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RESEARCH PAPER · Inorganic Chemistry · 2008

Synthetic Approaches for Noncentrosymmetric Molybdates

Desmond J. Hubbard, Alexander R. Johnston, Hernan Sanchez Casalongue, Amy Narducci Sarjeant, Alexander J. Norquist

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Synthetic Approaches for Noncentrosymmetric MolybdatesOriginalNoncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?0ChemInform Abstract: Synthetic Approaches for Noncentrosymmetric Molybdates.0Charge density matching in templated molybdates26Simple Directed Material Design Through in Situ Substitution of Proton with Cu+ Ions1A Series of New Infrared NLO Semiconductors, ZnY6Si2S14, AlxDy3(SiyAl1−y)S7, and Al0.33Sm3SiS7134Noncentrosymmetry in New Templated Gallium Fluorophosphates34Novel Noncentrosymmetric Zinc Coordination Polymer Containing an Unusual Zinc Carboxylate−Sulfonate Substructure with a (10,3)-d Topology and Its Second-Harmonic-Generation Properties51How Does the Synthesis Temperature Impact Hybrid Organic−Inorganic Molybdate Material Design?39[R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers34Smart Heterostructures for Tailoring the Optical Properties of Photochromic Hybrid Organic–Inorganic Polyoxometalates61New organic–inorganic frameworks incorporating iso- and heteropolymolybdate units and a 3,3′,5,5′-tetramethyl-4,4′-bi-1H-pyrazole-2,2′-diium multiple hydrogen-bond donor4New Hybrid Layered Molybdates Based on 2/∞[MonO3n+1]2– Units (n = 7, 9) with Systematic Organic–Inorganic Interfaces20UV Nonlinear Optical Crystal Ba2[B6O9(OH)4] Featuring Unique Chiral Layers with a New B18O42 Circle Based on BO3 and BO4 Units97Tuning the Photochromic Properties of Molybdenum Bisphosphonate Polyoxometalates67Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks17Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)7Noncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)4Noncentrosymmetric Organic Solid and Its Zinc Coordination Polymer with Diamonded Network Prepared from an Ionothermal Reaction: Syntheses, Crystal Structures, and Second-Order Nonlinear Optics Properties58Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State21From Racemic Units to Polar Materials23Sulfonium Polyoxometalates: A New Class of Solid-State Photochromic Hybrid Organic–Inorganic Materials74Molybdenum-catalysed oxidation of cyclohexene with hydrogen peroxide in the presence of alcohols and X-ray structures of octamolybdate [C4mim]4[Mo8O26] and tetraperoxodimolybdate [Htmpy]2[{MoO(O2)2}2(μ-O)] complexes22Steric-Induced Layer Flection in Templated Vanadium Tellurites11Formation Principles for Templated Vanadium Selenite Oxalates22A Nitrate Nonlinear Optical Crystal Pb16(OH)16(NO3)16 with a Large Second-Harmonic Generation Response57F−/OH− substitution in [H4tren]4+ and [H3tren]3+ hydroxyfluorotitanates(IV) and classification of tren cation configurations11Formation Principles for Vanadium Selenites: The Role of pH on Product Composition12Metal(II)-Directed Various Polyoxometalates-Based Hybrid Compounds: Assembly, Structures and Properties5Role of Noncovalent Interactions in Vanadium Tellurite Chain Connectivities14Synthesis, Crystal Structure, and Properties of the Sodium Molybdate Fluoride Na3MoO4F5Syntheses, structures, and characterizations of a new second-order nonlinear optical material: Pb2(SeO3)(NO3)232The role of inorganic acidity on templated vanadate composition and dimensionality4Two octamolybdate-based hybrids functionalized by 1,3-bis[tris(hydroxymethyl)methylamino]propane ligand6Hydrothermal synthesis and structural characterization of an organically-templated open-framework trimolybdates1Probing structural adaptability in templated vanadium selenites8Composition Space Analysis in the Development of Copper Molybdate Hybrids Decorated by a Bifunctional Pyrazolyl/1,2,4-Triazole Ligand31Molybdenum-oxygen anionic chain grafted by Cu-phen complex. Synthesis, crystal structure and properties2Structure directing role of amines and water molecules in the self-assembly of polyoxomolybdates9Pb@Pb8 Basket-like-Cluster-Based Lead Tellurate–Nitrate Kleinman-Forbidden Nonlinear-Optical Crystal: Pb9Te2O13(OH)(NO3)326Understanding structural adaptability: a reactant informatics approach to experiment design12A Robust Framework Based on Polymeric Octamolybdate Anions and Copper(II) Complexes of Tetradentate N-donor Ligands13Syntheses, Structures, and Properties of Non-Centrosymmetric Quaternary Tellurates BiMTeO6 (M = Al, Ga)21Templated vanadium tellurites: Identifying the effects of low density attractions on inorganic layer topology4Synthesis, crystal structure and properties of a new noncentrosymmetric tetraoxidomolybdate(VI)3Machine-Learning-Assisted Synthesis of Polar Racemates32Rare example of chiral and achiral polymorphs of a metal-oxide/organic hybrid compound2Inorganic-organic crystalline synthetic bilayers consisting of polyoxomolybdate and double-chained surfactants4The crystal structure of catena-poly[bis[3-azoniapentane-1,5-diammonium][bis(μ4-oxo)-tetrakis(μ3-oxo)-heptakis(μ2-oxo)-tetradecaoxo-octa-molybdenum] dihydrate], (C8H36N6O29Mo8) n0Symmetry-Dependent Intermolecular π–π Stacking Directed by Hydrogen Bonding in Racemic Copper-Phenanthroline Compounds12Synthesis and Characterization of Ammonium Potassium Tellurium Polyoxomolybdate: (NH4)2K2TeMo6O22·2H2O with One-Dimensional Anionic Polymeric Chain [TeMo6O22]4−5Predicting inorganic dimensionality in templated metal oxides8Predicting compositional changes of organic–inorganic hybrid materials with Augmented CycleGAN4Recent progress in polyoxometalate–viologen photochromic hybrids: structural design, photochromic mechanism, and applications96Machine learning and experiments: A synergy for the development of functional materials19Investigation of the Ferroelectric, Magnetic and Magnetoelectric Properties in Honeycomb-Layered YCrTeO62Polyoxometalate (POM)-based crystalline hybrid photochromic materials104Regulating the Hydrodeoxygenation Activity of Molybdenum Carbide with Different Diamines as Carbon Sources8Structure Transformation of Methylammonium Polyoxomolybdates via In-Solution Acidification and Solid-State Heating from Methylammonium Monomolybdate and Application as Negative Staining Reagents for Coronavirus Observation6

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  1. Noncentrosymmetry in Mixed Metal Oxide-Fluorides, Can We Control It?

    MRS Proceedings · 2008-01-01

    Rachelle Ann F. Pinlac, Michael R. Marvel, Julien Lesage, Kenneth Reinhard Poeppelmeier

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  2. ChemInform Abstract: Synthetic Approaches for Noncentrosymmetric Molybdates.

    ChemInform · 2008-11-20

    Desmond J. Hubbard, Alexander R. Johnston, Hernan Sanchez Casalongue, Amy Narducci Sarjeant, Alexander J. Norquist

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  3. Charge density matching in templated molybdates

    Journal of Solid State Chemistry · 2009-03-07

    Hernan Sanchez Casalongue, Sarah J. Choyke, Amy Narducci Sarjeant, Joshua Schrier, Alexander J. Norquist

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  4. Simple Directed Material Design Through in Situ Substitution of Proton with Cu+ Ions

    Journal of Inorganic and Organometallic Polymers and Materials · 2009-06-08

    Qi‐Bing Bo, Zhong-Xi Sun, Guoxin Sun, Allan Holmgren

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  5. A Series of New Infrared NLO Semiconductors, ZnY6Si2S14, AlxDy3(SiyAl1−y)S7, and Al0.33Sm3SiS7

    Inorganic Chemistry · 2009-07-09

    Sheng‐Ping Guo, Guo‐Cong Guo, Ming‐Sheng Wang, Jian‐Ping Zou, Gang Xu, Guojian Wang, Xifa Long, Jin‐Shun Huang

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  6. Noncentrosymmetry in New Templated Gallium Fluorophosphates

    Inorganic Chemistry · 2009-10-28

    Sarah J. Choyke, Samuel M. Blau, A.A. Larner, Amy Narducci Sarjeant, Jeongho Yeon, P. Shiv Halasyamani, Alexander J. Norquist

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  7. Novel Noncentrosymmetric Zinc Coordination Polymer Containing an Unusual Zinc Carboxylate−Sulfonate Substructure with a (10,3)-d Topology and Its Second-Harmonic-Generation Properties

    Inorganic Chemistry · 2010-08-24

    Qing‐Yan Liu, Yu‐Ling Wang, Zeng-Mei Shan, Rong Cao, Yun-Liang Jiang, Zujian Wang, Er-Lei Yang

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  8. How Does the Synthesis Temperature Impact Hybrid Organic−Inorganic Molybdate Material Design?

    Inorganic Chemistry · 2010-11-16

    Rémi Dessapt, D. Kervern, Martine Bujoli‐Doeuff, Philippe Deniard, M. Evain, Stéphane Jobic

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  9. [R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers

    Journal of Solid State Chemistry · 2011-04-20

    Ethan C. Glor, Samuel M. Blau, Jeongho Yeon, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

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  10. Smart Heterostructures for Tailoring the Optical Properties of Photochromic Hybrid Organic–Inorganic Polyoxometalates

    Inorganic Chemistry · 2011-08-22

    Rémi Dessapt, Marie Gabard, Martine Bujoli‐Doeuff, Philippe Deniard, Stéphane Jobic

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  11. New organic–inorganic frameworks incorporating iso- and heteropolymolybdate units and a 3,3′,5,5′-tetramethyl-4,4′-bi-1H-pyrazole-2,2′-diium multiple hydrogen-bond donor

    Acta Crystallographica Section C Crystal Structure Communications · 2011-11-16

    Liliana Lukashuk, A.B. Lysenko, Harald Krautscheid, K.V. Domasevitch

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  12. New Hybrid Layered Molybdates Based on 2/∞[MonO3n+1]2– Units (n = 7, 9) with Systematic Organic–Inorganic Interfaces

    Inorganic Chemistry · 2011-12-15

    Martine Bujoli‐Doeuff, Rémi Dessapt, Philippe Deniard, Stéphane Jobic

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  13. UV Nonlinear Optical Crystal Ba2[B6O9(OH)4] Featuring Unique Chiral Layers with a New B18O42 Circle Based on BO3 and BO4 Units

    Inorganic Chemistry · 2012-01-19

    Li Wang, Shilie Pan, Li‐Xian Chang, Jianyang Hu, Hongwei Yu

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  14. Tuning the Photochromic Properties of Molybdenum Bisphosphonate Polyoxometalates

    Inorganic Chemistry · 2012-01-27

    Hani El Moll, Anne Dolbecq, Israel Martyr Mbomekalle, Jérôme Marrot, Philippe Deniard, Rémi Dessapt, Pierre Mialane

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  15. Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks

    Journal of Solid State Chemistry · 2012-02-21

    Matthew D. Smith, Samuel M. Blau, Kelvin B. Chang, T. Thao Tran, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

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  16. Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)

    Journal of Solid State Chemistry · 2012-02-24

    Maren Rasmussen, Christian Näther, Ulrich Bismayer, Wolfgang Bensch

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  17. Noncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)

    Journal of Coordination Chemistry · 2012-03-13

    Houcine Naı̈li

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  18. Noncentrosymmetric Organic Solid and Its Zinc Coordination Polymer with Diamonded Network Prepared from an Ionothermal Reaction: Syntheses, Crystal Structures, and Second-Order Nonlinear Optics Properties

    Crystal Growth & Design · 2012-08-16

    Yu‐Ling Wang, Jiang-Hong Fu, Jiajia Wei, Xiang Xu, Xinfa Li, Qing‐Yan Liu

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  19. Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks

    Inorganic Chemistry · 2012-09-24

    Jacob H. Olshansky, T. Thao Tran, Kristen J. Hernandez, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

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  20. Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State

    Inorganic Chemistry · 2012-09-27

    Romain Gautier, Kenneth Reinhard Poeppelmeier

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  21. From Racemic Units to Polar Materials

    Crystal Growth & Design · 2012-11-06

    Romain Gautier, Alexander J. Norquist, Kenneth Reinhard Poeppelmeier

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  22. Sulfonium Polyoxometalates: A New Class of Solid-State Photochromic Hybrid Organic–Inorganic Materials

    Inorganic Chemistry · 2013-01-08

    Khadija Hakouk, Olivier Oms, Anne Dolbecq, Hani El Moll, Jérôme Marrot, M. Evain, Florian Molton, Carole Duboc, Philippe Deniard, Stéphane Jobic, Pierre Mialane, Rémi Dessapt

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  23. Molybdenum-catalysed oxidation of cyclohexene with hydrogen peroxide in the presence of alcohols and X-ray structures of octamolybdate [C4mim]4[Mo8O26] and tetraperoxodimolybdate [Htmpy]2[{MoO(O2)2}2(μ-O)] complexes

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  24. Steric-Induced Layer Flection in Templated Vanadium Tellurites

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  25. Formation Principles for Templated Vanadium Selenite Oxalates

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  26. A Nitrate Nonlinear Optical Crystal Pb16(OH)16(NO3)16 with a Large Second-Harmonic Generation Response

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  27. F−/OH− substitution in [H4tren]4+ and [H3tren]3+ hydroxyfluorotitanates(IV) and classification of tren cation configurations

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    Jérôme Lhoste, Monique Body, Christophe Legein, Annie Hémon‐Ribaud, M. Leblanc, V. Maisonneuve

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  28. Formation Principles for Vanadium Selenites: The Role of pH on Product Composition

    Inorganic Chemistry · 2014-11-03

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  29. Metal(II)-Directed Various Polyoxometalates-Based Hybrid Compounds: Assembly, Structures and Properties

    Journal of Inorganic and Organometallic Polymers and Materials · 2014-12-16

    Xiuli Wang, Danna Liu, Hong‐Yan Lin, Na Han, Guo‐Cheng Liu

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  30. Role of Noncovalent Interactions in Vanadium Tellurite Chain Connectivities

    Inorganic Chemistry · 2015-01-08

    Anahita Nourmahnad, Matthew D. Smith, Mat­thias Zeller, Gregory M. Ferrence, Joshua Schrier, Alexander J. Norquist

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  31. Synthesis, Crystal Structure, and Properties of the Sodium Molybdate Fluoride Na3MoO4F

    Zeitschrift für anorganische und allgemeine Chemie · 2015-03-20

    Xiangyu Zhang, Danni Li, Zhihua Yang, Hongping Wu, Shilie Pan

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  32. Syntheses, structures, and characterizations of a new second-order nonlinear optical material: Pb2(SeO3)(NO3)2

    Journal of Alloys and Compounds · 2015-04-11

    Chang‐Yu Meng, Lei Geng, Wenting Chen, Ming‐Fang Wei, Kai Dai, Hong‐Yan Lu, Wen‐Dan Cheng

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  33. The role of inorganic acidity on templated vanadate composition and dimensionality

    Journal of Solid State Chemistry · 2015-08-06

    Anahita Nourmahnad, Malia B. Wenny, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  34. Two octamolybdate-based hybrids functionalized by 1,3-bis[tris(hydroxymethyl)methylamino]propane ligand

    Inorganic Chemistry Communications · 2015-09-03

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  35. Hydrothermal synthesis and structural characterization of an organically-templated open-framework trimolybdates

    International Journal of the Physical Sciences · 2015-10-16

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  36. Probing structural adaptability in templated vanadium selenites

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  37. Composition Space Analysis in the Development of Copper Molybdate Hybrids Decorated by a Bifunctional Pyrazolyl/1,2,4-Triazole Ligand

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    A.B. Lysenko, Ganna A. Senchyk, Liliana Lukashuk, K.V. Domasevitch, Marcel Handke, Jörg Lincke, Harald Krautscheid, Eduard B. Rusanov, Karl W. Krämer, Silvio Decurtins, Shi‐Xia Liu

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  38. Molybdenum-oxygen anionic chain grafted by Cu-phen complex. Synthesis, crystal structure and properties

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  39. Structure directing role of amines and water molecules in the self-assembly of polyoxomolybdates

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  40. Pb@Pb8 Basket-like-Cluster-Based Lead Tellurate–Nitrate Kleinman-Forbidden Nonlinear-Optical Crystal: Pb9Te2O13(OH)(NO3)3

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  41. Understanding structural adaptability: a reactant informatics approach to experiment design

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  42. A Robust Framework Based on Polymeric Octamolybdate Anions and Copper(II) Complexes of Tetradentate N-donor Ligands

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  43. Syntheses, Structures, and Properties of Non-Centrosymmetric Quaternary Tellurates BiMTeO6 (M = Al, Ga)

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  44. Templated vanadium tellurites: Identifying the effects of low density attractions on inorganic layer topology

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  45. Synthesis, crystal structure and properties of a new noncentrosymmetric tetraoxidomolybdate(VI)

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  46. Machine-Learning-Assisted Synthesis of Polar Racemates

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  47. Rare example of chiral and achiral polymorphs of a metal-oxide/organic hybrid compound

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  48. Inorganic-organic crystalline synthetic bilayers consisting of polyoxomolybdate and double-chained surfactants

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  49. The crystal structure of catena-poly[bis[3-azoniapentane-1,5-diammonium][bis(μ4-oxo)-tetrakis(μ3-oxo)-heptakis(μ2-oxo)-tetradecaoxo-octa-molybdenum] dihydrate], (C8H36N6O29Mo8) n

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  50. Symmetry-Dependent Intermolecular π–π Stacking Directed by Hydrogen Bonding in Racemic Copper-Phenanthroline Compounds

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