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RESEARCH PAPER · Inorganic Chemistry · 2012

Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates

Eric M. Villa, Connor J. Marr, Laurent J. Jouffret, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) PhosphatesOriginalSyntheses, Structures, and Spectroscopic Properties of Plutonium and Americium Phosphites and the Redetermination of the Ionic Radii of Pu(III) and Am(III)89ChemInform Abstract: Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates.0Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing Belts of Polyhedra35Structural changes within the alkaline earth uranyl phosphites9From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates28Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate22High temperature redox reactions with uranium: Synthesis and characterization of Cs(UO2)Cl(SeO3), Rb2(UO2)3O2(SeO3)2, and RbNa5U2(SO4)77Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids70High-Temperature, High-Pressure Hydrothermal Synthesis, Crystal Structures, and Spectroscopic Studies of a Uranium(IV) Phosphate (Na10U2P6O24) and the Isotypic Cerium(IV) Phosphate (Na10Ce2P6O24)27MOFs of Uranium and the Actinides95Topologically identical, but geometrically isomeric layers in hydrous α-, β-Rb[UO2(AsO3OH)(AsO2(OH)2)]·H2O and anhydrous Rb[UO2(AsO3OH)(AsO2(OH)2)]6Solid-state actinide acid phosphites from phosphorous acid melts3Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Th(AsIII4AsV4O18): a Mixed-Valent Oxoarsenic(III)/arsenic(V) Actinide Compound Obtained under Extreme Conditions17Morphotropy and Temperature-Driven Polymorphism in A2Th(AsO4)2 (A = Li, Na, K, Rb, Cs) Series19Influence of extreme conditions on the formation and structures of caesium uranium( vi ) arsenates10Preparation and crystal structure of K 2 Ce(PO 4 ) 2 : a new complex phosphate of Ce( iv ) having structure with one-dimensional channels28A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172A Cubic Non-Centrosymmetric Mixed-Valence Iron Borophosphate–Phosphite6Temperature dependent structural, vibrational and magnetic properties of K 3 Gd 5 (PO 4 ) 621Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions23Synthesis and crystal structure of cerium(IV) bis(phosphite)0An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation11A Large Family of Centrosymmetric and Chiral f-Element-Bearing Iodate Selenates Exhibiting Coordination Number and Dimensional Reductions26A Family of Layered Phosphates Crystallizing in a Rare Geometrical Isomer of the Phosphuranylite Topology: Synthesis, Characterization, and Computational Modeling of A4[(UO2)3O2(PO4)2] (A = Alkali Metal) Exhibiting Intralayer Ion Exchange21Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)25pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites7Thermodynamic investigations on K3Ln5(PO4)6 (Ln = Eu and Gd) compounds2New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid1Understanding the Polymorphism of A4[(UO2)3(PO4)2O2] (A = Alkali Metals) Uranyl Phosphate Framework Structures10Crystal Growth and Structure Characterization of Three Layered Uranyl Phosphates and Their Relation to the Phosphuranylite Family13Expansion of the structural diversity of f-element bearing molybdate iodates: synthesis, structures, and optical properties19Structural and Spectroscopic Investigation of Novel 2D and 3D Uranium Oxo-Silicates/Germanates and Some Statistical Aspects of Uranyl Coordination in Oxo-Salts14An experimental calorimetric and a DFT + U study of the thermodynamic properties of Cs 4 UO 2 4 WO 5 W 2 O 8 O 2 and Cs 4 [ UO 2 7 WO 5 3 O 3 ]4The role of 1-ethyl-3-methylimidazolium diethyl phosphate ionic liquid in uranyl phosphate compounds7Ligand‐Supported Facile Conversion of Uranyl(VI) into Uranium(IV) in Organic and Aqueous Media29Ligand‐Supported Facile Conversion of Uranyl(VI) into Uranium(IV) in Organic and Aqueous Media10Redox mechanism and stability of uranyl phosphites at mineral surfaces: Cooperative proton/electron transfer and high efficacy for Uranium(VI) reduction12Organophosphorus-Modified Lanthanide Nitrates as Potential Actinide Oxide Aerosol Surrogates6Stabilizing lanthanide periodate compounds by slowing periodate reduction at elevated temperatures with NaBiO3, a sacrificial oxidant0Periodic trends in trivalent actinide halides, phosphates, and arsenates5Equations of State and Crystal Structures of KCaPO4, KSrPO4, and K2Ce(PO4)2 under High Pressure: Discovery of a New Polymorph of KCaPO44Uranyl-Tc( vii )/Tc( v ) hybrid clusters5

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  1. Syntheses, Structures, and Spectroscopic Properties of Plutonium and Americium Phosphites and the Redetermination of the Ionic Radii of Pu(III) and Am(III)

    Inorganic Chemistry · 2012-07-17

    Justin N. Cross, Eric M. Villa, Shuao Wang, Juan Diwu, Matthew J. Polinski, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  2. ChemInform Abstract: Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates.

    ChemInform · 2012-08-16

    Eric M. Villa, Connor J. Marr, Laurent J. Jouffret, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  3. Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing Belts of Polyhedra

    Inorganic Chemistry · 2012-12-11

    Jie Qiu, Kévin Nguyen, Laurent J. Jouffret, Jennifer E. S. Szymanowski, Peter Carman Burns

    Read original paper ↗ ·

  4. Structural changes within the alkaline earth uranyl phosphites

    Dalton Transactions · 2013-01-01

    Eric M. Villa, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  5. From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates

    Inorganic Chemistry · 2013-01-09

    Eric M. Villa, Connor J. Marr, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  6. Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate

    Crystal Growth & Design · 2013-03-08

    Eric M. Villa, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  7. High temperature redox reactions with uranium: Synthesis and characterization of Cs(UO2)Cl(SeO3), Rb2(UO2)3O2(SeO3)2, and RbNa5U2(SO4)7

    Journal of Solid State Chemistry · 2013-08-13

    Jean‐Marie Babo, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  8. Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids

    Inorganic Chemistry · 2013-10-16

    Weiting Yang, Song Dang, Hao Wang, Tao Tian, Qing‐Jiang Pan, Zhong‐Ming Sun

    Read original paper ↗ ·

  9. High-Temperature, High-Pressure Hydrothermal Synthesis, Crystal Structures, and Spectroscopic Studies of a Uranium(IV) Phosphate (Na10U2P6O24) and the Isotypic Cerium(IV) Phosphate (Na10Ce2P6O24)

    Inorganic Chemistry · 2013-11-13

    Yu‐Hsien Lai, Yu‐Chih Chang, Tsz-Fung Wong, Wan‐Ju Tai, Wen‐Jung Chang, Kwang‐Hwa Lii

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  10. MOFs of Uranium and the Actinides

    Structure and bonding · 2014-01-01

    Juan Su, Jiesheng Chen

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  11. Topologically identical, but geometrically isomeric layers in hydrous α-, β-Rb[UO2(AsO3OH)(AsO2(OH)2)]·H2O and anhydrous Rb[UO2(AsO3OH)(AsO2(OH)2)]

    Journal of Solid State Chemistry · 2014-03-22

    Na Yu, Vladislav V. Klepov, Eric M. Villa, Dirk Bosbach, Evgeny V. Suleimanov, Wulf Depmeier, Thomas E. Albrecht‐Schmitt, Evgeny V. Alekseev

    Read original paper ↗ ·

  12. Solid-state actinide acid phosphites from phosphorous acid melts

    Journal of Solid State Chemistry · 2014-03-23

    George N. Oh, Peter Carman Burns

    Read original paper ↗ ·

  13. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  14. Th(AsIII4AsV4O18): a Mixed-Valent Oxoarsenic(III)/arsenic(V) Actinide Compound Obtained under Extreme Conditions

    Inorganic Chemistry · 2014-07-30

    Na Yu, Vladislav V. Klepov, Philip Kegler, Dirk Bosbach, Thomas E. Albrecht‐Schmitt, Evgeny V. Alekseev

    Read original paper ↗ ·

  15. Morphotropy and Temperature-Driven Polymorphism in A2Th(AsO4)2 (A = Li, Na, K, Rb, Cs) Series

    Inorganic Chemistry · 2014-10-02

    Na Yu, Vladislav V. Klepov, Giuseppe Modolo, Dirk Bosbach, Evgeny V. Suleimanov, Thorsten M. Gesing, Lars Robben, Evgeny V. Alekseev

    Read original paper ↗ ·

  16. Influence of extreme conditions on the formation and structures of caesium uranium( vi ) arsenates

    Dalton Transactions · 2015-01-01

    Na Yu, Philip Kegler, Vladislav V. Klepov, Jakob Dellen, Hartmut Schlenz, Eike M. Langer, Dirk Bosbach, Evgeny V. Alekseev

    Read original paper ↗ ·

  17. Preparation and crystal structure of K 2 Ce(PO 4 ) 2 : a new complex phosphate of Ce( iv ) having structure with one-dimensional channels

    Dalton Transactions · 2015-11-18

    Samatha Bevara, Srungarpu Nagabhusan Achary, S.J. Patwe, Anil Kumar Sinha, A. K. Tyagi

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  18. A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds

    The Canadian Mineralogist · 2016-01-01

    Aaron J. Lussier, Rachel A. K. Lopez, Peter Carman Burns

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  19. A Cubic Non-Centrosymmetric Mixed-Valence Iron Borophosphate–Phosphite

    Crystal Growth & Design · 2016-01-25

    Hooman Yaghoobnejad Asl, Ronetta Morris, T. Thao Tran, P. Shiv Halasyamani, K. Ghosh, Amitava Choudhury

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  20. Temperature dependent structural, vibrational and magnetic properties of K 3 Gd 5 (PO 4 ) 6

    Physical Chemistry Chemical Physics · 2017-01-01

    Samatha Bevara, Srungarpu Nagabhusan Achary, K. K. Mishra, T. R. Ravindran, Anil Kumar Sinha, Pulya Umamaheswara Sastry, A. K. Tyagi

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  21. Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions

    Inorganic Chemistry · 2017-05-26

    Lanhua Chen, Juan Diwu, Daxiang Gui, Yaxing Wang, Zhehui Weng, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

    Read original paper ↗ ·

  22. Synthesis and crystal structure of cerium(IV) bis(phosphite)

    Acta Crystallographica Section E Crystallographic Communications · 2017-08-04

    Stefano H. Byer, Eric M. Villa

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  23. An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation

    Inorganic Chemistry · 2018-01-10

    Daxiang Gui, Xing Dai, Tao Zheng, Xiangxiang Wang, Mark A. Silver, Lanhua Chen, Chao Zhang, Juan Diwu, Ruhong Zhou, Zhifang Chai, Shuao Wang

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  24. A Large Family of Centrosymmetric and Chiral f-Element-Bearing Iodate Selenates Exhibiting Coordination Number and Dimensional Reductions

    Inorganic Chemistry · 2018-01-18

    Meiying Qie, Jian Hung Lin, Fang Kong, Mark A. Silver, Zenghui Yue, Xiaomei Wang, Linjuan Zhang, Hongliang Bao, Thomas E. Albrecht‐Schmitt, Jian‐Qiang Wang

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  25. A Family of Layered Phosphates Crystallizing in a Rare Geometrical Isomer of the Phosphuranylite Topology: Synthesis, Characterization, and Computational Modeling of A4[(UO2)3O2(PO4)2] (A = Alkali Metal) Exhibiting Intralayer Ion Exchange

    Inorganic Chemistry · 2018-04-02

    Christian A. Juillerat, Emily E. Moore, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  26. Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)2

    Inorganic Chemistry · 2018-07-31

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

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  27. pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites

    Crystal Growth & Design · 2018-08-03

    Jakob T. Dovgan, Matthew J. Polinski, Brandon Q. Mercado, Eric M. Villa

    Read original paper ↗ ·

  28. Thermodynamic investigations on K3Ln5(PO4)6 (Ln = Eu and Gd) compounds

    Journal of Alloys and Compounds · 2018-09-04

    Rimpi Dawar, Samatha Bevara, Srungarpu Nagabhusan Achary, P. D. Babu, R.K. Mishra, A. K. Tyagi

    Read original paper ↗ ·

  29. New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid

    Minerals · 2018-11-01

    Eric M. Villa, Justin N. Cross, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  30. Understanding the Polymorphism of A4[(UO2)3(PO4)2O2] (A = Alkali Metals) Uranyl Phosphate Framework Structures

    Crystal Growth & Design · 2018-12-13

    Vancho Kocevski, Christian A. Juillerat, Emily E. Moore, Hans‐Conrad zur Loye, Theodore M. Besmann

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  31. Crystal Growth and Structure Characterization of Three Layered Uranyl Phosphates and Their Relation to the Phosphuranylite Family

    Crystal Growth & Design · 2018-12-18

    Christian A. Juillerat, Hans‐Conrad zur Loye

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  32. Expansion of the structural diversity of f-element bearing molybdate iodates: synthesis, structures, and optical properties

    Dalton Transactions · 2019-01-01

    Jian Hung Lin, Qi Liu, Zenghui Yue, Kariem Diefenbach, Liwei Cheng, Yue‐Jian Lin, Jian‐Qiang Wang

    Read original paper ↗ ·

  33. Structural and Spectroscopic Investigation of Novel 2D and 3D Uranium Oxo-Silicates/Germanates and Some Statistical Aspects of Uranyl Coordination in Oxo-Salts

    Inorganic Chemistry · 2019-07-16

    Haijian Li, Eike M. Langer, Philip Kegler, Evgeny V. Alekseev

    Read original paper ↗ ·

  34. An experimental calorimetric and a DFT + U study of the thermodynamic properties of Cs 4 UO 2 4 WO 5 W 2 O 8 O 2 and Cs 4 [ UO 2 7 WO 5 3 O 3 ]

    The Journal of Chemical Thermodynamics · 2019-07-24

    Maxim I. Lelet, Maria L. Yakun’kova, Piotr M. Kowalski, Evgeny V. Suleimanov, Charles A. Geiger, Evgeny V. Alekseev

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  35. The role of 1-ethyl-3-methylimidazolium diethyl phosphate ionic liquid in uranyl phosphate compounds

    Journal of Solid State Chemistry · 2019-09-06

    Tsuyoshi A. Kohlgruber, Stephanie A. Mackley, Fabrice Dal Bo, Sergey M. Aksenov, Peter Carman Burns

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  36. Ligand‐Supported Facile Conversion of Uranyl(VI) into Uranium(IV) in Organic and Aqueous Media

    Angewandte Chemie International Edition · 2020-02-04

    Radmila Faizova, Farzaneh Fadaei‐Tirani, Rizlan Bernier‐Latmani, Marinella Mazzanti

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  37. Ligand‐Supported Facile Conversion of Uranyl(VI) into Uranium(IV) in Organic and Aqueous Media

    Angewandte Chemie · 2020-02-04

    Radmila Faizova, Farzaneh Fadaei‐Tirani, Rizlan Bernier‐Latmani, Marinella Mazzanti

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  38. Redox mechanism and stability of uranyl phosphites at mineral surfaces: Cooperative proton/electron transfer and high efficacy for Uranium(VI) reduction

    Chemosphere · 2020-04-30

    Qian Wang, Tingting Li, Xiaoxiao Huang, Gang Yang

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  39. Organophosphorus-Modified Lanthanide Nitrates as Potential Actinide Oxide Aerosol Surrogates

    Inorganic Chemistry · 2020-11-24

    Timothy J. Boyle, Xavier J. Robinson, Fernando Guerrero, Diana Perales, Joshua A. Hubbard, Roger E. Cramer

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  40. Stabilizing lanthanide periodate compounds by slowing periodate reduction at elevated temperatures with NaBiO3, a sacrificial oxidant

    Polyhedron · 2021-04-18

    Colin N. Reedy, Eric M. Villa

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  41. Periodic trends in trivalent actinide halides, phosphates, and arsenates

    Dalton Transactions · 2023-01-01

    Ashutosh Parimi, Emmalee Mosher, Georg Schreckenbach

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  42. Equations of State and Crystal Structures of KCaPO4, KSrPO4, and K2Ce(PO4)2 under High Pressure: Discovery of a New Polymorph of KCaPO4

    Crystal Growth & Design · 2023-02-28

    Daniel Errandonea, Srungarpu Nagabhusan Achary, Daniel Díaz-Anichtchenko, Enrico Bandiello, Tomás Marqueño, Rakesh Shukla, A. K. Tyagi, Cătălin Popescu, Frederico Alabarse

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  43. Uranyl-Tc( vii )/Tc( v ) hybrid clusters

    Chemical Communications · 2024-01-01

    Mohammad Shohel, May Nyman

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