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RESEARCH PAPER · Journal of Solid State Chemistry · 2001

Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31

Philip M. Almond, Laura Deakin, Arthur Mar, Thomas E. Albrecht‐Schmitt

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Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31OriginalHydrothermal synthesis of the first organically templated open-framework uranium phosphate66Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)5322 New compounds and structures in the solid state2Organically templated uranium(vi) sulfates: understanding phase stability using composition space83Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17The effects of linear diamine chain length in uranium sulfates48Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)130[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Structural variation in organically templated uranium sulfate fluorides42Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system159Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)81Product evolution in the Np(IV) fluorophosphate system15Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions31Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31Oxo ligand functionalization in the uranyl ion (UO22+)335(NH4)7U6F310Structural chemistry of organically-templated metal fluorides61Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?130Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Application of a Mild Hydrothermal Approach Containing an in Situ Reduction Step to the Growth of Single Crystals of the Quaternary U(IV)-Containing Fluorides Na4MU6F30 (M = Mn2+, Co2+, Ni2+, Cu2+, and Zn2+) Crystal Growth, Structures, and Magnetic Properties60Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F1341Uranium(IV) Halide (F−, Cl−, Br−, and I−) Monoarene Complexes59Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties28Fluoride-coordination chemistry in molecular and low-dimensional magnetism67Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties12Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides18Inorganic Synthesis of Actinides3Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides24Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride14NanMTh6F30: A Large Family of Quaternary Thorium Fluorides8Solubilité et fluoration d’oxydes d’uranium en milieu liquide ionique0CO2 Activation with Formation of Uranium Carbonate Complexes in a Closed Synthetic Cycle17Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)3Homopiperazine (Hexahydro-1,4-diazepine)5Nitrogen-Containing Molecules: Natural and Synthetic Products Including Coordination Compounds1A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate0

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  1. Hydrothermal synthesis of the first organically templated open-framework uranium phosphate

    Chemical Communications · 2001-10-31

    Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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  2. Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)

    Journal of Solid State Chemistry · 2001-11-01

    Amanda C. Bean, Thomas E. Albrecht‐Schmitt

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  3. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

    Martin P. Attfield

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  4. Organically templated uranium(vi) sulfates: understanding phase stability using composition space

    Journal of Materials Chemistry · 2002-11-12

    Paul M. Thomas, Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  5. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

    Inorganic Chemistry · 2003-03-25

    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  6. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

    Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

    Read original paper ↗ ·

  7. Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)

    Inorganic Chemistry · 2003-10-04

    Lauren A. Borkowski, Christopher L. Cahill

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  8. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot M. O'Hare

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  9. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

    Inorganic Chemistry · 2004-11-23

    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  10. Structural variation in organically templated uranium sulfate fluorides

    Dalton Transactions · 2005-01-01

    M.B. Doran, Ben E. Cockbain, Dermot M. O'Hare

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  11. Syntheses, structures and fluorescent properties of two novel coordination polymers in the U–Cu–H 3 pdc system

    Dalton Transactions · 2005-01-01

    M. Frisch, Christopher L. Cahill

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  12. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

    Inorganic Chemistry · 2005-07-29

    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  13. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

    Inorganic Chemistry · 2006-01-27

    Chih-Min Wang, Chia-Hsien Liao, Pei-Lin Chen, Kwang‐Hwa Lii

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  14. Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)

    Journal of Fluorine Chemistry · 2006-09-20

    Thierry Loiseau, Gérard Férey

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  15. Product evolution in the Np(IV) fluorophosphate system

    Journal of Solid State Chemistry · 2006-09-30

    Travis H. Bray, Tyler A. Sullens, Tatiana Y. Shvareva, Richard E. Sykora, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  16. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

    Dalton Transactions · 2007-01-01

    Chih-Min Wang, Yi‐Ying Wu, Pei-Lin Chen, Kwang‐Hwa Lii

    Read original paper ↗ ·

  17. Synthesis, crystal structure and optical properties of [Ag(UO2)3(OAc)9][Zn(H2O)4(CH3CH2OH)2]: A novel compound containing closed-shell 3d10, 4d10 and 5d10 metal ions

    Dalton Transactions · 2007-01-01

    Geng‐Geng Luo, Li-Rong Lin, Rong‐Bin Huang, Lan‐Sun Zheng

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  18. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

    Inorganic Chemistry · 2007-08-24

    Sukhendu Bikas Mandal, Manabendra Chandra, Srinivasan Natarajan

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  19. Oxo ligand functionalization in the uranyl ion (UO22+)

    Coordination Chemistry Reviews · 2009-06-22

    Skye Fortier, Trevor W. Hayton

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  20. (NH4)7U6F31

    Numerical data and functional relationships in science and technology. Group III, Condensed matter · 2010-01-01

    Pierre Villars, Karin CENZUAL, J.L.C. Daams, Roman E. GLADYSHEVSKII, O. Shcherban, Vitaly Dubenskyy, V. Kuprysyuk, Igor SAVYSYUK

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  21. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  22. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

    Inorganic Chemistry · 2010-02-12

    Vandavasi Koteswara Rao, K. Bharathi, Ramanath Prabhu, Manabendra Chandra, Srinivasan Natarajan

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  23. Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?

    Journal of Physics Condensed Matter · 2011-03-01

    James Floyd Scott, R. Blinc

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  24. Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis

    RSC Advances · 2012-11-14

    Qing‐Jiang Pan, Yong-Ming Wang, Run-Xue Wang, Hongyue Wu, Weiting Yang, Zhong‐Ming Sun, Hong‐Xing Zhang

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  25. Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source

    Journal of Fluorine Chemistry · 2014-01-03

    Jacob Olchowka, Christophe Volkringer, Natacha Henry, Thierry Loiseau

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  26. Application of a Mild Hydrothermal Approach Containing an in Situ Reduction Step to the Growth of Single Crystals of the Quaternary U(IV)-Containing Fluorides Na4MU6F30 (M = Mn2+, Co2+, Ni2+, Cu2+, and Zn2+) Crystal Growth, Structures, and Magnetic Properties

    Journal of the American Chemical Society · 2014-03-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

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  27. Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13

    Inorganic Chemistry · 2014-05-27

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

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  28. Uranium(IV) Halide (F−, Cl−, Br−, and I−) Monoarene Complexes

    Inorganic Chemistry · 2014-08-01

    Dominik P. Halter, Henry S. La Pierre, Frank W. Heinemann, Karsten Meyer

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  29. Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties

    Inorganic Chemistry · 2015-02-05

    Jeongho Yeon, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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  30. Fluoride-coordination chemistry in molecular and low-dimensional magnetism

    Coordination Chemistry Reviews · 2015-04-10

    Kasper S. Pedersen, Mikkel A. Sørensen, Jesper Bendix

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  31. Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties

    Journal of Solid State Chemistry · 2015-05-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

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  32. Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides

    Inorganic Chemistry Frontiers · 2017-01-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

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  33. Inorganic Synthesis of Actinides

    Elsevier eBooks · 2017-01-01

    Wei‐Qun Shi, L. Mei, Zhifang Chai

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  34. Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O

    RSC Advances · 2018-01-01

    Alexander T. Chemey, Joseph M. Sperling, Thomas E. Albrecht‐Schmitt

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  35. Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides

    Inorganic Chemistry · 2018-04-10

    Vladislav V. Klepov, Justin B. Felder, Hans‐Conrad zur Loye

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  36. Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride

    Inorganic Chemistry · 2018-12-20

    Alexander T. Chemey, Cristian Celis‐Barros, Kevin Huang, Joseph M. Sperling, Cory J. Windorff, Ryan Baumbach, David E Graf, Dayán Páez‐Hernández, Michael Ruf, David E. Hobart, Thomas E. Albrecht‐Schmitt

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  37. NanMTh6F30: A Large Family of Quaternary Thorium Fluorides

    Crystal Growth & Design · 2018-12-31

    Vladislav V. Klepov, Gregory W. Morrison, Hans‐Conrad zur Loye

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  38. Solubilité et fluoration d’oxydes d’uranium en milieu liquide ionique

    Unknown journal · 2019-10-31

    Florian Joly

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  39. CO2 Activation with Formation of Uranium Carbonate Complexes in a Closed Synthetic Cycle

    Organometallics · 2020-01-09

    Pablo Waldschmidt, Christopher J. Hoerger, Judith Riedhammer, Frank W. Heinemann, Christina Hauser, Karsten Meyer

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  40. Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)

    European Journal of Inorganic Chemistry · 2020-04-29

    Benjamin Scheibe, Juliane März, Moritz Schmidt, Thorsten Stumpf, Florian Kraus

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  41. Homopiperazine (Hexahydro-1,4-diazepine)

    Molbank · 2021-04-10

    R. A. Aitken, Dheirya K. Sonecha, Alexandra M. Z. Slawin

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  42. Nitrogen-Containing Molecules: Natural and Synthetic Products Including Coordination Compounds

    MDPI eBooks · 2021-11-01

    Matiadis, Dimitrios, Eleftherios G. Halevas

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  43. A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate

    Ionics · 2023-05-15

    Li Wang, Jie Qin, Youyuan Ran, Lan Chen

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