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RESEARCH PAPER · Chemistry of Materials · 1998

The First Fully Fluorinated Organically Templated Materials: Synthesis, Structures, and Physical Properties of [H3N(CH2)3NH3]U2F10·2H2O, [H3N(CH2)4NH3]U2F10·3H2O, [H3N(CH2)6NH3]U2F10·2H2O, and [HN(CH2CH2NH3)3]U5F24

Robin J. Francis, P. Shiv Halasyamani, Dermot O’Hare

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The First Fully Fluorinated Organically Templated Materials: Synthesis, Structures, and Physical Properties of [H3N(CH2)3NH3]U2F10·2H2O, [H3N(CH2)4NH3]U2F10·3H2O, [H3N(CH2)6NH3]U2F10·2H2O, and [HN(CH2CH2NH3)3]U5F24OriginalNew Layered Uranium(VI) Molybdates: Syntheses and Structures of (NH3(CH2)3NH3)(H3O)2(UO2)3(MoO4)5, C(NH2)3(UO2)(OH)(MoO4), (C4H12N2)(UO2)(MoO4)2, and (C5H14N2)(UO2)(MoO4)2·H2O120Chapter 16. Scandium, yttrium, the lanthanides and the actinides3Chapter 21. New compounds and structures1Oxyfluorinated Open Frameworks8Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride63Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties67Hydrothermal Syntheses of Layered Uranium Oxyfluorides: Illustrations of Dimensional Reduction43Hydrothermal Syntheses, Structures, and Fluorescence Spectroscopy of New One-Dimensional Uranium Oxyfluorides Built from Edge-Sharing [UO2F5] Pentagonal Bipyramids78Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]44Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions115Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F3143Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O22Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)73Hydrothermal synthesis of the first organically templated open-framework uranium phosphate66Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)53Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides8The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O29Synthesis of Cyclical Diamine Templated Uranium Sulfates103Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates56The effects of linear diamine chain length in uranium sulfates48[(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework852D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties78Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)130[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system159The Role of Amine Sulfates in Hydrothermal Uranium Chemistry63Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)81Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23[(CH3)2NH(CH2)2NH(CH3)2][(UO2)2F2(HPO4)2]: a new organically templated layered uranium phosphate fluoride - synthesis, structure, characterization, and ion-exchange reactions9Old materials with new tricks: multifunctional open-framework materials1073Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6Synthesis and property of three novel organically templated layered cerium materials6Uranyl Ion Complexation by Citric and Citramalic Acids in the Presence of Diamines61Hydrothermal Vanadium Fluoride Chemistry: Four New V3+ Chain Structures29Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families46Probing the Reactivity of the Potent AgF2 Oxidizer. Part 1: Organic Compounds12The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Probing the Reactivity of the Potent AgF2 Oxidizer. Part 2: Inorganic Compounds28Synthesis, Structure and Thermal Property of [(n-C16H33)N(CH3)3]2[TiF6]·2H2O7Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands40The theory-driven quest for a novel family of superconductors: fluorides31Oxo ligand functionalization in the uranyl ion (UO22+)335Magnetic Properties5Structural chemistry of organically-templated metal fluorides61Novel Layered Hybrid Fluoroaluminate in the Composition Space Diagram of the Al(OH)3-HguaCl-HFaq-EtOH System18Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18Polyanion Condensation in Inorganic and Hybrid Fluoroaluminates6Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium48Fluoroaluminates of purine and DNA bases, adenine, guanine: [Hpur]2·(AlF5), [Hade]3·(AlF6)·6.5H2O, [Hguan]3·(Al3F12)9Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds72Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine10Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties32From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Anionic uranyl oxyfluorides as a bifunctional platform for highly selective ion-exchange and photocatalytic degradation of organic dyes13Facile Ionic Liquid‐Assisted Strategy for Direct Precipitation of Eu2+‐Activated Nanophosphors under Ambient Conditions18

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  1. New Layered Uranium(VI) Molybdates: Syntheses and Structures of (NH3(CH2)3NH3)(H3O)2(UO2)3(MoO4)5, C(NH2)3(UO2)(OH)(MoO4), (C4H12N2)(UO2)(MoO4)2, and (C5H14N2)(UO2)(MoO4)2·H2O

    Inorganic Chemistry · 1998-12-31

    P. Shiv Halasyamani, Robin J. Francis, Susan M. Walker, Dermot O’Hare

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  2. Chapter 16. Scandium, yttrium, the lanthanides and the actinides

    Annual Reports Section A (Inorganic Chemistry) · 1999-01-01

    S. A. Cotton

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  3. Chapter 21. New compounds and structures

    Annual Reports Section A (Inorganic Chemistry) · 1999-01-01

    William T. A. Harrison

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  4. Oxyfluorinated Open Frameworks

    Elsevier eBooks · 2000-01-01

    Gérard Férey, Thierry Loiseau, Didier Riou

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  5. Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride

    Inorganic Chemistry · 2000-08-01

    Simon Allen, Stephen H. Barlow, P. Shiv Halasyamani, J. Frederick W. Mosselmans, Dermot O’Hare, Susan M. Walker, Richard I. Walton

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  6. Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties

    Chemistry of Materials · 2000-09-15

    Philip M. Almond, Laura Deakin, Melissa J. Porter, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  7. Hydrothermal Syntheses of Layered Uranium Oxyfluorides: Illustrations of Dimensional Reduction

    Inorganic Chemistry · 2000-10-26

    Catherine E. Talley, Amanda C. Bean, Thomas E. Albrecht‐Schmitt

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  8. Hydrothermal Syntheses, Structures, and Fluorescence Spectroscopy of New One-Dimensional Uranium Oxyfluorides Built from Edge-Sharing [UO2F5] Pentagonal Bipyramids

    Journal of Solid State Chemistry · 2000-11-01

    Philip M. Almond, Catherine E. Talley, Amanda C. Bean, Shane M. Peper, Thomas E. Albrecht‐Schmitt

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  9. Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]

    Inorganic Chemistry · 2001-01-17

    Philip M. Almond, Laura Deakin, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  10. Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions

    Chemistry of Materials · 2001-03-20

    Amanda C. Bean, Shane M. Peper, Thomas E. Albrecht‐Schmitt

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  11. Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31

    Journal of Solid State Chemistry · 2001-04-01

    Philip M. Almond, Laura Deakin, A. Mar, Thomas E. Albrecht‐Schmitt

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  12. Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O

    Journal of Solid State Chemistry · 2001-06-01

    Richard E. Sykora, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  13. Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)

    Inorganic Chemistry · 2001-06-30

    Amanda C. Bean, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  14. Hydrothermal synthesis of the first organically templated open-framework uranium phosphate

    Chemical Communications · 2001-10-31

    Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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  15. Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)

    Journal of Solid State Chemistry · 2001-11-01

    Amanda C. Bean, Thomas E. Albrecht‐Schmitt

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  16. Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides

    Chemistry of Materials · 2001-11-17

    Richard E. Sykora, Thomas E. Albrecht‐Schmitt

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  17. The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O

    Chemical Communications · 2002-01-01

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  18. Synthesis of Cyclical Diamine Templated Uranium Sulfates

    Chemistry of Materials · 2002-11-12

    Alexander J. Norquist, Paul M. Thomas, M.B. Doran, Dermot O’Hare

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  19. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

    Inorganic Chemistry · 2003-03-25

    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  20. Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates

    Chemistry of Materials · 2003-04-16

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  21. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

    Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  22. [(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework

    Journal of the American Chemical Society · 2003-09-26

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  23. 2D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties

    European Journal of Inorganic Chemistry · 2003-10-01

    Yong‐Rong Xie, Hong Lin Zhao, Xisen Wang, Zhi‐Rong Qu, Ren‐Gen Xiong, Xiang Xue, Zi‐Ling Xue, Xiao‐Zeng You

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  24. Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)

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    Lauren A. Borkowski, Christopher L. Cahill

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  25. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

    Inorganic Chemistry · 2004-11-23

    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  26. Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system

    Dalton Transactions · 2005-01-01

    M. Frisch, Christopher L. Cahill

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  27. The Role of Amine Sulfates in Hydrothermal Uranium Chemistry

    Inorganic Chemistry · 2005-05-01

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  28. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

    Inorganic Chemistry · 2005-07-29

    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  29. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

    Inorganic Chemistry · 2006-01-27

    Chih-Min Wang, Chia-Hsien Liao, Pei-Lin Chen, Kwang‐Hwa Lii

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  30. Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)

    Journal of Fluorine Chemistry · 2006-09-20

    Thierry Loiseau, Gérard Férey

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  31. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  32. [(CH3)2NH(CH2)2NH(CH3)2][(UO2)2F2(HPO4)2]: a new organically templated layered uranium phosphate fluoride - synthesis, structure, characterization, and ion-exchange reactions

    Dalton Transactions · 2007-01-01

    Kang Min Ok, M.B. Doran, Dermot O’Hare

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  33. Old materials with new tricks: multifunctional open-framework materials

    Chemical Society Reviews · 2007-01-01

    Daniel Maspoch, Daniel Ruiz‐Molina, Jaume Veciana

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  34. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

    Dalton Transactions · 2007-01-01

    Chih-Min Wang, Yi‐Ying Wu, Pei-Lin Chen, Kwang‐Hwa Lii

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  35. Synthesis and property of three novel organically templated layered cerium materials

    Microporous and Mesoporous Materials · 2007-01-11

    Dan Wang, Ranbo Yu, Hong Wang, Xiaotian Li, Xianran Xing

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  36. Uranyl Ion Complexation by Citric and Citramalic Acids in the Presence of Diamines

    Inorganic Chemistry · 2007-02-13

    P. Thuéry

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  37. Hydrothermal Vanadium Fluoride Chemistry: Four New V3+ Chain Structures

    Inorganic Chemistry · 2007-04-21

    David W. Aldous, Nicholas F. Stephens, Philip Lightfoot

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  38. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

    Inorganic Chemistry · 2007-08-24

    Sukhendu Bikas Mandal, Manabendra Chandra, Srinivasan Natarajan

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  39. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  40. Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families

    CrystEngComm · 2007-12-14

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  41. Probing the Reactivity of the Potent AgF2 Oxidizer. Part 1: Organic Compounds

    Collection of Czechoslovak Chemical Communications · 2008-01-01

    Dorota Grzybowska, Przemysław J. Malinowski, Zoran Mazej, Wojciech Grochala

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  42. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  43. Probing the Reactivity of the Potent AgF2 Oxidizer. Part 2: Inorganic Compounds

    Zeitschrift für anorganische und allgemeine Chemie · 2008-10-27

    Przemysław J. Malinowski, Zoran Mazej, Wojciech Grochala

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  44. Synthesis, Structure and Thermal Property of [(n-C16H33)N(CH3)3]2[TiF6]·2H2O

    Acta Physico-Chimica Sinica · 2008-11-01

    G LIU, Guoxing Li, F LIAO, J LIN

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  45. Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands

    CrystEngComm · 2008-11-19

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  46. The theory-driven quest for a novel family of superconductors: fluorides

    Journal of Materials Chemistry · 2009-01-01

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  47. Oxo ligand functionalization in the uranyl ion (UO22+)

    Coordination Chemistry Reviews · 2009-06-22

    Skye Fortier, Trevor W. Hayton

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  48. Magnetic Properties

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    Norman M. Edelstein, G. H. Lander

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  49. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  50. Novel Layered Hybrid Fluoroaluminate in the Composition Space Diagram of the Al(OH)3-HguaCl-HFaq-EtOH System

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