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RESEARCH PAPER · Inorganic Chemistry · 1998

[pyH]2[Cu(py)4(MX6)2] (MX6 = ZrF62-, NbOF52-, MoO2F42-; py = Pyridine): Rarely Observed Ordering of Metal Oxide Fluoride Anions

Kevin R. Heier, Alexander J. Norquist, Christopher G. Wilson, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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[pyH]2[Cu(py)4(MX6)2] (MX6 = ZrF62-, NbOF52-, MoO2F42-; py = Pyridine): Rarely Observed Ordering of Metal Oxide Fluoride AnionsOriginalComposition Space Diagrams for Mixed Transition Metal Oxide Fluorides99The Polar [WO2F4]2- Anion in the Solid State65Cu(C10H9N3)2MOF5·2H2O (M = Nb, Ta): Aligned [MOF5]2- Oxide Fluoride Anions35Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster14The Structure-Directing Properties of [VOF5]2-66Polar Compounds Constructed with the [Cr2O7]2- Anion32Understanding the Role of Helical Chains in the Formation of Noncentrosymmetric Solids275The Ordered [WO2F4]2- Anion48From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds62Out-of-Center Distortions in d0 Transition Metal Oxide Fluoride Anions124Niobium and Tantalum7Zirconium and Hafnium6Synthesis, Crystal Structure, and Characterization of the First Nb3 Triangular Cluster Compound Bonded to Fluorine Ligands: Association of Nb3IiFi3Fa8La Units and NbIVL6 Octahedra with L = O and F4Alignment of acentric MoO3F33− anions in a polar material: (Ag3MoO3F3)(Ag3MoO4)Cl440Probing helix formation in chains of vertex-linked octahedra44Examining the Out-of-Center Distortion in the [NbOF5]2- Anion271Ag4V2O6F2: An Electrochemically Active and High Silver Density Phase84Catechol derivatives of Group 4 and 5 compounds51Synthesis and Characterization of the Face-Sharing Bioctahedral [Mo2O6F3]3- Anion23Diaquabis(1,10-phenanthroline-κ2N,N′)zinc(II) pentafluorooxoniobate(V)3Diaquabis(1,10-phenanthroline-κ2N,N′)cadmium(II) pentafluorooxoniobate(V)2Evidence for Nonpolar Alignment of [NbOF5]2- Anions in Cd(pyridine)4NbOF5 Chains24Phase transitions in oxyfluoride (NH4)2WO2F416Diaquabis(1,10-phenanthroline-κ2 N,N′)manganese(II) pentafluorooxoniobate(V)2Cluster chemistry in the solid state: Structured diffuse scattering, oxide/fluoride ordering and polar behaviour in transition metal oxyfluorides35Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis72Two Organically Templated Niobium and Zinconiobium Fluorophosphates: Low Temperature Hydrothermal Syntheses of NbOF(PO4)2(C2H10N2)2 and Zn3(NbOF)(PO4)4(C2H10N2)217Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O18[Mo16O53F2]12-: a New Polyoxofluoromolybdate Anion34Cation−Anion Interactions and Polar Structures in the Solid State196Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?0Orientational disorder and phase transitions in crystals of (NH4)2NbOF517Synthetic Approaches for Noncentrosymmetric Molybdates59Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F429Charge density matching in templated molybdates26Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions46Calorimetric and dielectric studies of the (NH4)2MoO2F4 oxyfluoride11Investigation of thermal expansion, phase diagrams, and barocaloric effect in the (NH4)2WO2F4 and (NH4)2MoO2F4 oxyfluorides55Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids34Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F416Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques8Alkali metal cation complexation and solvent interactions by robust chromium(III) fluoride complexes27Hydrothermal syntheses, crystal structures and characterizations of two new metal-fluorides based on niobium and tantalum19A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates8Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?129Intramolecular mobility and phase transitions in ammonium oxofluoroniobates (NH4)2NbOF5 and (NH4)3NbOF6, a NMR and DFT study20Hydrothermal synthesis, crystal structure and property of a barbell-like copper complex with {(μ-F)[(μ-O)2(NbF4)2]} as the handle bar4Mixed metalII–metalIV hybrid fluorides11Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates9“Fluoride molecular scissors”: A rational construction of new Mo(VI) oxofluorido/1,2,4-triazole MOFs16Synthesis, crystal and electronic structure, and theoretical investigations of charge-transfer, optical, and bonding properties of a [VF6]3− anion compound2Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks17Octahedral Rotation‐Induced Ferroelectricity in Cation Ordered Perovskites345Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Chemistry of Polar Transition-Metal Oxides1New series of hybrid fluoroferrates synthesized with triazoles: various dimensionalities and Mössbauer studies28Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)16Steric-Induced Layer Flection in Templated Vanadium Tellurites11Ba2YFeO5.5: A Ferromagnetic Pyroelectric Phase Prepared by Topochemical Oxidation.17Bonding and Structure of Oxofluoroniobate-Based Glasses7Self-assembly, geometric and electronic structures, and structure-directing properties of organic–inorganic hybrid salt containing [WO2F4]2− anions and protonated 2-(2-hydroxyphenyl)benzimidazole cations0catena-Poly[bis(μ-2,2′-bipyridin-6-olato)-κ3N,N′:O;O:N,N′-dicopper(I,II) [[tetrafluoridoniobium(V)]-μ-oxido]]3Tetrakis(pyridine-κN)bis(tetrafluoridoborato-κF)copper(II)0Unprecedented Trapping of Difluorooctamolybdate Anions within an α-Polonium Type Coordination Network13Alignment of Acentric Units in Infinite Chains: A “Lock and Key” Model16Synthesis and crystal structures of (pyH)2[Mo2O4F6] and (pipH2)[Mo2O4F6]; vibrational band assignment for [Mo2O4F6]2− anion4Role of Noncovalent Interactions in Vanadium Tellurite Chain Connectivities14Incipient spin–dipole coupling in a 1D helical-chain metal–organic hybrid5Variable Asymmetric Chains in Transition Metal Oxyfluorides: Structure–Second-Harmonic-Generation Property Relationships16An Asymmetric Anion‐Pillared Metal–Organic Framework as a Multisite Adsorbent Enables Simultaneous Removal of Propyne and Propadiene from Propylene107An Asymmetric Anion‐Pillared Metal–Organic Framework as a Multisite Adsorbent Enables Simultaneous Removal of Propyne and Propadiene from Propylene41A series of oxyfluoride chains containing asymmetric basic building units of both early- and late-transition metal cations5Red Phosphor Rb2NbOF5:Mn4+ for Warm White Light-Emitting Diodes with a High Color-Rendering Index77M 2 (SeO 3 )F 2 (M = Zn, Cd): understanding the structure directing effect of [SeO 3 ] 2− groups on constructing ordered oxyfluorides14Variable Chains Found in Mixed Transition Metal Oxyfluorides with Heterocyclic Ligands9Mixed Transition Metal (Oxy)fluoride Paramagnet Chains: Synthesis, Structure, and Characterization11Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph31A Potassium Tungsten Oxyfluoride with Strong Second-Harmonic Generation Response Derived from Anion-Ordered Functional Motif18Novel layered heterobimetallic fluorides with large optical band gaps3Chromium(VI) Oxyfluoride Dianions, [Cr2O4F6]2− and [CrO2F4]2−; Syntheses and Structures of [XeF5]2[Cr2O4F6], [XeF5]2[Cr2O4F6] ⋅ nX (X=HF, n=4; X=XeOF4, n=2), and [XeF5][Xe2F11][CrO2F4]1Targeting Oxide Concentration in Tantalum Oxide-Fluoride Anions0

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  1. Composition Space Diagrams for Mixed Transition Metal Oxide Fluorides

    Inorganic Chemistry · 1998-11-20

    Alexander J. Norquist, Kevin R. Heier, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  2. The Polar [WO2F4]2- Anion in the Solid State

    Inorganic Chemistry · 1999-02-02

    Kevin R. Heier, Alexander J. Norquist, P. Shiv Halasyamani, A. Duarte, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  3. Cu(C10H9N3)2MOF5·2H2O (M = Nb, Ta): Aligned [MOF5]2- Oxide Fluoride Anions

    Inorganic Chemistry · 1999-07-01

    Alexander J. Norquist, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  4. Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster

    Chemistry of Materials · 2000-06-16

    Alexander J. Norquist, Margaret E. Welk, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  5. The Structure-Directing Properties of [VOF5]2-

    Inorganic Chemistry · 2000-08-16

    Margaret E. Welk, Alexander J. Norquist, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  6. Polar Compounds Constructed with the [Cr2O7]2- Anion

    Inorganic Chemistry · 2001-03-16

    Alexander J. Norquist, Kevin R. Heier, P. Shiv Halasyamani, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  7. Understanding the Role of Helical Chains in the Formation of Noncentrosymmetric Solids

    Journal of the American Chemical Society · 2001-07-11

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  8. The Ordered [WO2F4]2- Anion

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    Margaret E. Welk, Alexander J. Norquist, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  9. From Linear Inorganic Chains to Helices: Chirality in the M(pyz)(H2O)2MoO2F4 (M = Zn, Cd) Compounds

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  10. Out-of-Center Distortions in d0 Transition Metal Oxide Fluoride Anions

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  11. Niobium and Tantalum

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  12. Zirconium and Hafnium

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  13. Synthesis, Crystal Structure, and Characterization of the First Nb3 Triangular Cluster Compound Bonded to Fluorine Ligands: Association of Nb3IiFi3Fa8La Units and NbIVL6 Octahedra with L = O and F

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    Stéphane Cordier, Olivier Hernandez, Jean‐Yves Thépot, Alex Shames, Christiane Perrin

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  14. Alignment of acentric MoO3F33− anions in a polar material: (Ag3MoO3F3)(Ag3MoO4)Cl

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  15. Probing helix formation in chains of vertex-linked octahedra

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  16. Examining the Out-of-Center Distortion in the [NbOF5]2- Anion

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    Heather K. Izumi, Janet E. Kirsch, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  17. Ag4V2O6F2: An Electrochemically Active and High Silver Density Phase

    Journal of the American Chemical Society · 2005-04-07

    Erin M. Sorensen, Heather K. Izumi, John T. Vaughey, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  18. Catechol derivatives of Group 4 and 5 compounds

    Polyhedron · 2005-05-25

    Timothy J. Boyle, Louis J. Tribby, Todd Michael Alam, S.D. Bunge, Gregory P. Holland

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  19. Synthesis and Characterization of the Face-Sharing Bioctahedral [Mo2O6F3]3- Anion

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  20. Diaquabis(1,10-phenanthroline-κ2N,N′)zinc(II) pentafluorooxoniobate(V)

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  21. Diaquabis(1,10-phenanthroline-κ2N,N′)cadmium(II) pentafluorooxoniobate(V)

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  22. Evidence for Nonpolar Alignment of [NbOF5]2- Anions in Cd(pyridine)4NbOF5 Chains

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  23. Phase transitions in oxyfluoride (NH4)2WO2F4

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  24. Diaquabis(1,10-phenanthroline-κ2 N,N′)manganese(II) pentafluorooxoniobate(V)

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  25. Cluster chemistry in the solid state: Structured diffuse scattering, oxide/fluoride ordering and polar behaviour in transition metal oxyfluorides

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  26. Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis

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  27. Two Organically Templated Niobium and Zinconiobium Fluorophosphates: Low Temperature Hydrothermal Syntheses of NbOF(PO4)2(C2H10N2)2 and Zn3(NbOF)(PO4)4(C2H10N2)2

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  28. Effects of Reaction Gel Dehydration on the Synthesis of Cu(NC5H5)4VOF4 and [Cu(NC5H5)4VOF4][Cu(NC5H5)4(H2O)VOF4]·H2O

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  29. [Mo16O53F2]12-: a New Polyoxofluoromolybdate Anion

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  30. Cation−Anion Interactions and Polar Structures in the Solid State

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  31. Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?

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  32. Orientational disorder and phase transitions in crystals of (NH4)2NbOF5

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  33. Synthetic Approaches for Noncentrosymmetric Molybdates

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  34. Disorder in crystals of dioxofluorotungstates, (NH4)2WO2F4 and Rb2WO2F4

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  35. Charge density matching in templated molybdates

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  36. Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions

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  37. Calorimetric and dielectric studies of the (NH4)2MoO2F4 oxyfluoride

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  38. Investigation of thermal expansion, phase diagrams, and barocaloric effect in the (NH4)2WO2F4 and (NH4)2MoO2F4 oxyfluorides

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  39. Microporosity, Optical Bandgap Sizes, and Photocatalytic Activity of M(I)-Nb(V) (M = Cu, Ag) Oxyfluoride Hybrids

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  40. Orientational disorder and phase transitions in crystals of dioxofluoromolybdate, (NH4)2MoO2F4

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  41. Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques

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  42. Alkali metal cation complexation and solvent interactions by robust chromium(III) fluoride complexes

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  43. Hydrothermal syntheses, crystal structures and characterizations of two new metal-fluorides based on niobium and tantalum

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  44. A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates

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  45. Multiferroic magnetoelectric fluorides: why are there so many magnetic ferroelectrics?

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  46. Intramolecular mobility and phase transitions in ammonium oxofluoroniobates (NH4)2NbOF5 and (NH4)3NbOF6, a NMR and DFT study

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  47. Hydrothermal synthesis, crystal structure and property of a barbell-like copper complex with {(μ-F)[(μ-O)2(NbF4)2]} as the handle bar

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  48. Mixed metalII–metalIV hybrid fluorides

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  49. Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates

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  50. “Fluoride molecular scissors”: A rational construction of new Mo(VI) oxofluorido/1,2,4-triazole MOFs

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