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RESEARCH PAPER · Inorganic Chemistry · 2005

The Role of Amine Sulfates in Hydrothermal Uranium Chemistry

Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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The Role of Amine Sulfates in Hydrothermal Uranium ChemistryOriginalOrganically-templated metal sulfates, selenites and selenates194Scandium, yttrium, the lanthanides and the actinides9Synthesis, structure, and property of a uranium–potassium–organic coordination polymer containing infinite metal oxide sheets16A uranium–potassium-organic framework solids: Hydrothermal synthesis, structure, and property of K[(UO2)3 (μ3-OH)3(μ2-OH) (C7H4O4N)2]OH30Synthesis and structure of the first organic–inorganic hybrid tin (II) chlorosulfate: [C6N2H14][SnCl2SO4]2Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis72Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]17Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Synthesis and structural characterization of four new organically-directed bismuth sulfates5Hydrothermal syntheses and crystal structures of new uranyl complexes: UO2( p -C7H4O2Br)2(H2O) and UO2( m -C7H4O2Br)26Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates45A novel uranyl complex UO2(tci)(C3H5N2) · H2O: Synthesis, crystal structure and characterization19Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Charge density matching in templated molybdates26Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization23The Role of Stereoactive Lone Pairs in Templated Vanadium Tellurite Charge Density Matching21Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling69New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates8Nanoscale Chemistry of Uranyl Selenates1Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)35Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates9Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21Syntheses and crystal structures of two novel alkaline uranyl chromates A2(UO2)(CrO4)2 (A=Rb, Cs) with bidentate coordination mode of uranyl ions by chromate anions20Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks17Isopropylammonium Layered Uranyl Chromates: Syntheses and Crystal Structures of [(CH3)2CHNH3]3[(UO2)3(CrO4)2O(OH)3] and[(CH3)2CHNH3]2[(UO2)2(CrO4)3(H2O)]30Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Crystal Chemistry of Uranium Oxides and Minerals27Steric-Induced Layer Flection in Templated Vanadium Tellurites11Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)11Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids70MOFs of Uranium and the Actinides95A Supramolecular Double Sulfate Salt with a Lamellar Type: Crystal Structure and Thermal Behavior21K2Na8(UO2)8Mo4O24[(S,Mo)O4], the first uranium molybdosulfate: synthesis, crystal structure, and comparison to related compounds5Formation Principles for Vanadium Selenites: The Role of pH on Product Composition12Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Role of Noncovalent Interactions in Vanadium Tellurite Chain Connectivities14Layered structure of a supramolecular hybrid sulfate salts: Thermal stability and magnetic behavior13Probing structural adaptability in templated vanadium selenites8Use of Zwitterionic Ligands in Uranyl Hybrid Materials: Explorations on the Structural Features that Control Water Ordering and Mobility6Structural unit charge density and molecular cation templating effects on orientational geometric isomerism and interlayer spacing in 2-D uranyl sulfates11Effect of solution acidity on the structure of amino acid-bearing uranyl compounds7Effect of Ionothermal Conditions on the Crystallization of Organically Templated Uranyl Sulfate Compounds6Structure Evolution and Thermal Decomposition of Supramolecular and Lamellar Hybrid Sulfates Templated by 4-Aminopyridinium4Secondary Role of Aliphatic and Heterocyclic Amines in the Formation of Low-Temperature Amine-Bearing U, Np, and Pu(VI) Chromates2Hydrogen bond network and bond valence analysis on uranyl sulfate compounds with organic-based interstitial cations5Organically Templated Uranyl Sulfates and Selenates: Structural Complexity and Crystal Chemical Restrictions for Isotypic Compounds Formation7

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  1. Organically-templated metal sulfates, selenites and selenates

    Chemical Society Reviews · 2006-01-01

    C. N. R. Rao, J. N. Behera, Meenakshi Dan-Hardi

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  2. Scandium, yttrium, the lanthanides and the actinides

    Annual Reports Section A (Inorganic Chemistry) · 2006-01-01

    S. A. Cotton

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  3. Synthesis, structure, and property of a uranium–potassium–organic coordination polymer containing infinite metal oxide sheets

    Journal of Molecular Structure · 2006-03-01

    Weihai Zhang, Jianshe Zhao

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  4. A uranium–potassium-organic framework solids: Hydrothermal synthesis, structure, and property of K[(UO2)3 (μ3-OH)3(μ2-OH) (C7H4O4N)2]OH

    Inorganic Chemistry Communications · 2006-03-14

    Weihai Zhang, Jianshe Zhao

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  5. Synthesis and structure of the first organic–inorganic hybrid tin (II) chlorosulfate: [C6N2H14][SnCl2SO4]

    Journal of Molecular Structure · 2006-04-27

    Ying Wang, Jianing Xu, Jinyu Sun, Li Wang, Fuxing Sun, Yong Fan, Ming-Hong Xin, Suhua Shi, Guangshan Zhu

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  6. Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis

    Inorganic Chemistry · 2006-06-10

    Thomas R. Veltman, Adam K. Stover, Amy Narducci Sarjeant, Kang Min Ok, P. Shiv Halasyamani, Alexander J. Norquist

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  7. Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]

    Journal of Solid State Chemistry · 2006-11-14

    Kang Min Ok, Dermot O’Hare

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  8. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  9. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

    Elsevier eBooks · 2007-01-01

    Sergey V. Krivovichev, Peter Carman Burns

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  10. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  11. Synthesis and structural characterization of four new organically-directed bismuth sulfates

    Dalton Transactions · 2008-01-01

    Yunlong Fu, Yu Zhang, Zhiwei Xu

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  12. Hydrothermal syntheses and crystal structures of new uranyl complexes: UO2( p -C7H4O2Br)2(H2O) and UO2( m -C7H4O2Br)2

    Journal of Coordination Chemistry · 2008-07-29

    Yige Cai, Weihai Zhang, Sun Qingjin, Zhang Weiping, Zhao Jian-she, Miao Jianyu, Zhanli Ren, Liu Chi-yang

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  13. Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates

    Journal of Solid State Chemistry · 2008-11-21

    Jie Ling, Ginger E. Sigmon, Peter Carman Burns

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  14. A novel uranyl complex UO2(tci)(C3H5N2) · H2O: Synthesis, crystal structure and characterization

    Inorganic Chemistry Communications · 2008-12-01

    Lingling Liang, Yige Cai, Ng Seik Weng, Ronglan Zhang, Jianshe Zhao, Jifeng Wang, Hongling Wu

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  15. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  16. Anion-topology approach

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    Sergey V. Krivovichev

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  17. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  18. Copyright Page

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  19. Dedication

    Unknown journal · 2009-01-22

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  20. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  21. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  22. Preface

    Unknown journal · 2009-01-22

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  23. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  24. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

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  25. Charge density matching in templated molybdates

    Journal of Solid State Chemistry · 2009-03-07

    Hernan Sanchez Casalongue, Sarah J. Choyke, Amy Narducci Sarjeant, Joshua Schrier, Alexander J. Norquist

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  26. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

    Inorganic Chemistry · 2009-10-30

    Jie Ling, Shijun Wu, Fanrong Chen, Antonio Simonetti, J. T. Shafer, Thomas E. Albrecht‐Schmitt

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  27. A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems

    Journal of Solid State Chemistry · 2009-11-01

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

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  28. Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization

    Russian Journal of General Chemistry · 2009-12-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  29. The Role of Stereoactive Lone Pairs in Templated Vanadium Tellurite Charge Density Matching

    Inorganic Chemistry · 2010-05-11

    Kelvin B. Chang, Desmond J. Hubbard, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  30. Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling

    European Journal of Inorganic Chemistry · 2010-05-25

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  31. New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates

    Journal of Solid State Chemistry · 2010-07-25

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  32. A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates

    Crystal Growth & Design · 2010-09-08

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  33. Nanoscale Chemistry of Uranyl Selenates

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  34. Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)

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  35. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

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  36. Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates

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  37. Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]

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  38. Syntheses and crystal structures of two novel alkaline uranyl chromates A2(UO2)(CrO4)2 (A=Rb, Cs) with bidentate coordination mode of uranyl ions by chromate anions

    Journal of Solid State Chemistry · 2012-01-30

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  39. Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks

    Journal of Solid State Chemistry · 2012-02-21

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  40. Isopropylammonium Layered Uranyl Chromates: Syntheses and Crystal Structures of [(CH3)2CHNH3]3[(UO2)3(CrO4)2O(OH)3] and[(CH3)2CHNH3]2[(UO2)2(CrO4)3(H2O)]

    Zeitschrift für anorganische und allgemeine Chemie · 2012-03-29

    Oleg I. Siidra, Еvgeny V. Nazarchuk, Sergey V. Krivovichev

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  41. Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine

    Journal of Solid State Chemistry · 2012-09-05

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  42. Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks

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  43. Crystal Chemistry of Uranium Oxides and Minerals

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  44. Steric-Induced Layer Flection in Templated Vanadium Tellurites

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  45. Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)

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  46. Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids

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  47. MOFs of Uranium and the Actinides

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  48. A Supramolecular Double Sulfate Salt with a Lamellar Type: Crystal Structure and Thermal Behavior

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  49. K2Na8(UO2)8Mo4O24[(S,Mo)O4], the first uranium molybdosulfate: synthesis, crystal structure, and comparison to related compounds

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  50. Formation Principles for Vanadium Selenites: The Role of pH on Product Composition

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