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RESEARCH PAPER · Inorganic Chemistry · 2008

Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d Systems

A.N. Alsobrook, Wei Zhan, Thomas E. Albrecht‐Schmitt

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Use of Bifunctional Phosphonates for the Preparation of Heterobimetallic 5f−3d SystemsOriginal[M(OOCC6H4PO3H)(H2O)] (M(II) = Mn, Co, Ni): layered metal phosphonates showing variable magnetic behavior30Interconversion of two new nickel(II) coordination polymers with different topologies: synthesis, structure and magnetic properties10Layered copper compounds based on 4-(3-bromothienyl)phosphonate (BTP): weak ferromagnetism observed in [Cu2(4,4′-bpy)0.5(BTP)2]·H2O30Metal phosphonates based on (4-carboxypiperidyl)-N-methylenephosphonate: in situ ligand cleavage and metamagnetism in Co3(O3PCH2-NHC5H9-COO)2(O3PCH2-NC5H10)(H2O)22Syntheses, crystal structures, thermal stabilities, luminescence and magnetism of two 3D pillared metal phosphonates19Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines693,5-Diphosphonobenzoic Acid, a New Rigid Heterotrifunctional Building Block to Design Metal Organic Frameworks. Illustration with the Characterization of Cu5[(O3P)2-C6H3-CO2]2(H2O)621Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds45Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials113Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions29The use of phosphonates for constructing 3d–4f clusters at high oxidation states: synthesis and characterization of two unusual heterometallic CeMn complexes63Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates66Enhanced Photoluminescence Features of Rare Earth Phenylphosphonate Hybrid Nanostructures Synthesized under Nonaqueous Conditions16Supramolecular chemistry with uranyl tetrahalide ([UO2X4]2−) anions44A Lanthanide Ion-Decorated Uranyl−Organic Two-Dimensional Assembly with all-cis 1,2,3,4,5,6-Cyclohexanehexacarboxylic Acid52Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates80Room temperature assembly of a uranyl carboxyphosphonate: Synthesis, characterization and UO22+ hydrolysis34Co3(2-OOCC6H4PO3)2(H2O)3·H2O: A layered metal phosphonate showing reversible dehydration–rehydration behavior and ferrimagnetism29One-dimensional uranium–organic coordination polymers: crystal and electronic structures of uranyl-diacetohydroxamate19From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt55Uranyl carboxyphosphonates that incorporate Cd(II)20Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates69Pillared and open-framework uranyl diphosphonates32Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates67Uranyl–organic one- and two-dimensional assemblies with 2,2′-bipyridine-3,3′-dicarboxylic, biphenyl-3,3′,4,4′-tetracarboxylic and bicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acids50Synthesis, crystal structure and magnetic characterization of metal(II) coordination polymers based on 2-carboxyethylphosphonic acid and 1,10-phenanthroline (metal=Cu, Co, Cd)8Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril32Uranyl Sensitization of Samarium(III) Luminescence in a Two-Dimensional Coordination Polymer127Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties37Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties32Synthesis, crystal structures, and infrared spectroscopy of a series of lanthanide phosphonoacetate coordination polymers9Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures46Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O15Structural Study of Hydrated/Dehydrated Manganese Thiophene-2,5-diphosphonate Metal Organic Frameworks, Mn2(O3P–C4H2S–PO3)·2H2O33The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding40From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Uranium diphosphonates templated by interlayer organic amines22Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate71Structural Observations of Heterometallic Uranyl Copper(II) Carboxylates and Their Solid‐State Topotactic Transformation upon Dehydration63One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids29Uranyl–3d block metal ion heterometallic carboxylate complexes including additional chelating nitrogen donors37Uranyl–copper(ii) heterometallic oxalate complexes: coordination polymers and frameworks47Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies75Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels33Molecular Copper(II) Complexes Derived from Phosphonoacetic Acid: Crystal Structures and Magnetic Behavior8Use of Metalloligands [CuL] (H2L = Salen Type Di-Schiff Bases) in the Formation of Heterobimetallic Copper(II)-Uranyl Complexes: Photophysical Investigations, Structural Variations, and Theoretical Calculations87The crystal chemistry of uranium carboxylates394Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands33Chiral one- to three-dimensional uranyl–organic assemblies from (1R,3S)-(+)-camphoric acid47MOFs of Uranium and the Actinides95Uranyl–Organic Frameworks with Polycarboxylates: Unusual Effects of a Coordinating Solvent77Structural Variation within Heterometallic Uranyl Hybrids Based on Flexible Alkyldiphosphonate Ligands40Three New Silver Uranyl Diphosphonates: Structures and Properties23Postsynthetic Rearrangement/Metalation as a Route to Bimetallic Uranyl Coordination Polymers: Syntheses, Structures, and Luminescence70Incorporation of Cu2+ Ions into Nanotubular Uranyl Diphosphonates28CuPYDC Metalloligands and Postsynthetic Rearrangement/Metalation as Routes to Bimetallic Uranyl Containing Hybrid Materials: Syntheses, Structures, and Fluorescence37Uranyl Ion Complexes with all-cis-1,3,5-Cyclohexanetricarboxylate: Unexpected Framework and Nanotubular Assemblies55Copper(I) and Copper(II) Uranyl Heterometallic Hybrid Materials49Uranyl Ion Complexes with trans‐3‐(3‐Pyridyl)acrylic Acid Including a Uranyl–Copper(II) Heterometallic Framework21Use of 2,2-Bipyrimidine for the Preparation of UO22+-3d Diphosphonates18Uranyl–Organic Hybrids Designed from Hydroxyphosphonate14Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Uranyl and Uranyl–3d Block Cation Complexes with 1,3-Adamantanedicarboxylate: Crystal Structures, Luminescence, and Magnetic Properties68Structural chemistry of uranium phosphonates143Uranyl Ion Complexes with 1,1′-Biphenyl-2,2′,6,6′-tetracarboxylic Acid: Structural and Spectroscopic Studies of One- to Three-Dimensional Assemblies36Molecular Metal Phosphonates220Two Uranyl Complexes with Pyromellitic Acid. A Heterometallic Complex with U=O–CuII Interaction7Structural Variations in the Uranyl/4,4′-Biphenyldicarboxylate System. Rare Examples of 2D → 3D Polycatenated Uranyl–Organic Networks78Silver Ion-Mediated Heterometallic Three-Fold Interpenetrating Uranyl–Organic Framework52Two Types of 2D Layered Iodoargentates Based on Trimeric [Ag3I7] Secondary Building Units and Hexameric [Ag6I12] Ternary Building Units: Syntheses, Crystal Structures, and Efficient Visible Light Responding Photocatalytic Properties108A New Form of Triple-Stranded Helicate Found in Uranyl Complexes of Aliphatic α,ω-Dicarboxylates34Counter-ion control of structure in uranyl ion complexes with 2,5-thiophenedicarboxylate39Directing dimensionality in uranyl malate and copper uranyl malate compounds15Uranyl Ion Complexes with Long-Chain Aliphatic α,ω-Dicarboxylates and 3d-Block Metal Counterions34UO22+-polycarboxylate heterometallic complexes: structure, spectra, and photocatalytic properties12Counterion-Induced Variations in the Dimensionality and Topology of Uranyl Pimelate Complexes41Modulation of the Structure and Properties of Uranyl Ion Coordination Polymers Derived from 1,3,5-Benzenetriacetate by Incorporation of Ag(I) or Pb(II)46Series of Hydrated Heterometallic Uranyl-Cobalt(II) Coordination Polymers with Aromatic Polycarboxylate Ligands: Formation of U═O—Co Bonding upon Dehydration Process29Recent advances in structural studies of heterometallic uranyl-containing coordination polymers and polynuclear closed species93Construction of Uranyl Organic Hybrids by Phosphonate and in Situ Generated Carboxyphosphonate Ligands39Efficient tetracycline adsorption and photocatalytic degradation of rhodamine B by uranyl coordination polymer49Syntheses, Structures, and Comparisons of Heterometallic Uranyl Iodobenzoates with Monovalent Cations27Structural Consequences of 1,4-Cyclohexanedicarboxylate Cis/Trans Isomerism in Uranyl Ion Complexes: From Molecular Species to 2D and 3D Entangled Nets67Molecular and polymeric uranyl and thorium hybrid materials featuring methyl substituted pyrazole dicarboxylates and heterocyclic 1,3-diketones11Crown Ethers and Their Alkali Metal Ion Complexes as Assembler Groups in Uranyl–Organic Coordination Polymers with cis-1,3-, cis-1,2-, and trans-1,2-Cyclohexanedicarboxylates34Bimetallic Uranyl Organic Frameworks Supported by Transition-Metal-Ion-Based Metalloligand Motifs: Synthesis, Structure Diversity, and Luminescence Properties48Three Different Modes of Association between Metal Cations in Heterometallic Uranyl–CoIII and Uranyl–MnII Species7Luminescent complexes associated with isonicotinic acid10Structural Tuning and Sensitization of Uranyl Phosphonates by Incorporation of Countercations into the Framework16Two uranyl-copper(II) bimetallic coordination polymers containing trans-3,3(pyridyl)acrylic acid: Structural variance through synthetic subtleties9Actinides12The presence of mixed-valent silver in the uranyl phenylenediphosphonate framework5Layered Uranyl Phosphonates Encapsulating Co(II)/Mn(II)/Zn(II) Ions: Exfoliation into Nanosheets and Its Impact on Magnetic and Luminescent Properties11Chemical and Redox Speciation of Uranyl with Three Environmentally Relevant Bifunctional Chelates: Multi-Technique Approach Combined with Theoretical Estimations14Cation directed formation of uranyl phosphonocarboxylates frameworks comprised of cross-linked chains1Structural variation in Uranyl-Phosphonate networks utilizing tetrahedral Silicon-Centered phosphonate linkers2The Biological Impact of Some Phosphonic and Phosphinic Acid Derivatives on Human Osteosarcoma7Layered metal phosphonates: Structures and properties7Alkali Metal-Directed Assembly and Structural Characterization of Layered Uranyl Tetrakisphosphonates2Synthesis, structure, and spectroscopic characterization of a novel series of uranyl perrhenates0Structural insights into uranyl oxo interactions for advanced ligand design0

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  1. [M(OOCC6H4PO3H)(H2O)] (M(II) = Mn, Co, Ni): layered metal phosphonates showing variable magnetic behavior

    CrystEngComm · 2009-01-01

    Jintang Li, Tony D. Keene, Deng‐Ke Cao, Silvio Decurtins, Li‐Min Zheng

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  2. Interconversion of two new nickel(II) coordination polymers with different topologies: synthesis, structure and magnetic properties

    Journal of Materials Chemistry · 2009-01-01

    Bowen Hu, Jiong‐Peng Zhao, Qian Yang, Fu‐Chen Liu, Xian‐He Bu

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  3. Layered copper compounds based on 4-(3-bromothienyl)phosphonate (BTP): weak ferromagnetism observed in [Cu2(4,4′-bpy)0.5(BTP)2]·H2O

    Dalton Transactions · 2009-01-01

    Lirong Guo, Feng Zhu, Yu Chen, Yizhi Li, Li‐Min Zheng

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  4. Metal phosphonates based on (4-carboxypiperidyl)-N-methylenephosphonate: in situ ligand cleavage and metamagnetism in Co3(O3PCH2-NHC5H9-COO)2(O3PCH2-NC5H10)(H2O)

    Dalton Transactions · 2009-01-01

    Shou-Zeng Hou, Deng‐Ke Cao, Xun-Gao Liu, Yizhi Li, Li‐Min Zheng

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  5. Syntheses, crystal structures, thermal stabilities, luminescence and magnetism of two 3D pillared metal phosphonates

    Dalton Transactions · 2009-01-01

    Ruibiao Fu, Shengmin Hu, Xin‐Tao Wu

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  6. Homometallic Uranium(VI) Phosphonoacetates Containing Interlayer Dipyridines

    Inorganic Chemistry · 2009-06-22

    Karah E. Knope, Christopher L. Cahill

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  7. 3,5-Diphosphonobenzoic Acid, a New Rigid Heterotrifunctional Building Block to Design Metal Organic Frameworks. Illustration with the Characterization of Cu5[(O3P)2-C6H3-CO2]2(H2O)6

    Crystal Growth & Design · 2009-09-22

    Jean‐Michel Rueff, Olivier Pérez, Ch. Simon, Christophe Lorilleux, Hélène Couthon‐Gourvès, Paul‐Alain Jaffrès

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  8. Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds

    Inorganic Chemistry · 2009-11-02

    A.N. Alsobrook, Thomas E. Albrecht‐Schmitt

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  9. Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials

    Chemical Communications · 2010-01-01

    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  10. Homometallic UO22+ diphosphonates assembled under ambient and hydrothermal conditions

    Dalton Transactions · 2010-01-01

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  11. The use of phosphonates for constructing 3d–4f clusters at high oxidation states: synthesis and characterization of two unusual heterometallic CeMn complexes

    Dalton Transactions · 2010-01-01

    Mei Wang, Daqiang Yuan, Chengbing Ma, Ming-Jian Yuan, Ming‐Qiang Hu, Na Li, Hui Chen, Changneng Chen, Qiutian Liu

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  12. Synthesis and Characterization of 1‐, 2‐, and 3‐Dimensional Bimetallic UO22+/Zn2+ Phosphonoacetates

    European Journal of Inorganic Chemistry · 2010-01-29

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  13. Enhanced Photoluminescence Features of Rare Earth Phenylphosphonate Hybrid Nanostructures Synthesized under Nonaqueous Conditions

    The Journal of Physical Chemistry C · 2010-03-05

    Weihua Di, Rute A. S. Ferreira, Marc‐Georg Willinger, Xinguang Ren, Nicola Pinna

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  14. Supramolecular chemistry with uranyl tetrahalide ([UO2X4]2−) anions

    Comptes Rendus Chimie · 2010-03-30

    Nicholas P. Deifel, Christopher L. Cahill

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  15. A Lanthanide Ion-Decorated Uranyl−Organic Two-Dimensional Assembly with all-cis 1,2,3,4,5,6-Cyclohexanehexacarboxylic Acid

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  16. Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates

    Inorganic Chemistry · 2010-05-13

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  17. Room temperature assembly of a uranyl carboxyphosphonate: Synthesis, characterization and UO22+ hydrolysis

    Inorganic Chemistry Communications · 2010-06-10

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  18. Co3(2-OOCC6H4PO3)2(H2O)3·H2O: A layered metal phosphonate showing reversible dehydration–rehydration behavior and ferrimagnetism

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    Pengfei Wang, Deng‐Ke Cao, Song‐Song Bao, Haojun Jin, Yizhi Li, Tianwei Wang, Li‐Min Zheng

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  19. One-dimensional uranium–organic coordination polymers: crystal and electronic structures of uranyl-diacetohydroxamate

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  20. From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt

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  21. Uranyl carboxyphosphonates that incorporate Cd(II)

    Journal of Solid State Chemistry · 2011-04-14

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  22. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

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  23. Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates

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  24. Pillared and open-framework uranyl diphosphonates

    Journal of Solid State Chemistry · 2011-07-06

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  25. Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates

    Crystal Growth & Design · 2011-08-30

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  26. Uranyl–organic one- and two-dimensional assemblies with 2,2′-bipyridine-3,3′-dicarboxylic, biphenyl-3,3′,4,4′-tetracarboxylic and bicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acids

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  27. Synthesis, crystal structure and magnetic characterization of metal(II) coordination polymers based on 2-carboxyethylphosphonic acid and 1,10-phenanthroline (metal=Cu, Co, Cd)

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  28. Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril

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  29. Uranyl Sensitization of Samarium(III) Luminescence in a Two-Dimensional Coordination Polymer

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  30. Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties

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  31. Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties

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  32. Synthesis, crystal structures, and infrared spectroscopy of a series of lanthanide phosphonoacetate coordination polymers

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  33. Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures

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  34. Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O

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  35. Structural Study of Hydrated/Dehydrated Manganese Thiophene-2,5-diphosphonate Metal Organic Frameworks, Mn2(O3P–C4H2S–PO3)·2H2O

    Inorganic Chemistry · 2012-09-20

    Jean‐Michel Rueff, Olivier Pérez, Alain Pautrat, Nicolas Barrier, Gary B. Hix, Sylvie Hernot, Hélène Couthon‐Gourvès, Paul‐Alain Jaffrès

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  36. The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding

    Inorganic Chemistry · 2012-09-28

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  37. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

    Inorganic Chemistry · 2012-10-24

    Weiting Yang, Hongyue Wu, Run-Xue Wang, Qing‐Jiang Pan, Zhong‐Ming Sun, Hongjie Zhang

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  38. Uranium diphosphonates templated by interlayer organic amines

    Journal of Solid State Chemistry · 2012-10-24

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Thomas E. Albrecht‐Schmitt, Rodney Charles Ewing

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  39. Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate

    Inorganic Chemistry · 2012-12-07

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  40. Structural Observations of Heterometallic Uranyl Copper(II) Carboxylates and Their Solid‐State Topotactic Transformation upon Dehydration

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  41. One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids

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  42. Uranyl–3d block metal ion heterometallic carboxylate complexes including additional chelating nitrogen donors

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    P. Thuéry

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  43. Uranyl–copper(ii) heterometallic oxalate complexes: coordination polymers and frameworks

    Dalton Transactions · 2013-01-01

    P. Thuéry, Éric Rivière

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  44. Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies

    Inorganic Chemistry · 2013-02-21

    Weiting Yang, Tao Tian, Hongyue Wu, Qing‐Jiang Pan, Song Dang, Zhong‐Ming Sun

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  45. Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels

    Inorganic Chemistry · 2013-05-23

    Tao Tian, Weiting Yang, Hao Wang, Song Dang, Qing‐Jiang Pan, Zhong‐Ming Sun

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  46. Molecular Copper(II) Complexes Derived from Phosphonoacetic Acid: Crystal Structures and Magnetic Behavior

    European Journal of Inorganic Chemistry · 2013-06-03

    Franz Andreas Mautner, M.S. El Fallah, Olivier Roubeau, Saskia Speed, Simon J. Teat, Ramón Vicente

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  47. Use of Metalloligands [CuL] (H2L = Salen Type Di-Schiff Bases) in the Formation of Heterobimetallic Copper(II)-Uranyl Complexes: Photophysical Investigations, Structural Variations, and Theoretical Calculations

    Inorganic Chemistry · 2013-06-20

    Soumavo Ghosh, Saptarshi Biswas, Antonio Bauzá, Miquel Barceló‐Oliver, Antonio Frontera, Ashutosh Ghosh

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  48. The crystal chemistry of uranium carboxylates

    Coordination Chemistry Reviews · 2013-09-08

    Thierry Loiseau, Ionut Mihalcea, Natacha Henry, Christophe Volkringer

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  49. Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands

    European Journal of Inorganic Chemistry · 2013-11-25

    P. Thuéry

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  50. Chiral one- to three-dimensional uranyl–organic assemblies from (1R,3S)-(+)-camphoric acid

    CrystEngComm · 2014-01-01

    P. Thuéry, Jack McB. Harrowfield

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