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RESEARCH PAPER · Inorganic Chemistry · 2008

Structural Variation within Homometallic Uranium(VI) Carboxyphosphonates: In Situ Ligand Synthesis, Directed Assembly, Metal−Ligand Coordination and Hydrogen Bonding

Karah E. Knope, Christopher L. Cahill

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Structural Variation within Homometallic Uranium(VI) Carboxyphosphonates: In Situ Ligand Synthesis, Directed Assembly, Metal−Ligand Coordination and Hydrogen BondingOriginalPentavalent Uranium Oxide via Reduction of [UO 2 ] 2+ Under Hydrothermal Reaction Conditions †83A novel 3D Mn(II) coordination polymer involving 4,4′-dipyridylsulfide and 4,4′-dipyridyltrisulfide obtained by in situ ligand formation from 4,4′-dipyridyldisulfide56Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines69Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds45Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks79Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials113Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions29Uranyl–organic assemblies with the macrocyclic ligand 1,4,8,11-tetraazacyclotetradecane-1,4,8,11-tetraacetate (TETA)34In Situ Synthesis of an Imidazolate‐4‐amide‐5‐imidate Ligand and Formation of a Microporous Zinc–Organic Framework with H2‐and CO2‐Storage Ability135In Situ Synthesis of an Imidazolate‐4‐amide‐5‐imidate Ligand and Formation of a Microporous Zinc–Organic Framework with H2‐and CO2‐Storage Ability31Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates66Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates80Room temperature assembly of a uranyl carboxyphosphonate: Synthesis, characterization and UO22+ hydrolysis34Synthesis, structure and fluorescence properties of a uranyl-2,5-pyridinedicarboxylic acid coordination polymer: The missing member of the UO22+-2,n-pyridinedicarboxylic series34Hydrothermal Synthesis of Uranyl Squarates and Squarate-Oxalates: Hydrolysis Trends and in Situ Oxalate Formation82Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium48Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]15Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction23From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt55Uranyl carboxyphosphonates that incorporate Cd(II)20Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Uranyl Ion Complexation by Aliphatic Dicarboxylic Acids in the Presence of Cucurbiturils as Additional Ligands or Structure-Directing Agents124Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates69Uranyl–Alkali Metal Ion Heterometallic Complexes with Cucurbit[6]uril and a Sulfonated Catechol67Syntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents59Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates67Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril32Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77Uranyl Sensitization of Samarium(III) Luminescence in a Two-Dimensional Coordination Polymer127Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties37Synthesis, crystal structures, and infrared spectroscopy of a series of lanthanide phosphonoacetate coordination polymers9Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures46Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding40From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Uranium diphosphonates templated by interlayer organic amines22Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate71One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids29Supramolecular networks formation in crystals of 3-carboxybenzylphosphonic acid, its complexes and salts: from coordination bonds to weak intermolecular interactions5Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies75Syntheses, structures and luminescent properties of two organic templated uranyl phosphonates18Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels33Molecular Copper(II) Complexes Derived from Phosphonoacetic Acid: Crystal Structures and Magnetic Behavior8Osteopontin: A Uranium Phosphorylated Binding‐Site Characterization59The crystal chemistry of uranium carboxylates394Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands33Isolation of a series of uranium organophosphinates11MOFs of Uranium and the Actinides95Use of Charge-Assisted Hydrogen Bonding in the Supramolecular Assembly of Hybrid Uranyl Materials39Structural Variation within Heterometallic Uranyl Hybrids Based on Flexible Alkyldiphosphonate Ligands40Three New Silver Uranyl Diphosphonates: Structures and Properties23Synthesis and characterization of 1-D uranyl thiodigycolate coordination polymers10A new organically templated open-framework uranyl ethylenediphosphonate6The influence of pressure on the structure of a 2D uranium(VI) carboxyphosphonoate compound11Syntheses, Structures, Luminescence, and Photocatalytic Properties of a Series of Uranyl Coordination Polymers46Homochiral 3D coordination polymer with unprecedented three-directional helical topology from achiral precursor: synthesis, crystal structure, and luminescence properties of uranyl succinate metal–organic framework24Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Synthetic, structural, and luminescence study of uranyl coordination polymers containing chelating terpyridine and trispyridyltriazine ligands34In situ synthesis of amide-imidate-imidazolate ligand and formation of metal-organic frameworks: Application for gas storage11Hybrid Materials Based on Multifunctional Phosphonic Acids4Probing the Influence of Phosphonate Bonding Modes to Uranium(VI) on Structural Topology and Stability: A Complementary Experimental and Computational Investigation51In situ ligand generation for novel Mn(II) and Ni(II) coordination polymers with disulfide ligand: Solvothermal syntheses, structures and magnetic properties4Role of N-Donor Sterics on the Coordination Environment and Dimensionality of Uranyl Thiophenedicarboxylate Coordination Polymers53Structural chemistry of uranium phosphonates143Structural and spectroscopic characterization of two new layered uranyl(VI) p-xylenediphosphonate compounds synthesized via ionothermal method13A Family of Uranyl Coordination Polymers Containing O-Donor Dicarboxylates and Trispyridyltriazine Guests36Structural Variations of the First Family of Heterometallic Uranyl Carboxyphosphinate Assemblies by Synergy between Carboxyphosphinate and Imidazole Ligands21Inorganic Synthesis of Actinides3New complexes constructed from in situ nitration of (1 H -tetrazol-5-yl)phenol: synthesis, structures and properties27Construction of Uranyl Organic Hybrids by Phosphonate and in Situ Generated Carboxyphosphonate Ligands39Synthesis, Crystal Structure, and Characterization of Two Novel One- and Two-Dimensionally Polymeric Copper(II) Phosphonoacetates2A new uranyl triphosphonate constructed from semi-rigid triphosphonate ligand: New method for the construction of higher dimensional uranyl phosponates6Influence of Pyrazine/Piperazine Based Guest Molecules in the Crystal Structures of Uranyl Thiophene Dicarboxylate Coordination Polymers: Structural Diversities and Photocatalytic Activities for the Degradation of Organic Dye47Fabrication of New Uranyl Phosphonates by Varying Quaternary Ammonium Cation: Synthesis, Structure, Luminescent Properties, and Single-Crystal to Single-Crystal Transformation18Coordination chemistry of flexible benzene-1,3,5-tricarboxamide derived carboxylates; notable structural resilience and vaguely familiar packing motifs17Crystal Structure and Characterization of Two Layered Copper(II) Coordination Polymers with Anions of 3‐Phosphonopropionic Acid and ( RS )‐2‐Phosphonobutyric Acid1Actinides12Synthesis, Characterization, and Solid-State Structural Chemistry of Uranium(IV) Aliphatic Dicarboxylates7Chemical and Redox Speciation of Uranyl with Three Environmentally Relevant Bifunctional Chelates: Multi-Technique Approach Combined with Theoretical Estimations14Cation directed formation of uranyl phosphonocarboxylates frameworks comprised of cross-linked chains1Unusual redox stability of pentavalent uranium with hetero-bifunctional phosphonocarboxylate: insight into aqueous speciation9

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  1. Pentavalent Uranium Oxide via Reduction of [UO 2 ] 2+ Under Hydrothermal Reaction Conditions †

    Inorganic Chemistry · 2008-10-09

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  2. A novel 3D Mn(II) coordination polymer involving 4,4′-dipyridylsulfide and 4,4′-dipyridyltrisulfide obtained by in situ ligand formation from 4,4′-dipyridyldisulfide

    CrystEngComm · 2009-01-01

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  3. Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines

    Inorganic Chemistry · 2009-06-22

    Karah E. Knope, Christopher L. Cahill

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  4. Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds

    Inorganic Chemistry · 2009-11-02

    A.N. Alsobrook, Thomas E. Albrecht‐Schmitt

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  5. Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks

    Crystal Growth & Design · 2009-11-19

    P. Thuéry, B. Masci

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  6. Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials

    Chemical Communications · 2010-01-01

    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  7. Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions

    Dalton Transactions · 2010-01-01

    Karah E. Knope, Christopher L. Cahill

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  8. Uranyl–organic assemblies with the macrocyclic ligand 1,4,8,11-tetraazacyclotetradecane-1,4,8,11-tetraacetate (TETA)

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  9. In Situ Synthesis of an Imidazolate‐4‐amide‐5‐imidate Ligand and Formation of a Microporous Zinc–Organic Framework with H2‐and CO2‐Storage Ability

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  10. In Situ Synthesis of an Imidazolate‐4‐amide‐5‐imidate Ligand and Formation of a Microporous Zinc–Organic Framework with H2‐and CO2‐Storage Ability

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    Franziska Debatin, Arne Thomas, Alexandra Kelling, Niklas Hedin, Zoltán Bacsik, Irena Senkovska, Stefan Kaskel, Matthias Junginger, Holger Müller, Uwe Schilde, Christian Jäger, Alwin Friedrich, Hans‐Jürgen Holdt

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  11. Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates

    European Journal of Inorganic Chemistry · 2010-01-29

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  12. Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates

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    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  13. Room temperature assembly of a uranyl carboxyphosphonate: Synthesis, characterization and UO22+ hydrolysis

    Inorganic Chemistry Communications · 2010-06-10

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  14. Synthesis, structure and fluorescence properties of a uranyl-2,5-pyridinedicarboxylic acid coordination polymer: The missing member of the UO22+-2,n-pyridinedicarboxylic series

    Inorganic Chemistry Communications · 2010-06-10

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  15. Hydrothermal Synthesis of Uranyl Squarates and Squarate-Oxalates: Hydrolysis Trends and in Situ Oxalate Formation

    Inorganic Chemistry · 2010-06-16

    Clare E. Rowland, Christopher L. Cahill

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  16. Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium

    Inorganic Chemistry · 2010-07-27

    Padmini Ramaswamy, Ramanath Prabhu, Srinivasan Natarajan

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  17. Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]

    American Mineralogist · 2010-08-01

    Joanne E. Stubbs, Jeffrey E. Post, David C. Elbert, Peter J. Heaney, David R. Veblen

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  18. Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction

    CrystEngComm · 2010-09-06

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  19. From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt

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    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  20. Uranyl carboxyphosphonates that incorporate Cd(II)

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  21. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

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  22. Uranyl Ion Complexation by Aliphatic Dicarboxylic Acids in the Presence of Cucurbiturils as Additional Ligands or Structure-Directing Agents

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  23. Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates

    Crystal Growth & Design · 2011-05-18

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  24. Uranyl–Alkali Metal Ion Heterometallic Complexes with Cucurbit[6]uril and a Sulfonated Catechol

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  25. Syntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents

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  26. Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates

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  27. Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril

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  28. Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules

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  29. Uranyl Sensitization of Samarium(III) Luminescence in a Two-Dimensional Coordination Polymer

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  30. Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties

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  31. Synthesis, crystal structures, and infrared spectroscopy of a series of lanthanide phosphonoacetate coordination polymers

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  32. Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures

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  33. Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures

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  34. The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding

    Inorganic Chemistry · 2012-09-28

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  35. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

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  36. Uranium diphosphonates templated by interlayer organic amines

    Journal of Solid State Chemistry · 2012-10-24

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Thomas E. Albrecht‐Schmitt, Rodney Charles Ewing

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  37. Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate

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  38. One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids

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  39. Supramolecular networks formation in crystals of 3-carboxybenzylphosphonic acid, its complexes and salts: from coordination bonds to weak intermolecular interactions

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  40. Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies

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  41. Syntheses, structures and luminescent properties of two organic templated uranyl phosphonates

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  42. Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels

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  43. Molecular Copper(II) Complexes Derived from Phosphonoacetic Acid: Crystal Structures and Magnetic Behavior

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  44. Osteopontin: A Uranium Phosphorylated Binding‐Site Characterization

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  45. The crystal chemistry of uranium carboxylates

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  46. Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands

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  47. Isolation of a series of uranium organophosphinates

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  48. MOFs of Uranium and the Actinides

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  49. Use of Charge-Assisted Hydrogen Bonding in the Supramolecular Assembly of Hybrid Uranyl Materials

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  50. Structural Variation within Heterometallic Uranyl Hybrids Based on Flexible Alkyldiphosphonate Ligands

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