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RESEARCH PAPER · Inorganic Chemistry · 2012

Mixed-Valent Uranium(IV,VI) Diphosphonate: Synthesis, Structure, and Spectroscopy

Juan Diwu, Thomas E. Albrecht‐Schmitt

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Mixed-Valent Uranium(IV,VI) Diphosphonate: Synthesis, Structure, and SpectroscopyOriginalDiphosphates and diphosphonates in polyoxometalate chemistry173The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding40From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Crystal Growth, Structural Characterization, and Magnetic Properties of New Uranium(IV) Containing Mixed Metal Oxalates: Na2U2M(C2O4)6(H2O)4 (M = Mn2+, Fe2+, Co2+, and Zn2+)33Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels33Mixed Formate-Dicarboxylate Coordination Polymers with Tetravalent Uranium: Occurrence of Tetranuclear {U4O4} and Hexanuclear {U6O4(OH)4} Motifs66U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient In Situ Route That Creates U4+ under Mild Hydrothermal Conditions38B-α-[AsW 9 O 33 ] 9− polyoxometalates incorporating hexanuclear uranium {U 6 O 8 }-like clusters bearing the U IV form or unprecedented mixed valence U IV /U VI involving direct U VI O–U IV bonding27Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Structural chemistry of uranium phosphonates143A Mixed‐Valent Uranium Phosphonate Framework Containing UIV, UV, and UVI39Benchmarking Uranyl Peroxide Capsule Chemistry in Organic Media20U(IV) Aqueous Speciation from the Monomer to UO2 Nanoparticles: Two Levels of Control from Zwitterionic Glycine Ligands51Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions23A first principles study of energetics and electronic structural responses of uranium-based coordination polymers to Np incorporation5Uranium(IV) Chloride Complexes: UCl62– and an Unprecedented U(H2O)4Cl4 Structural Unit26Porous Uranium Diphosphonate Frameworks with Trinuclear Units Templated by Organic Ammonium Hydrolyzed from Amine Solvents23An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation11Solution and Solid State Structural Chemistry of Th(IV) and U(IV) 4-Hydroxybenzoates42Time-controlled synthesis of the 3D coordination polymer U(1,2,3-Hbtc) 2 followed by the formation of molecular poly-oxo cluster {U 14 } containing hemimellitate uranium( iv )14Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster64Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster4Pyridine Diphosphonate Ligand for Stabilization of Tetravalent Uranium and Neptunium in Aqueous Medium under Aerobic Conditions2Alkali Counterion-Dependent Crystallization of Uranium(IV)–Chloro Structural Units6Porous and functional metal phosphonate frameworks0

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  1. Diphosphates and diphosphonates in polyoxometalate chemistry

    Chemical Society Reviews · 2012-01-01

    Abhishek Banerjee, Bassem S. Bassil, Gerd‐Volker Röschenthaler, Ulrich Kortz

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  2. The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding

    Inorganic Chemistry · 2012-09-28

    Tao Tian, Weiting Yang, Qing‐Jiang Pan, Zhong‐Ming Sun

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  3. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

    Inorganic Chemistry · 2012-10-24

    Weiting Yang, Hongyue Wu, Run-Xue Wang, Qing‐Jiang Pan, Zhong‐Ming Sun, Hongjie Zhang

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  4. Crystal Growth, Structural Characterization, and Magnetic Properties of New Uranium(IV) Containing Mixed Metal Oxalates: Na2U2M(C2O4)6(H2O)4 (M = Mn2+, Fe2+, Co2+, and Zn2+)

    Inorganic Chemistry · 2013-02-01

    Jeongho Yeon, Mark D. Smith, Athena S. Sefat, Hans‐Conrad zur Loye

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  5. Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels

    Inorganic Chemistry · 2013-05-23

    Tao Tian, Weiting Yang, Hao Wang, Song Dang, Qing‐Jiang Pan, Zhong‐Ming Sun

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  6. Mixed Formate-Dicarboxylate Coordination Polymers with Tetravalent Uranium: Occurrence of Tetranuclear {U4O4} and Hexanuclear {U6O4(OH)4} Motifs

    Crystal Growth & Design · 2013-06-19

    Clément Falaise, Christophe Volkringer, Thierry Loiseau

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  7. U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient In Situ Route That Creates U4+ under Mild Hydrothermal Conditions

    Inorganic Chemistry · 2013-07-08

    Jeongho Yeon, Mark D. Smith, Athena S. Sefat, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  8. B-α-[AsW 9 O 33 ] 9− polyoxometalates incorporating hexanuclear uranium {U 6 O 8 }-like clusters bearing the U IV form or unprecedented mixed valence U IV /U VI involving direct U VI O–U IV bonding

    Dalton Transactions · 2015-01-01

    Sylvain Duval, Sophie Sobanska, Pascal Roussel, Thierry Loiseau

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  9. Hybrid Materials of the f-Elements Part I

    Elsevier eBooks · 2015-01-01

    Korey Prescott Carter, Christopher L. Cahill

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  10. Hybrid Materials of the f-Elements Part II

    Elsevier eBooks · 2015-01-01

    Robert G. Surbella, Christopher L. Cahill

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  11. Structural chemistry of uranium phosphonates

    Coordination Chemistry Reviews · 2015-05-30

    Weiting Yang, T. Gannon Parker, Zhong‐Ming Sun

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  12. A Mixed‐Valent Uranium Phosphonate Framework Containing UIV, UV, and UVI

    Chemistry - A European Journal · 2016-06-29

    Lanhua Chen, Tao Zheng, Song‐Song Bao, Linjuan Zhang, Hsin‐Kuan Liu, Li‐Min Zheng, Jian‐Qiang Wang, Yaxing Wang, Juan Diwu, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  13. Benchmarking Uranyl Peroxide Capsule Chemistry in Organic Media

    European Journal of Inorganic Chemistry · 2016-11-04

    Harrison A. Neal, Jennifer E. S. Szymanowski, Jeremy B. Fein, Peter Carman Burns, May Nyman

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  14. U(IV) Aqueous Speciation from the Monomer to UO2 Nanoparticles: Two Levels of Control from Zwitterionic Glycine Ligands

    Inorganic Chemistry · 2017-05-16

    Clément Falaise, Harrison A. Neal, May Nyman

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  15. Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions

    Inorganic Chemistry · 2017-05-26

    Lanhua Chen, Juan Diwu, Daxiang Gui, Yaxing Wang, Zhehui Weng, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  16. A first principles study of energetics and electronic structural responses of uranium-based coordination polymers to Np incorporation

    Radiochimica Acta · 2017-06-29

    Saumitra Saha, Udo Becker

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  17. Uranium(IV) Chloride Complexes: UCl62– and an Unprecedented U(H2O)4Cl4 Structural Unit

    Inorganic Chemistry · 2017-07-31

    Jennifer N. Wacker, Monica Vasiliu, Kevin Huang, Ryan Baumbach, Jeffery A. Bertke, David A. Dixon, Karah E. Knope

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  18. Porous Uranium Diphosphonate Frameworks with Trinuclear Units Templated by Organic Ammonium Hydrolyzed from Amine Solvents

    Inorganic Chemistry · 2017-10-17

    Zhi‐Hui Zhang, Ganna A. Senchyk, Yi Liu, Tyler L. Spano, Jennifer E. S. Szymanowski, Peter Carman Burns

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  19. An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation

    Inorganic Chemistry · 2018-01-10

    Daxiang Gui, Xing Dai, Tao Zheng, Xiangxiang Wang, Mark A. Silver, Lanhua Chen, Chao Zhang, Juan Diwu, Ruhong Zhou, Zhifang Chai, Shuao Wang

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  20. Solution and Solid State Structural Chemistry of Th(IV) and U(IV) 4-Hydroxybenzoates

    Inorganic Chemistry · 2018-06-07

    Nicole A. Vanagas, Jennifer N. Wacker, Christopher L. Rom, Elliot N. Glass, Ian Colliard, Yusen Qiao, Jeffery A. Bertke, Edward Van Keuren, Eric J. Schelter, May Nyman, Karah E. Knope

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  21. Time-controlled synthesis of the 3D coordination polymer U(1,2,3-Hbtc) 2 followed by the formation of molecular poly-oxo cluster {U 14 } containing hemimellitate uranium( iv )

    RSC Advances · 2019-01-01

    Maxime Dufaye, Nicolas P. Martin, Sylvain Duval, Christophe Volkringer, Atsushi Ikeda‐Ohno, Thierry Loiseau

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  22. Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster

    Angewandte Chemie International Edition · 2021-02-17

    Mingxing Zhang, Chengyu Liang, Guo‐Dong Cheng, Junchang Chen, Yumin Wang, Yumin Wang, Linwei He, Liwei Cheng, Shicheng Gong, Duo Zhang, Jiong Li, Shu‐Xian Hu, Juan Diwu, Guozhong Wu, Yaxing Wang, Yaxing Wang, Zhifang Chai, Shuao Wang

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  23. Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster

    Angewandte Chemie · 2021-02-17

    Mingxing Zhang, Chengyu Liang, Guo‐Dong Cheng, Junchang Chen, Yumin Wang, Yumin Wang, Linwei He, Liwei Cheng, Shicheng Gong, Duo Zhang, Jiong Li, Shu‐Xian Hu, Juan Diwu, Guozhong Wu, Yaxing Wang, Yaxing Wang, Zhifang Chai, Shuao Wang

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  24. Pyridine Diphosphonate Ligand for Stabilization of Tetravalent Uranium and Neptunium in Aqueous Medium under Aerobic Conditions

    Inorganic Chemistry · 2024-02-06

    Parveen Kumar Verma, Bholanath Mahanty, Arunasis Bhattacharyya, Petr Igorevich Matveev, Nataliya E. Borisova, Stepan Nikolaevich Kalmykov, Prasanta K. Mohapatra

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  25. Alkali Counterion-Dependent Crystallization of Uranium(IV)–Chloro Structural Units

    Inorganic Chemistry · 2025-06-12

    Madeline C. Shore, Jennifer N. Wacker, Pere Miró, Jeffery A. Bertke, Karah E. Knope

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  26. Porous and functional metal phosphonate frameworks

    Elsevier eBooks · 2025-11-29

    Tao Zheng, Yuhao Lei, Juwei Du

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