheng

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  50. Syntheses and characterization of non-molecular phenyl- and methyl-phosphonates and ethylenediphosphonates of thorium and cerium

    Dalton Transactions · 2026-01-01

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