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RESEARCH PAPER · Chemistry of Materials · 2000

Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties

Philip M. Almond, Laura Deakin, Melissa J. Porter, Arthur Mar, Thomas E. Albrecht‐Schmitt

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Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic PropertiesOriginal21 New compounds and structures in the solid state1Hydrothermal Syntheses of Layered Uranium Oxyfluorides: Illustrations of Dimensional Reduction43Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]44Building Unit and Topological Evolution in the Hydrothermal DABCO−U−F System66Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions115Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F3143Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O22Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)73Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)53Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides8Syntheses and Crystal Structures of Two Topologically Related Modifications of Cs2[(UO2)2(MoO4)3]94Organically templated uranium(vi) sulfates: understanding phase stability using composition space83Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17The effects of linear diamine chain length in uranium sulfates48Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)130[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Ethylenediammonium decafluorodineptunate(IV)4[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system159Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51[N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)38UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)81Product evolution in the Np(IV) fluorophosphate system15Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]17Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions31Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d Systems103Oxo ligand functionalization in the uranyl ion (UO22+)335Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Magnetic Properties5Structural chemistry of organically-templated metal fluorides61Experimental Evidence for Magnetic Exchange in Di- and Trinuclear Uranium(IV) Ethynylbenzene Complexes74Novel Layered Hybrid Fluoroaluminate in the Composition Space Diagram of the Al(OH)3-HguaCl-HFaq-EtOH System18Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18A new clover-shaped trinuclear uranium(VI) complex: Synthesis, structure and photoluminescence property26Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates80Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes49Combination of covalent and hydrogen bonding in the formation of 3D uranyl-carboxylate networks28Synthesis, structural and emission studies of a bis (carbamoyl methyl) sulfone complex of uranyl nitrate11Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds72Uranyl carboxyphosphonates that incorporate Cd(II)20Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine10Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Synthesis and Characterization of a Novel Tetranuclear 5f Compound: A New Synthon for Exploring U(IV) Chemistry34Barium uranyl diphosphonates16Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties32Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Actinide oxalates, solid state structures and applications160Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F1341Uranium(IV) Halide (F−, Cl−, Br−, and I−) Monoarene Complexes59Uranium(VI) coordination polymers with pyromellitate ligand: Unique 1D channel structures and diverse fluorescence32Fluoride-coordination chemistry in molecular and low-dimensional magnetism67Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties12Diverse Lanthanide Coordination and Selective Ion Exchange in the Microporous Selenites Na4Ln4(SeO3)7O·nH2O (Ln = Gd, Tb, Dy, Ho, Er, Tm, and Yb)5Inorganic Synthesis of Actinides3Mechanistic Insights into Concerted C–C Reductive Elimination from Homoleptic Uranium Alkyls15Chromium chains as polydentate fluoride ligands for actinides and group IV metals4Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12Organosoluble tetravalent actinide di- and trifluorides2NanMTh6F30: A Large Family of Quaternary Thorium Fluorides8Insight into γ-Irradiation-Induced Structure Evolution of Uranium(IV) Germanates as Crystalline Nuclear Waste Forms2

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  1. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2000-01-01

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  2. Hydrothermal Syntheses of Layered Uranium Oxyfluorides: Illustrations of Dimensional Reduction

    Inorganic Chemistry · 2000-10-26

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  3. Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]

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    Philip M. Almond, Laura Deakin, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  4. Building Unit and Topological Evolution in the Hydrothermal DABCO−U−F System

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  5. Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions

    Chemistry of Materials · 2001-03-20

    Amanda C. Bean, Shane M. Peper, Thomas E. Albrecht‐Schmitt

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  6. Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31

    Journal of Solid State Chemistry · 2001-04-01

    Philip M. Almond, Laura Deakin, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  7. Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O

    Journal of Solid State Chemistry · 2001-06-01

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  8. Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)

    Inorganic Chemistry · 2001-06-30

    Amanda C. Bean, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  9. Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)

    Journal of Solid State Chemistry · 2001-11-01

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  10. Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides

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  11. Syntheses and Crystal Structures of Two Topologically Related Modifications of Cs2[(UO2)2(MoO4)3]

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  12. Organically templated uranium(vi) sulfates: understanding phase stability using composition space

    Journal of Materials Chemistry · 2002-11-12

    Paul M. Thomas, Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  13. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

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    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  14. The effects of linear diamine chain length in uranium sulfates

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    Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  15. Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)

    Inorganic Chemistry · 2003-10-04

    Lauren A. Borkowski, Christopher L. Cahill

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  16. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

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    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot M. O'Hare

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  17. Ethylenediammonium decafluorodineptunate(IV)

    Acta Crystallographica Section E Structure Reports Online · 2004-06-19

    Tyler A. Sullens, Philip M. Almond, Thomas E. Albrecht‐Schmitt

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  18. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

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    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  19. Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system

    Dalton Transactions · 2005-01-01

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  20. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

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    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  21. [N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)

    Journal of Materials Chemistry · 2006-01-01

    Kang Min Ok, M.B. Doran, Dermot M. O'Hare

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  22. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

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  23. Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)

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  24. Product evolution in the Np(IV) fluorophosphate system

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  25. Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]

    Journal of Solid State Chemistry · 2006-11-14

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  26. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

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  27. Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions

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  28. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

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  29. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

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  30. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  31. Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d Systems

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  32. Oxo ligand functionalization in the uranyl ion (UO22+)

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  33. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

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  34. Magnetic Properties

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  35. Structural chemistry of organically-templated metal fluorides

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    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  36. Experimental Evidence for Magnetic Exchange in Di- and Trinuclear Uranium(IV) Ethynylbenzene Complexes

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  37. Novel Layered Hybrid Fluoroaluminate in the Composition Space Diagram of the Al(OH)3-HguaCl-HFaq-EtOH System

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  38. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

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  39. A new clover-shaped trinuclear uranium(VI) complex: Synthesis, structure and photoluminescence property

    Inorganic Chemistry Communications · 2010-05-01

    Di Sun, Na Zhang, Qin-Juan Xu, Rong‐Bin Huang, Lan‐Sun Zheng

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  40. Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates

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  41. Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes

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    Shuao Wang, Evgeny V. Alekseev, Jared T. Stritzinger, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  42. Combination of covalent and hydrogen bonding in the formation of 3D uranyl-carboxylate networks

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  43. Synthesis, structural and emission studies of a bis (carbamoyl methyl) sulfone complex of uranyl nitrate

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  44. Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds

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  45. Uranyl carboxyphosphonates that incorporate Cd(II)

    Journal of Solid State Chemistry · 2011-04-14

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  46. Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine

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  47. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

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  48. Synthesis and Characterization of a Novel Tetranuclear 5f Compound: A New Synthon for Exploring U(IV) Chemistry

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  49. Barium uranyl diphosphonates

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  50. Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties

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