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RESEARCH PAPER · Chemical Communications · 2001

Hydrothermal synthesis of the first organically templated open-framework uranium phosphate

Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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Hydrothermal synthesis of the first organically templated open-framework uranium phosphateOriginal22 New compounds and structures in the solid state2Strategies for the synthesis of porous metal phosphonate materials54ChemInform Abstract: Hydrothermal Synthesis of the First Organically Templated Open‐Framework Uranium Phosphate.0Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates65Expanding the Remarkable Structural Diversity of Uranyl Tellurites: Hydrothermal Preparation and Structures of K[UO2Te2O5(OH)], Tl3{(UO2)2[Te2O5(OH)](Te2O6)}·2H2O, β-Tl2[UO2(TeO3)2], and Sr3[UO2(TeO3)2](TeO3)257Synthesis of Cyclical Diamine Templated Uranium Sulfates103Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17The effects of linear diamine chain length in uranium sulfates48Structures and synthesis of framework Rb and Cs uranyl arsenates and their relationships with their phosphate analogues312D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties78Structures and syntheses of framework triuranyl diarsenate hydrates45[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates40[N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)38The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure15New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)88Uranium and Uranium Compounds18Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate75Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons2Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Actinides and Life's Origins84Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O2Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families46PF6− Hydrolysis as a route to unique uranium phosphate materials43The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate12Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370[H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl17Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands40Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks79Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers6New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]15Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds72Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine10Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21Uranyl and/or Rare-Earth Mellitates in Extended Organic–Inorganic Networks: A Unique Case of Heterometallic Cation–Cation Interaction with UVI═O–LnIII Bonding (Ln = Ce, Nd)117Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O15Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14Crystal Chemistry of Uranium Oxides and Minerals27Synthesis, IR spectroscopy and crystal structure of [(UO2)2{Be(H2O)2(PO4)2}]·(H2O), the first compound with a trimer beryllophosphate anion5Complex Inorganic Actinide Materials1Topological analysis of the layered uranyl compounds bearing slabs with UO2:TO4ratio of 2:35The role of 1-ethyl-3-methylimidazolium diethyl phosphate ionic liquid in uranyl phosphate compounds7Insights on uranium uptake mechanisms by ion exchange resins with chelating functionalities: Chelation vs. anion exchange146Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3Exploring the Role of Organic Functional Groups in the Ionothermal Synthesis of Uranyl Phosphate Materials3Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis10Modularity, polytypism, topology, and complexity of crystal structures of inorganic compounds (Review)32Hydrothermal synthesis and structure of organically templated layered neptunyl( vi ) phosphate (NpO 2 ) 3 (PO 4 ) 2 (Terpy)0Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  1. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

    Martin P. Attfield

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  2. Strategies for the synthesis of porous metal phosphonate materials

    Journal of Materials Chemistry · 2002-01-01

    Gary B. Hix, Adele Turner, Benson M. Kariuki, M. Tremayne, Elizabeth J. Maclean

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  3. ChemInform Abstract: Hydrothermal Synthesis of the First Organically Templated Open‐Framework Uranium Phosphate.

    ChemInform · 2002-01-29

    Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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  4. Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates

    Journal of Solid State Chemistry · 2002-08-01

    Andrew J. Locock, Peter Carman Burns

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  5. Expanding the Remarkable Structural Diversity of Uranyl Tellurites: Hydrothermal Preparation and Structures of K[UO2Te2O5(OH)], Tl3{(UO2)2[Te2O5(OH)](Te2O6)}·2H2O, β-Tl2[UO2(TeO3)2], and Sr3[UO2(TeO3)2](TeO3)2

    Inorganic Chemistry · 2002-09-18

    Philip M. Almond, Thomas E. Albrecht‐Schmitt

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  6. Synthesis of Cyclical Diamine Templated Uranium Sulfates

    Chemistry of Materials · 2002-11-12

    Alexander J. Norquist, Paul M. Thomas, M.B. Doran, Dermot M. O'Hare

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  7. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

    Inorganic Chemistry · 2003-03-25

    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  8. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

    Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  9. Structures and synthesis of framework Rb and Cs uranyl arsenates and their relationships with their phosphate analogues

    Journal of Solid State Chemistry · 2003-09-16

    Andrew J. Locock, Peter Carman Burns

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  10. 2D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties

    European Journal of Inorganic Chemistry · 2003-10-01

    Yong‐Rong Xie, Hong Lin Zhao, Xisen Wang, Zhi‐Rong Qu, Ren‐Gen Xiong, Xiang Xue, Zi‐Ling Xue, Xiao‐Zeng You

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  11. Structures and syntheses of framework triuranyl diarsenate hydrates

    Journal of Solid State Chemistry · 2003-10-15

    Andrew J. Locock, Peter Carman Burns

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  12. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot M. O'Hare

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  13. Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates

    Journal of Solid State Chemistry · 2004-06-21

    Andrew J. Locock, Peter Carman Burns

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  14. [N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)

    Journal of Materials Chemistry · 2006-01-01

    Kang Min Ok, M.B. Doran, Dermot M. O'Hare

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  15. The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure

    Journal of Solid State Chemistry · 2006-06-22

    Suzy Surblé, S. Obbade, S. Saad, S. Yagoubi, C. Dion, F. Abraham

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  16. New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)

    Inorganic Chemistry · 2006-11-15

    Kang Min Ok, Jaewook Baek, P. Shiv Halasyamani, Dermot M. O'Hare

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  17. Uranium and Uranium Compounds

    Kirk-Othmer Encyclopedia of Chemical Technology · 2006-11-17

    David L. Clark, Mary P. Neu, Wolfgang Runde, D. Webster Keogh

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  18. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  19. Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate

    Chemistry of Materials · 2006-12-24

    Tatiana Y. Shvareva, S. Skanthakumar, L. Soderholm, Abraham Clearfield, Thomas E. Albrecht‐Schmitt

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  20. Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons

    Elsevier eBooks · 2007-01-01

    Richard E. Sykora, Tatiana Y. Shvareva, Thomas E. Albrecht‐Schmitt

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  21. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

    Inorganic Chemistry · 2007-08-24

    Sukhendu Bikas Mandal, Manabendra Chandra, Srinivasan Natarajan

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  22. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  23. Actinides and Life's Origins

    Astrobiology · 2007-12-01

    Zachary R. Adam

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  24. Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O

    Solid State Sciences · 2007-12-04

    Yaqin Yu, Thomas E. Albrecht‐Schmitt

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  25. Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families

    CrystEngComm · 2007-12-14

    P. Thuéry

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  26. PF6− Hydrolysis as a route to unique uranium phosphate materials

    Chemical Communications · 2008-01-01

    Nicholas P. Deifel, K.T. Holman, Christopher L. Cahill

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  27. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  28. Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate

    Journal of Solid State Chemistry · 2008-05-17

    Travis H. Bray, John D. Gorden, Thomas E. Albrecht‐Schmitt

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  29. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  30. [H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl

    Inorganic Chemistry · 2008-08-23

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  31. Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands

    CrystEngComm · 2008-11-19

    P. Thuéry

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  32. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  33. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  34. Basic concepts

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  35. Copyright Page

    Unknown journal · 2009-01-22

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  36. Dedication

    Unknown journal · 2009-01-22

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  37. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  38. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  39. Preface

    Unknown journal · 2009-01-22

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  40. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  41. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  42. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

    Inorganic Chemistry · 2009-10-30

    Jie Ling, Shijun Wu, Fanrong Chen, Antonio Simonetti, J. T. Shafer, Thomas E. Albrecht‐Schmitt

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  43. A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems

    Journal of Solid State Chemistry · 2009-11-01

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

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  44. Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks

    Crystal Growth & Design · 2009-11-19

    P. Thuéry, B. Masci

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  45. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

    Inorganic Chemistry · 2010-02-12

    Vandavasi Koteswara Rao, K. Bharathi, Ramanath Prabhu, Manabendra Chandra, Srinivasan Natarajan

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  46. U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers

    IOP Conference Series Materials Science and Engineering · 2010-03-01

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

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  47. New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates

    Journal of Solid State Chemistry · 2010-07-25

    Laurent J. Jouffret, Zhenmian Shao, Murielle Rivenet, F. Abraham

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  48. Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]

    American Mineralogist · 2010-08-01

    Joanne E. Stubbs, Jeffrey E. Post, David C. Elbert, Peter J. Heaney, David R. Veblen

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  49. Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds

    Crystal Growth & Design · 2011-03-09

    Pius O. Adelani, Allen G. Oliver, Thomas E. Albrecht‐Schmitt

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  50. Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine

    Inorganic Chemistry · 2011-04-15

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

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