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RESEARCH PAPER · Journal of the American Chemical Society · 2022

Chemical Recycling of Polyethylene by Tandem Catalytic Conversion to Propylene

Nicholas M. Wang, Garrett Strong, Vanessa DaSilva, Lijun Gao, Rafael Huacuja, Ivan A. Konstantinov, Mari S. Rosen, Alex J. Nett, Sean W. Ewart, Roland Geyer, Susannah L. Scott, Damien Guironnet

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Chemical Recycling of Polyethylene by Tandem Catalytic Conversion to PropyleneOriginalMicroplastic materials in the environment: Problem and strategical solutions201Understanding the Structure–Activity Relationships in Catalytic Conversion of Polyolefin Plastics by Zeolite-Based Catalysts: A Critical Review269Towards a Cradle‐to‐Cradle Polyolefin Lifecycle11Towards a Cradle‐to‐Cradle Polyolefin Lifecycle1Catalytic Chemical Recycling of Post-Consumer Polyethylene188Atomically inner tandem catalysts for electrochemical reduction of carbon dioxide30Bis(pentafluorophenyl)borane-catalyzed E -selective isomerization of terminal alkenes to internal alkenes10Catalytic conversion of polyethylene into aromatics with Pt/ZSM-5: insights into reaction pathways and rate-controlling step regulation53Evolution of light olefins during the pyrolysis of polyethylene in a two-stage process49Heterogeneous Pt-catalyzed transfer dehydrogenation of long-chain alkanes with ethylene7Tandem oxidative and thermal cracking of polypropylene at low temperatures21The E factor at 30: a passion for pollution prevention339Thiol–ene Click Chemistry Incorporates Hydroxyl Functionality on Polycyclooctene to Tune Properties30Cationic Tantalum Hydrides Catalyze Hydrogenolysis and Alkane Metathesis Reactions of Paraffins and Polyethylene38Multicatalysis enables turning plastic waste into chemical commodities2Metal-catalyzed plastic depolymerization79Recent Advances in Catalytic Chemical Recycling of Polyolefins104Catalytic Biorefining of Natural Oils to Basic Olefinic Building Blocks of Proven Chemical Valorization Schemes10Catalytic Biorefining of Natural Oils to Basic Olefinic Building Blocks of Proven Chemical Valorization Schemes1The role of porosity and acidity in the catalytic upcycling of polyethylene8Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance63Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance4Highly Robust and Efficient Blechert-Type Cyclic(alkyl)(amino)carbene Ruthenium Complexes for Olefin Metathesis32Making Persistent Plastics Degradable14Degradation of Polyacrylates by One-Pot Sequential Dehydrodecarboxylation and Ozonolysis82Low-Temperature Dehydrogenation of Cyclooctane by Using Pincer Iridium Complexes Bearing an N,N′-Diarylated PNCNP Ligand7Composition analysis of post‐consumer recycled blends of linear low‐ and low‐density polyethylene using a solution‐based technique11Highly Selective Catalytic Oxi‐upcycling of Polyethylene to Aliphatic Dicarboxylic Acid under a Mild Hydrogen‐Free Process7Highly Selective Catalytic Oxi‐upcycling of Polyethylene to Aliphatic Dicarboxylic Acid under a Mild Hydrogen‐Free Process73Bifunctional tandem catalytic upcycling of polyethylene to surfactant-range alkylaromatics101Spectroscopic investigations to reveal synergy between polystyrene waste and paraffin wax in super-hydrophobic sand14Sustainable developments in polyolefin chemistry: Progress, challenges, and outlook204Efficient solvent- and hydrogen-free upcycling of high-density polyethylene into separable cyclic hydrocarbons171Hydrogen-free catalytic depolymerization of waste polyolefins at mild temperatures43Efficient upcycling of high-density polyethylene into separable cyclic hydrocarbons1Upcycling of polyethylenes by catalysis0Circular Polyolefins: Advances toward a Sustainable Future76Regulating crystalline morphology jointly by dynamic shearing and solid phase stretching endows polyethylene high modulus, strength and heat-resistance6Review and recommendations for sustainable pathways of recycling commodity plastic waste across different economic regions51Chemical upcycling of polyethylene, polypropylene, and mixtures to high-value surfactants349Hydroformylation of pyrolysis oils to aldehydes and alcohols from polyolefin waste195Activity of Silica-Alumina for the Conversion of Polyethylene into Tunable Aromatics Below Pyrolytic Temperatures20Plastics upcycling made more sustainable and practical21Quantifying synergy for mixed end-scission and random-scission catalysts in polymer upcycling12Solvent‐Free Depolymerization of Plastic Waste Enabled by Plastic‐Catalyst Interfacial Engineering55Solvent‐Free Depolymerization of Plastic Waste Enabled by Plastic‐Catalyst Interfacial Engineering3Homogeneous Catalysis in Plastic Waste Upcycling: A DFT Study on the Role of Imperfections in Polymer Chains15Co-upcycling of polyvinyl chloride and polyesters199Biodegradable polymers from lignocellulosic biomass and synthetic plastic waste: An emerging alternative for biomedical applications63End-of-Life Plastics Management: A Review7Ce-Promoted PtSn-Based Catalyst for Hydrocracking of Polyolefin Plastic Waste into High Yield of Gasoline-Range Products60Total revalorization of high impact polystyrene (HIPS): enhancing styrene recovery and upcycling of the rubber phase33Selective Electrocatalytic Degradation of Ether‐Containing Polymers31Selective Electrocatalytic Degradation of Ether‐Containing Polymers1Closed-loop recycling of semi-aromatic polyesters upcycled from poly(ethylene terephthalate)10The thermodynamics and kinetics of depolymerization: what makes vinyl monomer regeneration feasible?98A butadiene-derived semicrystalline polyolefin with two-tiered chemical recyclability23Thiol-ene click chemistry incorporates carboxylic acid-terminated alkane pendants on polycyclooctene to tune properties14Controlled degradation of chemically stable poly(aryl ethers) via directing group-assisted catalysis6Depolymerization of waste polyethylene to linear alkenes via sequential dehydrogenation and metathesis19Design of depolymerizable polymers toward a circular economy69Modern mechanistic approaches for the depolymerization of commodity plastics via organometallic catalysis0Ruthenium-catalyzed “open-loop” recycling of polyethylene via tandem isomerization-metathesis (ISOMET)12Synergistic catalysis for promoting selective C–C/C–O cleavage in plastic waste: structure–activity relationship and rational design of heterogeneous catalysts for liquid hydrocarbon production18Sustainable high-density polyethylene via chemical recycling: From modification to polymerization methods45Catalytic conversion of mixed polyolefins under mild atmospheric pressure48Artificial Processive Catalytic Systems3Pickering emulsion droplets and solid microspheres acting synergistically for continuous-flow cascade reactions49Population Balance Equations for Reactive Separation in Polymer Upcycling20Upcycling Waste Plastics with a C–C Backbone by Heterogeneous Catalysis45Circular olefin copolymers made de novo from ethylene and α-olefins83Depolymerization within a Circular Plastics System387Recent Progresses and Challenges in Upcycling of Plastics through Selective Catalytic Oxidation15Synthesis and Deconstruction of Polyethylene-type Materials194Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes3Chloride and Hydride Transfer as Keys to Catalytic Upcycling of Polyethylene into Liquid Alkanes29“Inverted” Cyclic(Alkyl)(Amino)Carbene (CAAC) Ruthenium Complex Catalyzed Isomerization Metathesis (ISOMET) of Long Chain Olefins to Propylene at Low Ethylene Pressure15Structural Design of Single‐Atom Catalysts for Enhancing Petrochemical Catalytic Reaction Process31A Microkinetic Model for Isomerizing Ethenolysis8Complete hydrogenolysis of mixed plastic wastes101Three-stage pyrolysis-catalytic dry reforming of waste polyolefins over MFI and Ni-MFI catalysts for BTEX and syngas production8Oxidative Upcycling of Polyethylene to Long Chain Diacid over Co‐MCM‐41 Catalyst12Oxidative Upcycling of Polyethylene to Long Chain Diacid over Co‐MCM‐41 Catalyst58i PP/HDPE blends compatibilized by a polyester: An unconventional concept to valuable products25Deconstruction of Polymers through Olefin Metathesis101A Merger of Relay Catalysis with Dynamic Kinetic Resolution Enables Enantioselective β‐C(sp3)−H Arylation of Alcohols0A Merger of Relay Catalysis with Dynamic Kinetic Resolution Enables Enantioselective β‐C(sp3)−H Arylation of Alcohols11Indolo[3,2-b]carbazole-based Hyper-Crosslinked organic polymers for adsorptive separation of C3H6/C2H412Lifecycle Management for Sustainable Plastics: Recent Progress from Synthesis, Processing to Upcycling87Catalytic chemical recycling and upcycling of polyolefin plastics27Recent advances in polyolefin plastic waste upcycling via mild heterogeneous catalysis route from catalyst development to process design25Mild Catalytic Degradation of Crystalline Polyethylene Units in a Solid State Assisted by Carboxylic Acid Groups23Multi‐Catalytic Metal‐Based Homogeneous‐Heterogeneous Systems in Organic Chemistry11Recycling polyolefin plastic waste at short contact times via rapid joule heating93Active species in chloroaluminate ionic liquids catalyzing low-temperature polyolefin deconstruction22Deconstruction of unsaturated polymers through photo-mediated oxidation under O27Recycling the polyethylene into fuels via an olefin-intermediate tandem catalysis over Fe2O3/USY catalysts3Copolymerization of Olefins and Conjugated Dienes: A Promising Approach to Produce Recyclable Polyolefins14Polyoxymethylene Upcycling into Methanol and Methyl Groups Catalyzed by a Manganese Pincer Complex18Circular Melt-Spun Textile Fibers from Polyethylene-like Long-Chain Polyesters7Industrial and Laboratory Technologies for the Chemical Recycling of Plastic Waste70Catalytic Upcycling of Polyolefins316Depolymerization of Polycarbonates by Transesterification without Using Base, Ionic Liquid, and Additives8Oxidative degradation and upcycling of polyethylene wastes40Reshaping catalysis beyond the conventional0Polyolefin waste to light olefins with ethylene and base-metal heterogeneous catalysts151N2O deconstruction of polycyclooctene to generate carbonyl-functionalized macromonomers3Selective Upcycling of Polyolefins into High-Value Nitrogenated Chemicals80Surface-Activated Mechano-Catalysis for Ambient Conversion of Plastic Waste48Identifying kinetic models from reactor measurements2Oxidation by Dehydrogenation0Tailoring the Properties of Chemically Recyclable Polyethylene‐Like Multiblock Polymers by Modulating the Branch Structure32Tailoring the Properties of Chemically Recyclable Polyethylene‐Like Multiblock Polymers by Modulating the Branch Structure9Installing a Trigger to Upcycle High-Density Polyethylene42Hydroaminoalkylation for Amine Functionalization of Vinyl‐Terminated Polyethylene Enables Direct Access to Responsive Functional Materials14Hydroaminoalkylation for Amine Functionalization of Vinyl‐Terminated Polyethylene Enables Direct Access to Responsive Functional Materials3Close-loop chemical recycling unlocked via waste polyolefins-ethylene co-metathesis2The new developments of the design and application of novel propane dehydrogenation catalysts0One-pot catalytic conversion of polyethylene wastes to gasoline through a dual-catalyst system41Upcycling Polyethylene to High‐Purity Hydrogen under Ambient Conditions via Mechanocatalysis2Upcycling Polyethylene to High‐Purity Hydrogen under Ambient Conditions via Mechanocatalysis15Chemical transformation of polyurethane into valuable polymers26Polyethylene hydrogenolysis by dilute RuPt alloy to achieve H2-pressure-independent low methane selectivity70Kinetic Models for Polymer Upcycling by Tag-and-Cut Strategies6Heterogeneous catalysis strategies for polyolefin plastic upcycling: co-reactant-assisted and direct transformation under mild conditions15Micron-level aggregate initiated ultra hydrophobicity with enhanced intumescent flame retardancy, smoke suppression, and toughness simultaneously in polypropylene23Recent Progress in Polyolefin Plastic: Polyethylene and Polypropylene Transformation and Depolymerization Techniques22Depolymerization by transition metal complexes: strategic approaches to convert polymeric waste into feedstocks3Upcycling of waste plastics: strategies, status-quo, and prospects3An efficient strategy for simultaneous gold deposition and obtention of hierarchical Au/TS-1 applied to liquid-phase propylene epoxidation0Ethylene and alkyl acrylate copolymers made-to-order using dynamic cation switching polymerization and evidence for improved polymer degradability with low polar group density0Highly adaptable oxidative upcycling of polyolefins to multifunctional chemicals containing oxygen and nitrogen9Influence of functional additives, fillers, and pigments on thermal and catalytic pyrolysis of polyethylene for waste plastic upcycling61Low temperature polyolefin deconstruction via tandem cracking-hydrogenation2Recent developments in recycling of post-consumer polyethylene waste33Upcycling polyethersulfones to luminescent materials by aminolysis4UV-driven anchor carbon dots towards flame-retardant polypropylene with durable anti-UV aging and recyclable performance0Conversion of Polypropylene to Light Olefins by HMFI Catalysts below Pyrolytic Temperature: Catalytic, Spectroscopic, and Theoretical Studies3Ruthenium‐Catalyzed Deconstruction of Polyolefins: A Strategy to Up‐cycle Waste Polyethylene to Value‐Added Alkene1Ruthenium‐Catalyzed Deconstruction of Polyolefins: A Strategy to Up‐cycle Waste Polyethylene to Value‐Added Alkene20Room Temperature Ethene to Propene (ETP) Tandem Catalysis using Single Crystalline Solid‐State Molecular Pre‐Catalysts2Room Temperature Ethene to Propene (ETP) Tandem Catalysis using Single Crystalline Solid‐State Molecular Pre‐Catalysts0Synthesis of Polyamides Bearing Directing Groups and Their Catalytic Depolymerization3Emerging Plastic Recycling Strategies Based on Photothermal Conversion15Anionic Surfactants from Reactive Separation of Hydrocarbons Derived from Polyethylene Upcycling8Polymer Molecular Weight Distributions: A Tutorial on Transformations between Number Density, Mass Density, and Linear/Logarithmic Axes4Effects of Pretreatment Conditions and Branched Alkanes on Mo/MCM-41 Catalysts in Tandem Alkane Cross-metathesis for Non-hydrogen Polyolefin Recycling3In-Situ Thermometry Reveals Fragmentation Behavior Based on Local Temperature in α-Olefin Polymerization Catalysts7Recycling homocarbon backbone polymers toward a circular materials economy12Exploring biotechnology for plastic recycling, degradation and upcycling for a sustainable future43

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