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RESEARCH PAPER · Inorganic Chemistry · 2007

In Situ Hydrothermal Reduction of Neptunium(VI) as a Route to Neptunium(IV) Phosphonates

Travis H. Bray, Anna‐Gay D. Nelson, Geng Bang Jin, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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In Situ Hydrothermal Reduction of Neptunium(VI) as a Route to Neptunium(IV) PhosphonatesOriginalFurther Examples of the Failure of Surrogates to Properly Model the Structural and Hydrothermal Chemistry of Transuranium Elements: Insights Provided by Uranium and Neptunium Diphosphonates50Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d Systems103Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate40Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate7Structural Variation within Homometallic Uranium(VI) Carboxyphosphonates: In Situ Ligand Synthesis, Directed Assembly, Metal−Ligand Coordination and Hydrogen Bonding82Syntheses, crystal structures, thermal stabilities, luminescence and magnetism of two 3D pillared metal phosphonates19Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems47Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]52Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Zn3(4-OOCC6H4PO3)2: A polar metal phosphonate with pillared layered structure showing SHG-activity and large dielectric anisotropy25USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES24Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates54Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates56Deviation Between the Chemistry of Ce(IV) and Pu(IV) and Routes to Ordered and Disordered Heterobimetallic 4f/5f and 5f/5f Phosphonates50Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates23Barium uranyl diphosphonates16Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates43Ligand Geometry Directed Polar Cobalt(II) Phosphonate Displaying Weak Ferromagnetism23From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates28Expansion of the Rich Structures and Magnetic Properties of Neptunium Selenites: Soft Ferromagnetism in Np(SeO3)213Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Probing the Influence of Phosphonate Bonding Modes to Uranium(VI) on Structural Topology and Stability: A Complementary Experimental and Computational Investigation51Emergence of californium as the second transitional element in the actinide series140Structural and spectroscopic characterization of two new layered uranyl(VI) p-xylenediphosphonate compounds synthesized via ionothermal method13A Mixed‐Valent Uranium Phosphonate Framework Containing UIV, UV, and UVI39Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions23Electrochemical, spectroscopic and theoretical studies on redox speciation of neptunium with phenylphosphonic acid7pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites7New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid1Actinides12Advancing understanding of actinide( iii ) (Ac, Am, Cm) aqueous complexation chemistry18The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds41An updated status and trends in actinide metal-organic frameworks (An-MOFs): From synthesis to application145Layered metal phosphonates: Structures and properties7

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  1. Further Examples of the Failure of Surrogates to Properly Model the Structural and Hydrothermal Chemistry of Transuranium Elements: Insights Provided by Uranium and Neptunium Diphosphonates

    Inorganic Chemistry · 2008-05-02

    Anna‐Gay D. Nelson, Travis H. Bray, Wei Zhan, Richard Geoffrey Haire, T.S. Sayler, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  2. Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d Systems

    Inorganic Chemistry · 2008-05-22

    A.N. Alsobrook, Wei Zhan, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  3. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie International Edition · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  4. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  5. Structural Variation within Homometallic Uranium(VI) Carboxyphosphonates: In Situ Ligand Synthesis, Directed Assembly, Metal−Ligand Coordination and Hydrogen Bonding

    Inorganic Chemistry · 2008-07-31

    Karah E. Knope, Christopher L. Cahill

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  6. Syntheses, crystal structures, thermal stabilities, luminescence and magnetism of two 3D pillared metal phosphonates

    Dalton Transactions · 2009-01-01

    Ruibiao Fu, Shengmin Hu, Xin‐Tao Wu

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  7. Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems

    Inorganic Chemistry · 2009-04-06

    Anna‐Gay D. Nelson, Travis H. Bray, Forrest A. Stanley, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  8. Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]

    Chemical Communications · 2010-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  9. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

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  10. Zn3(4-OOCC6H4PO3)2: A polar metal phosphonate with pillared layered structure showing SHG-activity and large dielectric anisotropy

    Dalton Transactions · 2010-01-01

    Jin-Tang Li, Deng‐Ke Cao, Tomoyuki Akutagawa, Li‐Min Zheng

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  11. USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES

    Comments on Inorganic Chemistry · 2010-03-30

    Juan Diwu, Anna‐Gay D. Nelson, Thomas E. Albrecht‐Schmitt

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  12. Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates

    Inorganic Chemistry · 2010-10-04

    Juan Diwu, Shuao Wang, Zuolei Liao, Peter Carman Burns, Thomas E. Albrecht‐Schmitt

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  13. Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates

    Inorganic Chemistry · 2011-02-03

    Shuao Wang, Eric M. Villa, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  14. Deviation Between the Chemistry of Ce(IV) and Pu(IV) and Routes to Ordered and Disordered Heterobimetallic 4f/5f and 5f/5f Phosphonates

    Inorganic Chemistry · 2011-04-25

    Juan Diwu, Shuao Wang, Justin J. Good, V.H. DiStefano, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  15. Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates

    European Journal of Inorganic Chemistry · 2011-08-05

    Eric M. Villa, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  16. Barium uranyl diphosphonates

    Journal of Solid State Chemistry · 2012-04-06

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Rodney Charles Ewing, Thomas E. Albrecht‐Schmitt

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  17. Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates

    Inorganic Chemistry · 2012-05-30

    Eric M. Villa, Connor J. Marr, Laurent J. Jouffret, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  18. Ligand Geometry Directed Polar Cobalt(II) Phosphonate Displaying Weak Ferromagnetism

    Crystal Growth & Design · 2012-12-12

    Tianhua Zhou, Zhangzhen He, Xiang Xu, Xiang-Ying Qian, Jiang‐Gao Mao

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  19. From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates

    Inorganic Chemistry · 2013-01-09

    Eric M. Villa, Connor J. Marr, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  20. Expansion of the Rich Structures and Magnetic Properties of Neptunium Selenites: Soft Ferromagnetism in Np(SeO3)2

    Inorganic Chemistry · 2014-06-25

    Kariem Diefenbach, Jian Hung Lin, Justin N. Cross, Naresh S. Dalal, Michael Shatruk, Thomas E. Albrecht‐Schmitt

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  21. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  22. Probing the Influence of Phosphonate Bonding Modes to Uranium(VI) on Structural Topology and Stability: A Complementary Experimental and Computational Investigation

    Inorganic Chemistry · 2015-03-27

    Tao Zheng, Qun‐Yan Wu, Yang Gao, Daxiang Gui, Shiwen Qiu, Lanhua Chen, Daopeng Sheng, Juan Diwu, Wei‐Qun Shi, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

    Read original paper ↗ ·

  23. Emergence of californium as the second transitional element in the actinide series

    Nature Communications · 2015-04-16

    Samantha K. Cary, Monica Vasiliu, Ryan Baumbach, Jared T. Stritzinger, Thomas D. Green, Kariem Diefenbach, Justin N. Cross, Kenneth L. Knappenberger, Guokui Liu, Mark A. Silver, A. Eugene DePrince, Matthew J. Polinski, Shelley M. Van Cleve, Jane H. House, Naoki Kikugawa, Andrew Gallagher, Alexandra A. Arico, David A. Dixon, Thomas E. Albrecht‐Schmitt

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  24. Structural and spectroscopic characterization of two new layered uranyl(VI) p-xylenediphosphonate compounds synthesized via ionothermal method

    Inorganica Chimica Acta · 2015-07-04

    Tao Zheng, Yang Gao, Lanhua Chen, Juan Diwu, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  25. A Mixed‐Valent Uranium Phosphonate Framework Containing UIV, UV, and UVI

    Chemistry - A European Journal · 2016-06-29

    Lanhua Chen, Tao Zheng, Song‐Song Bao, Linjuan Zhang, Hsin‐Kuan Liu, Li‐Min Zheng, Jian‐Qiang Wang, Yaxing Wang, Juan Diwu, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  26. Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions

    Inorganic Chemistry · 2017-05-26

    Lanhua Chen, Juan Diwu, Daxiang Gui, Yaxing Wang, Zhehui Weng, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  27. Electrochemical, spectroscopic and theoretical studies on redox speciation of neptunium with phenylphosphonic acid

    Inorganica Chimica Acta · 2018-06-20

    Ashutosh Srivastava, Rama Mohana Rao Dumpala, Neetika Rawat, Bhupendra Singh Tomar

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  28. pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites

    Crystal Growth & Design · 2018-08-03

    Jakob T. Dovgan, Matthew J. Polinski, Brandon Q. Mercado, Eric M. Villa

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  29. New Uranyl Open Framework and Sheet Compounds Formed via In-Situ Protonation of Piperazine by Phosphorous Acid

    Minerals · 2018-11-01

    Eric M. Villa, Justin N. Cross, Thomas E. Albrecht‐Schmitt

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  30. Actinides

    Elsevier eBooks · 2019-12-02

    Sascha T. Löffler, Karsten Meyer

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  31. Advancing understanding of actinide( iii ) (Ac, Am, Cm) aqueous complexation chemistry

    Chemical Science · 2021-01-01

    Zachary R. Jones, Maksim Y. Livshits, Frankie D. White, Elodie Dalodière, Maryline G. Ferrier, Laura M. Lilley, Karah E. Knope, Stosh A. Kozimor, Veronika Mocko, Brian L. Scott, Benjamin William Stein, Jennifer N. Wacker, David H. Woen

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  32. The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds

    Coordination Chemistry Reviews · 2021-06-05

    Sara E. Gilson, Peter Carman Burns

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  33. An updated status and trends in actinide metal-organic frameworks (An-MOFs): From synthesis to application

    Coordination Chemistry Reviews · 2021-07-07

    Kai Lv, Sebastian Fichter, Mei Gu, Juliane März, Moritz Schmidt

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  34. Layered metal phosphonates: Structures and properties

    Coordination Chemistry Reviews · 2025-03-15

    Jia‐Ge Jia, Song‐Song Bao, George K. H. Shimizu, Li‐Min Zheng

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