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RESEARCH PAPER · Dalton Transactions · 2010

Structural chemistry of organically-templated metal fluorides

Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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Structural chemistry of organically-templated metal fluoridesOriginalA binuclear molybdenum oxyfluoride: μ-oxido-bis[(2,2′-bipyridyl)fluoridodioxidomolybdenum(VI)]5A binuclear vanadium oxyfluoride: di-μ-oxido-bis[(2,2′-bipyridyl)fluoridooxidovanadium(V)]0A binuclear vanadium oxyfluoride: di-μ-oxido-bis[fluoridooxido(1,10-phenanthroline)vanadium(V)]2ChemInform Abstract: Structural Chemistry of Organically Templated Metal Fluorides0Fluoroaluminates of purine and DNA bases, adenine, guanine: [Hpur]2·(AlF5), [Hade]3·(AlF6)·6.5H2O, [Hguan]3·(Al3F12)92D zirconium fluorides: Synthesis, structure and NMR spectroscopy9Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides31Synthesis of hydrophobic layered luminescent films: Organic–inorganic hybrid mono-n-dodecyloxy-phosphinyl-cerium (terbium)2Crystallographic, magnetic and dielectric studies of the potential multiferroic cryolite (NH4)3FeF66Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?130Mixed metalII–metalIV hybrid fluorides11Fluoride-Rich, Hydrofluorothermal Routes to Functional Transition Metal (Mn, Fe, Co, Cu) Fluorophosphates77[H3tren]3+ and [H4tren]4+ fluoride zirconates or tantalates7An ionothermally prepared S = 1/2 vanadium oxyfluoride kagome lattice164Structural Phase Transition in the S = 1 / 2 Kagome System Cs 2 ZrCu 3 F 12 and a Comparison to the Valence-Bond-Solid Phase in Rb 2 SnCu 3 F 1222Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations9Electrochemical Synthesis of Graphite-Tetrafluoroaluminate Intercalation Compounds4The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures139Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )4The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)8AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids59New structural units in molybdenum oxyfluoride chemistry14Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)16Errors in the Calculation of 27Al Nuclear Magnetic Resonance Chemical Shifts10The first crystallographic example of a face-sharing fluoroaluminate anion Al 2 F 9 3−10The cubic [Ti8F36]4− anion found in the crystal structures of K4Ti8F36·8HF and Rb4Ti8F36·6HF21The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit18Stereochemistry of fluoride and mixed-ligand fluoride complexes of zirconium and hafnium22Crystal Structures and Raman Spectra of Imidazolium Poly[perfluorotitanate(IV)] Salts Containing the [TiF6]2–, ([Ti2F9]−)∞, and [Ti2F11]3– and the New [Ti4F20]4– and [Ti5F23]3– Anions28Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block27Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components13Fluoroferrates with (dabcoH2)2+ or (dabcoH)+ Cations7Synthesis, Structure and Characterisation of One Two-Dimensional Layered Vanadium Tellurite [H2en] n [V2Te2O10] n2Crystal Chemistry and Selected Physical Properties of Inorganic Fluorides and Oxide-Fluorides173Crystal structure of bis(propane-1,3-diammonium) hexafluoridoaluminate fluoride trihydrate2Crystal structure of bis(propane-1,3-diaminium) hexafluoridoaluminate diaquatetrafluoridoaluminate tetrahydrate4Hierarchical symmetry transfer and flexible charge matching in five [M(phen) 3 ] 2+ directed iodoargentates with 1 to 3D frameworks57Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Structure, thermal behavior and characterization of a new hybrid iron fluoride FeF4(2,2′-bipyridine)(H2O)26Hydrothermal synthesis, thermal decomposition and optical properties of Fe2F5(H2O)(Htaz)(taz)(Hdma)3Synthesis, crystal structure, and NMR investigation of 4-amino-1,2,4-triazolium hexafluoridotitanate(IV)7Extending the Family of V4+S= Kagome Antiferromagnets17Extending the Family of V4+S=${{ 1/2 }}$ Kagome Antiferromagnets4Dynamic Directing Effect and Symmetric Correlation in Three pH‐Modulated 1,4‐Diazabicyclo[2.2.2]octane/Iodoargentate Hybrids15Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials2Nature of phase transitions in ammonium oxofluorovanadates, a vibrational spectroscopy study of (NH4)3VO2F4 and (NH4)3VOF57Fluoroferrate templated with HAmTAZ: X-ray single crystal, thermal behaviour, vibrational study and magnetic characterization2Orientational disorder and phase transitions in ammonium oxofluorovanadates, (NH4)3VOF5 and (NH4)3VO2F41Transition‐Metal‐Mediated and ‐Catalyzed C−F Bond Activation by Fluorine Elimination524Übergangsmetallvermittelte und ‐katalysierte C‐F‐Bindungsaktivierung durch Fluoreliminierung75A hybrid fluoride layered perovskite, ( en H 2 )MnF 410Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands9Recent progress of d10 iodoargentate(I)/iodocuprate(I) hybrids: Structural diversity, directed synthesis, and photochromic/thermochromic properties149Solubilité et fluoration d’oxydes d’uranium en milieu liquide ionique0Influence of structure-directing polyhedra and heterocyclic ligands on the chain structures and O/F ordering in a series of zinc vanadium oxyfluorides1Synthesis, Crystal Structures and Characterization of Two Nonmetal Cation Tetrafluoroborates4Three-dimensional metal-halide open frameworks56Novel layered heterobimetallic fluorides with large optical band gaps3Layered Hybrid iron Fluorides2Solvothermal and hydrothermal methods for preparative solid-state chemistry5Extending the Family of Hybrid Layered Fluoride Perovskites2

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  1. A binuclear molybdenum oxyfluoride: μ-oxido-bis[(2,2′-bipyridyl)fluoridodioxidomolybdenum(VI)]

    Acta Crystallographica Section E Structure Reports Online · 2010-07-09

    P. DeBurgomaster, Jon A. Zubieta

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  2. A binuclear vanadium oxyfluoride: di-μ-oxido-bis[(2,2′-bipyridyl)fluoridooxidovanadium(V)]

    Acta Crystallographica Section E Structure Reports Online · 2010-08-10

    P. DeBurgomaster, Jon A. Zubieta

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  3. A binuclear vanadium oxyfluoride: di-μ-oxido-bis[fluoridooxido(1,10-phenanthroline)vanadium(V)]

    Acta Crystallographica Section E Structure Reports Online · 2010-09-24

    P. DeBurgomaster, Jon A. Zubieta

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  4. ChemInform Abstract: Structural Chemistry of Organically Templated Metal Fluorides

    ChemInform · 2010-10-28

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  5. Fluoroaluminates of purine and DNA bases, adenine, guanine: [Hpur]2·(AlF5), [Hade]3·(AlF6)·6.5H2O, [Hguan]3·(Al3F12)

    Solid State Sciences · 2010-11-14

    Amandine Cadiau, Karim Adil, Annie Hémon‐Ribaud, M. Leblanc, A. Jouanneaux, Alexandra M. Z. Slawin, Philip Lightfoot, V. Maisonneuve

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  6. 2D zirconium fluorides: Synthesis, structure and NMR spectroscopy

    Solid State Sciences · 2010-12-03

    A. Ben Ali, Monique Body, M. Leblanc, V. Maisonneuve

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  7. Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides

    Dalton Transactions · 2011-01-01

    Farida H. Aidoudi, P.J. Byrne, Pheobe K. Allan, Simon J. Teat, Philip Lightfoot, Russell E. Morris

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  8. Synthesis of hydrophobic layered luminescent films: Organic–inorganic hybrid mono-n-dodecyloxy-phosphinyl-cerium (terbium)

    Journal of Materials Chemistry · 2011-01-01

    Qiuling Luo, Guanzhong Lu, Shaodian Shen, Xiuzhen Xiao, Dongsen Mao, Yanqin Wan

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  9. Crystallographic, magnetic and dielectric studies of the potential multiferroic cryolite (NH4)3FeF6

    Solid State Sciences · 2011-02-23

    Richard J. Goff, Chiu Chung Tang, Julia E. Parker, Finlay D. Morrison, Philip Lightfoot

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  10. Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?

    Journal of Physics Condensed Matter · 2011-03-01

    James Floyd Scott, R. Blinc

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  11. Mixed metalII–metalIV hybrid fluorides

    Journal of Fluorine Chemistry · 2011-05-02

    Jérôme Lhoste, Karim Adil, Armel Le Bail, M. Leblanc, Annie Hémon‐Ribaud, V. Maisonneuve

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  12. Fluoride-Rich, Hydrofluorothermal Routes to Functional Transition Metal (Mn, Fe, Co, Cu) Fluorophosphates

    Journal of the American Chemical Society · 2011-05-09

    Jennifer A. Armstrong, Edward R. Williams, Mark T. Weller

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  13. [H3tren]3+ and [H4tren]4+ fluoride zirconates or tantalates

    Journal of Fluorine Chemistry · 2011-05-22

    Mohamed Ali Saada, V. Maisonneuve, Jérôme Marrot, Nicolas Mercier, M. Leblanc, Annie Hémon‐Ribaud

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  14. An ionothermally prepared S = 1/2 vanadium oxyfluoride kagome lattice

    Nature Chemistry · 2011-08-26

    Farida H. Aidoudi, David W. Aldous, Richard J. Goff, Alexandra M. Z. Slawin, John Paul Attfield, Russell E. Morris, Philip Lightfoot

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  15. Structural Phase Transition in the S = 1 / 2 Kagome System Cs 2 ZrCu 3 F 12 and a Comparison to the Valence-Bond-Solid Phase in Rb 2 SnCu 3 F 12

    Chemistry of Materials · 2011-09-02

    Sandra A. Reisinger, Chiu Chung Tang, Stephen P. Thompson, Finlay D. Morrison, Philip Lightfoot

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  16. Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations

    Inorganica Chimica Acta · 2011-09-10

    Tiffany M. Smith, Michael Tichenor, Jose Marcelo Vargas, Charles J. O’Connor, Jon A. Zubieta

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  17. Electrochemical Synthesis of Graphite-Tetrafluoroaluminate Intercalation Compounds

    Journal of The Electrochemical Society · 2012-01-01

    Kazuhiko Matsumoto, Kosuke Takagi, Rika Hagiwara

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  18. The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures

    Journal of the American Chemical Society · 2012-02-15

    Martin D. Donakowski, Romain Gautier, Jeongho Yeon, Donald T. Moore, Juan C. Nino, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

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  19. Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-20

    Matic Lozinšek, Evgeny Goreshnik, Boris Žemva

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  20. The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-27

    Martin D. Donakowski, Anastasiya I. Vinokur, Kenneth Reinhard Poeppelmeier

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  21. AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids

    Inorganic Chemistry · 2012-07-25

    Ganna A. Senchyk, Valerii Bukhanko, A.B. Lysenko, Harald Krautscheid, Eduard B. Rusanov, A.N. Chernega, Mirosław Karbowiak, K.V. Domasevitch

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  22. New structural units in molybdenum oxyfluoride chemistry

    Journal of Fluorine Chemistry · 2012-08-09

    David W. Aldous, Philip Lightfoot

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  23. Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)

    Inorganica Chimica Acta · 2012-11-02

    Stephanie Jones, Jose Marcelo Vargas, Steven Pellizzeri, Charles J. O’Connor, Jon A. Zubieta

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  24. Errors in the Calculation of 27Al Nuclear Magnetic Resonance Chemical Shifts

    International Journal of Molecular Sciences · 2012-11-21

    Xianlong Wang, Chengfei Wang, Hui Zhao

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  25. The first crystallographic example of a face-sharing fluoroaluminate anion Al 2 F 9 3−

    Dalton Transactions · 2012-11-30

    Fei Jin Xu, Kazuhiko Matsumoto, Rika Hagiwara

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  26. The cubic [Ti8F36]4− anion found in the crystal structures of K4Ti8F36·8HF and Rb4Ti8F36·6HF

    Chemical Communications · 2013-01-01

    Igor M. Shlyapnikov, Evgeny Goreshnik, Zoran Mazej

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  27. The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit

    Journal of Solid State Chemistry · 2013-01-26

    Hongcheng Lu, Romain Gautier, Zuo-Xi Li, Wanqi Jie, Zheng‐Tang Liu, Kenneth Reinhard Poeppelmeier

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  28. Stereochemistry of fluoride and mixed-ligand fluoride complexes of zirconium and hafnium

    Coordination Chemistry Reviews · 2013-07-07

    Давидович Рувен Лейзерович, Dmitry V. Marinin, Vitalie Stavila, Kenton H. Whitmire

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  29. Crystal Structures and Raman Spectra of Imidazolium Poly[perfluorotitanate(IV)] Salts Containing the [TiF6]2–, ([Ti2F9]−)∞, and [Ti2F11]3– and the New [Ti4F20]4– and [Ti5F23]3– Anions

    Inorganic Chemistry · 2013-07-09

    Igor M. Shlyapnikov, Hélène P. A. Mercier, Evgeny Goreshnik, Gary J. Schrobilgen, Zoran Mazej

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  30. Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block

    Dalton Transactions · 2013-10-07

    Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

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  31. Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components

    Inorganica Chimica Acta · 2013-11-28

    Tiffany M. Smith, Luke Strauskulage, Kathryn Perrin, Diona Symester, Steve R. Freund, Jose Marcelo Vargas, Leonard Spînu, Jon A. Zubieta

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  32. Fluoroferrates with (dabcoH2)2+ or (dabcoH)+ Cations

    Zeitschrift für anorganische und allgemeine Chemie · 2014-02-13

    Ganna Darmograi, Laurent J. Jouffret, Annie Hémon‐Ribaud, M. Leblanc, Gilles Dujardin, V. Maisonneuve, Jérôme Lhoste

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  33. Synthesis, Structure and Characterisation of One Two-Dimensional Layered Vanadium Tellurite [H2en] n [V2Te2O10] n

    Journal of Cluster Science · 2014-04-04

    Zhen Chuan Yang, Yi‐Ping Chen, Zhenqiang Guo, Zhuchai You, Yan‐Qiong Sun, Liuqin Su

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  34. Crystal Chemistry and Selected Physical Properties of Inorganic Fluorides and Oxide-Fluorides

    Chemical Reviews · 2014-08-19

    M. Leblanc, V. Maisonneuve, A. Tressaud

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  35. Crystal structure of bis(propane-1,3-diammonium) hexafluoridoaluminate fluoride trihydrate

    Acta Crystallographica Section E Structure Reports Online · 2014-08-29

    Insaf Abdi, Khulood Al-Sadhan, A. Ben Ali

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  36. Crystal structure of bis(propane-1,3-diaminium) hexafluoridoaluminate diaquatetrafluoridoaluminate tetrahydrate

    Acta Crystallographica Section E Structure Reports Online · 2014-11-07

    Insaf Abdi, Khulood Al-Sadhan, A. Ben Ali

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  37. Hierarchical symmetry transfer and flexible charge matching in five [M(phen) 3 ] 2+ directed iodoargentates with 1 to 3D frameworks

    CrystEngComm · 2015-01-01

    Tanlai Yu, Yangbo Fu, Yangbo Fu, Yilin Wang, Pengfei Hao, Junju Shen, Yunlong Fu, Yunlong Fu

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  38. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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  39. Structure, thermal behavior and characterization of a new hybrid iron fluoride FeF4(2,2′-bipyridine)(H2O)2

    Chemical Research in Chinese Universities · 2015-01-06

    Mouna Smida, Hager Litaiem, Mohamed Dammak, Santiago García‐Granda

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  40. Hydrothermal synthesis, thermal decomposition and optical properties of Fe2F5(H2O)(Htaz)(taz)(Hdma)

    Arabian Journal of Chemistry · 2015-04-26

    Mouna Smida, Jérôme Lhoste, Mohamed Dammak, Santiago García‐Granda

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  41. Synthesis, crystal structure, and NMR investigation of 4-amino-1,2,4-triazolium hexafluoridotitanate(IV)

    Journal of Fluorine Chemistry · 2015-07-04

    V. Ya. Kavun, Давидович Рувен Лейзерович, Вера Богдановна Логвинова, Evgeniy B. Merkulov, В. В. Ткачев

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  42. Extending the Family of V4+S= Kagome Antiferromagnets

    Angewandte Chemie International Edition · 2015-10-30

    Lucy Clark, Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

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  43. Extending the Family of V4+S=${{ 1/2 }}$ Kagome Antiferromagnets

    Angewandte Chemie · 2015-10-30

    Lucy Clark, Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

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  44. Dynamic Directing Effect and Symmetric Correlation in Three pH‐Modulated 1,4‐Diazabicyclo[2.2.2]octane/Iodoargentate Hybrids

    European Journal of Inorganic Chemistry · 2016-08-12

    Tanlai Yu, Huihui Li, Pengfei Hao, Junju Shen, Yunlong Fu

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  45. Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials

    The Philosophical Magazine A Journal of Theoretical Experimental and Applied Physics · 2016-08-31

    A.H. Reshak

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  46. Nature of phase transitions in ammonium oxofluorovanadates, a vibrational spectroscopy study of (NH4)3VO2F4 and (NH4)3VOF5

    Spectrochimica Acta Part A Molecular and Biomolecular Spectroscopy · 2017-01-09

    Yu. V. Gerasimova, Aleksandr S. Oreshonkov, N. M. Laptash, Alexander N. Vtyurin, А. С. Крылов, N. P. Shestakov, A.A. Ershov, A. G. Kocharova

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  47. Fluoroferrate templated with HAmTAZ: X-ray single crystal, thermal behaviour, vibrational study and magnetic characterization

    Journal of the Iranian Chemical Society · 2017-03-14

    Mouna Smida, Santiago García‐Granda, Mohamed Dammak

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  48. Orientational disorder and phase transitions in ammonium oxofluorovanadates, (NH4)3VOF5 and (NH4)3VO2F4

    Acta Crystallographica Section B Structural Science Crystal Engineering and Materials · 2017-11-15

    Anatoly A. Udovenko, Evgeny I. Pogoreltsev, Yuri Marchenko, N. M. Laptash

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  49. Transition‐Metal‐Mediated and ‐Catalyzed C−F Bond Activation by Fluorine Elimination

    Angewandte Chemie International Edition · 2018-06-28

    Takeshi Fujita, Kohei Fuchibe, Junji Ichikawa

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  50. Übergangsmetallvermittelte und ‐katalysierte C‐F‐Bindungsaktivierung durch Fluoreliminierung

    Angewandte Chemie · 2018-06-28

    Takeshi Fujita, Kohei Fuchibe, Junji Ichikawa

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