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RESEARCH PAPER · Inorganic Chemistry · 2006

Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis

Thomas R. Veltman, Adam K. Stover, Amy Narducci Sarjeant, Kang Min Ok, P. Shiv Halasyamani, Alexander J. Norquist

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Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space AnalysisOriginalPoly[tetrakis(4-aminopyridinium) [hexadeca-μ-oxo-decaoxooctamolybdate(VI)]]5Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane39Synthesis, Characterization, and Photochromic Properties of Hybrid Organic−Inorganic Materials Based on Molybdate, DABCO, and Piperazine137Composition space analysis of templated molybdates25Poly[tris(p-xylylenediaminium) [tetradeca-μ-oxo-hexadecanonamolybdate(VI)] dihydrate]5[Mo16O53F2]12-: a New Polyoxofluoromolybdate Anion34Construction of different dimensional inorganic–organic hybrid materials based on polyoxometalates and metal–organic units via changing metal ions: from non-covalent interactions to covalent connections75Synthetic Approaches for Noncentrosymmetric Molybdates59A new supramolecular compound based on MnIII-Schiff-base and β-octamolybdate26Charge density matching in templated molybdates26Second-Order Nonlinear Optical Properties of Polyoxometalate Salts of a Chiral Stilbazolium Derivative67Hydrothermal Syntheses and Structural Characterizations of Polyoxometalate (Mo/W) Compounds Consisting of M-L Cations, (M = Mn, Co, Ni, Cu, Zn; L = 3-(2-Pyridyl)pyrazole)48Influence of the steric hindrance of organic amines on the supramolecular network based on polyoxovanadates26Noncentrosymmetry in New Templated Gallium Fluorophosphates34New synthetic route of polyoxometalate-based hybrids in choline chloride/urea eutectic media31The Role of Stereoactive Lone Pairs in Templated Vanadium Tellurite Charge Density Matching21Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques8A series of new supramolecular structures constructed from triethylenediamine and different polyoxometalates12How Does the Synthesis Temperature Impact Hybrid Organic−Inorganic Molybdate Material Design?39Three novel supramolecular hybrid compounds based on keggin polytungstates16Two new hybrid compounds assembled from Keggin-type polyoxometalates and transition metal coordination complexes12Four New Compounds Constructed from Bis‐Antimony‐Capped Keggin Polyoxoanions {PMo12Sb2O40} and Different Coordination Fragments30Top-Seeded Solution Growth, Morphology, and Properties of a Polar Crystal Cs2TeMo3O1277[R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers34Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates9Beyond Charge Density Matching: The Role of C–H···O Interactions in the Formation of Templated Vanadium Tellurites16Two multi-dimensional frameworks constructed from zinc coordination polymers with pyridine carboxylic acids8New compounds constructed from polyoxometalates and transition metal coordination complexes with lower positive charge38Synthesis, crystal structures and thermal behaviour of organic–inorganic hybrids incorporating a chiral diamine19New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)50New Hybrid Layered Molybdates Based on 2/∞[MonO3n+1]2– Units (n = 7, 9) with Systematic Organic–Inorganic Interfaces20Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)50Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks17Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)7Syntheses and structural characterization of four new organic–inorganic hybrid compounds based on bicapped Keggin polyoxometalate {PMo12Sb2O40}9Noncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)4Salt-flux synthesis of complex oxides: Cs0.33MoO3, CsFe(MoO4)2, and the inverse salt-inclusion phase Cs2Mo0.65O0.21Cl5.449Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State21Chiral polyoxometalate-based materials: From design syntheses to functional applications235From Racemic Units to Polar Materials23Chemistry of Polar Transition-Metal Oxides1Nonlinear Optical Properties of Coordination and Organometallic Complexes28New compounds constructed from bi-antimony capped Keggin polyoxoanions and different coordination fragments7Steric-Induced Layer Flection in Templated Vanadium Tellurites11New compounds based on polyoxometalates and transition metal complexes with a lower positive charge10The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior3Formation Principles for Templated Vanadium Selenite Oxalates22Two novel organic–inorganic hybrid molybdenum( v ) cobalt/nickel phosphate compounds based on isolated nanosized Mo/Co(Ni)/P cluster wheels40Formation Principles for Vanadium Selenites: The Role of pH on Product Composition12Flux crystal growth of Ba2TiOSi2O728Role of Noncovalent Interactions in Vanadium Tellurite Chain Connectivities14The role of inorganic acidity on templated vanadate composition and dimensionality4Probing structural adaptability in templated vanadium selenites8Spontaneous Resolution of Evans–Showell-Type Polyoxometalates in Constructing Chiral Inorganic–Organic Hybrid Architectures33Chiral polyoxomolybdate-based hybrid compounds obtained by spontaneous resolution: syntheses, structures and non-linear optical properties10Two octamolybdate-based coordination polymers with high photocatalytic activities under visible light irradiation2Understanding structural adaptability: a reactant informatics approach to experiment design12Anderson-Type Polyoxometalates Functionalized by Tetrathiafulvalene Groups: Synthesis, Electrochemical Studies, and NLO Properties51Syntheses, Structures, and Properties of Non-Centrosymmetric Quaternary Tellurates BiMTeO6 (M = Al, Ga)21Bi2ZnOB2O6: a polar material capable of photocatalytic degradation of Rhodamine B14Synthèse de polyoxométallates hybrides et étude de leurs propriétés en biologie et en optique0Synthesis, crystal structures, second harmonic generation response and temperature phase transitions of two noncentrosymmetric Cu(II)-hybrid halides compounds: [(R)-C7H16N2][CuX4] (X = Cl or Br)25Templated vanadium tellurites: Identifying the effects of low density attractions on inorganic layer topology4Synthesis, crystal structure and properties of a new noncentrosymmetric tetraoxidomolybdate(VI)3Machine-Learning-Assisted Synthesis of Polar Racemates32Symmetry-Dependent Intermolecular π–π Stacking Directed by Hydrogen Bonding in Racemic Copper-Phenanthroline Compounds12Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship24Crystalline Porous Materials for Nonlinear Optics91Anion-π stacks of Lindqvist superoctahedra [Mo6O19]2− supported by caffeinium and theophyllinium cations5Exploration of new chiral hybrid semiconducting palladium halide complexes: [(R)/(S)-2-Methylpiperazinediium]PdCl49Investigation of the Ferroelectric, Magnetic and Magnetoelectric Properties in Honeycomb-Layered YCrTeO62

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  1. Poly[tetrakis(4-aminopyridinium) [hexadeca-μ-oxo-decaoxooctamolybdate(VI)]]

    Acta Crystallographica Section E Structure Reports Online · 2006-07-06

    James R. Nelson, Amy Narducci Sarjeant, Alexander J. Norquist

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  2. Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane

    New Journal of Chemistry · 2006-11-24

    R. Atencio, Alexander Briceño, Pedro J. Silva, José A. Rodríguez, Jonathan C. Hanson

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  3. Synthesis, Characterization, and Photochromic Properties of Hybrid Organic−Inorganic Materials Based on Molybdate, DABCO, and Piperazine

    Inorganic Chemistry · 2007-02-27

    Violaine Coué, Rémi Dessapt, Martine Bujoli‐Doeuff, M. Evain, Stéphane Jobic

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  4. Composition space analysis of templated molybdates

    Solid State Sciences · 2007-04-11

    J.H. Nelson, Alexander R. Johnston, Amy Narducci Sarjeant, Alexander J. Norquist

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  5. Poly[tris(p-xylylenediaminium) [tetradeca-μ-oxo-hexadecanonamolybdate(VI)] dihydrate]

    Acta Crystallographica Section E Structure Reports Online · 2007-04-25

    J.H. Nelson, Amy Narducci Sarjeant, Alexander J. Norquist

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  6. [Mo16O53F2]12-: a New Polyoxofluoromolybdate Anion

    Inorganic Chemistry · 2007-05-01

    Adam K. Stover, Jesse Gutnick, Amy Narducci Sarjeant, Alexander J. Norquist

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  7. Construction of different dimensional inorganic–organic hybrid materials based on polyoxometalates and metal–organic units via changing metal ions: from non-covalent interactions to covalent connections

    Dalton Transactions · 2008-01-01

    Ya‐Qian Lan, Shun‐Li Li, Kui‐Zhan Shao, Xinlong Wang, Zhong‐Min Su

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  8. Synthetic Approaches for Noncentrosymmetric Molybdates

    Inorganic Chemistry · 2008-09-29

    Desmond J. Hubbard, Alexander R. Johnston, Hernan Sanchez Casalongue, Amy Narducci Sarjeant, Alexander J. Norquist

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  9. A new supramolecular compound based on MnIII-Schiff-base and β-octamolybdate

    Inorganic Chemistry Communications · 2008-12-04

    Yun‐Wu Li, Yonghui Wang, Yangguang Li, Enbo Wang

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  10. Charge density matching in templated molybdates

    Journal of Solid State Chemistry · 2009-03-07

    Hernan Sanchez Casalongue, Sarah J. Choyke, Amy Narducci Sarjeant, Joshua Schrier, Alexander J. Norquist

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  11. Second-Order Nonlinear Optical Properties of Polyoxometalate Salts of a Chiral Stilbazolium Derivative

    Inorganic Chemistry · 2009-05-29

    Jean‐Daniel Compain, Pierre Mialane, Anne Dolbecq, Jérôme Marrot, Anna Proust, Keitaro Nakatani, Pei Yu, F. Sécheresse

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  12. Hydrothermal Syntheses and Structural Characterizations of Polyoxometalate (Mo/W) Compounds Consisting of M-L Cations, (M = Mn, Co, Ni, Cu, Zn; L = 3-(2-Pyridyl)pyrazole)

    Crystal Growth & Design · 2009-08-31

    Xiutang Zhang, Peihai Wei, Daofeng Sun, Zhong‐Hai Ni, Jianmin Dou, Bin Li, Congwen Shi, Bo Hu

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  13. Influence of the steric hindrance of organic amines on the supramolecular network based on polyoxovanadates

    CrystEngComm · 2009-09-05

    Zhihui Yi, Xiao‐Yang Yu, Wujiong Xia, Liyan Zhao, Chao Yang, Chen Qian, Xiaolin Wang, Xianzhu Xu, Xiao Zhang

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  14. Noncentrosymmetry in New Templated Gallium Fluorophosphates

    Inorganic Chemistry · 2009-10-28

    Sarah J. Choyke, Samuel M. Blau, A.A. Larner, Amy Narducci Sarjeant, Jeongho Yeon, P. Shiv Halasyamani, Alexander J. Norquist

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  15. New synthetic route of polyoxometalate-based hybrids in choline chloride/urea eutectic media

    Inorganica Chimica Acta · 2009-12-18

    Shi-Ming Wang, Yun‐Wu Li, Yun‐Wu Li, Xiao‐Jia Feng, Yangguang Li, Yangguang Li, Enbo Wang

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  16. The Role of Stereoactive Lone Pairs in Templated Vanadium Tellurite Charge Density Matching

    Inorganic Chemistry · 2010-05-11

    Kelvin B. Chang, Desmond J. Hubbard, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  17. Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques

    Unknown journal · 2010-06-11

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  18. A series of new supramolecular structures constructed from triethylenediamine and different polyoxometalates

    Journal of Solid State Chemistry · 2010-10-02

    Yan Wang, Cheng‐Ling Pan, Li‐Na Xiao, Fengqing Wu, Hong Yan Ding, Yabing Liu, Zhong‐Min Gao, Dafang Zheng, Tie‐Gang Wang, Guangdi Yang, Xiao‐Bing Cui, Ji‐Qing Xu

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  19. How Does the Synthesis Temperature Impact Hybrid Organic−Inorganic Molybdate Material Design?

    Inorganic Chemistry · 2010-11-16

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  20. Three novel supramolecular hybrid compounds based on keggin polytungstates

    CrystEngComm · 2011-01-01

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  21. Two new hybrid compounds assembled from Keggin-type polyoxometalates and transition metal coordination complexes

    Journal of Solid State Chemistry · 2011-01-18

    Yan Wang, Bo Zou, Li‐Na Xiao, Ning Jin, Yu Peng, Fengqing Wu, Hong Yan Ding, Tie‐Gang Wang, Zhong‐Min Gao, Dafang Zheng, Xiao‐Bing Cui, Ji‐Qing Xu

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  22. Four New Compounds Constructed from Bis‐Antimony‐Capped Keggin Polyoxoanions {PMo12Sb2O40} and Different Coordination Fragments

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  23. Top-Seeded Solution Growth, Morphology, and Properties of a Polar Crystal Cs2TeMo3O12

    Crystal Growth & Design · 2011-03-25

    Junjie Zhang, Xutang Tao, Youxuan Sun, Zhonghan Zhang, Chengqian Zhang, Zeliang Gao, Haibing Xia, Sheng‐Qing Xia

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  24. [R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers

    Journal of Solid State Chemistry · 2011-04-20

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  25. Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates

    Crystal Growth & Design · 2011-05-04

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  26. Beyond Charge Density Matching: The Role of C–H···O Interactions in the Formation of Templated Vanadium Tellurites

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  27. Two multi-dimensional frameworks constructed from zinc coordination polymers with pyridine carboxylic acids

    Journal of Solid State Chemistry · 2011-10-08

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  28. New compounds constructed from polyoxometalates and transition metal coordination complexes with lower positive charge

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  29. Synthesis, crystal structures and thermal behaviour of organic–inorganic hybrids incorporating a chiral diamine

    Journal of Organometallic Chemistry · 2011-12-01

    Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Alexander J. Norquist, Tahar Mhiri, Thierry Bataille

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  30. New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)

    Inorganic Chemistry · 2011-12-06

    Jeongho Yeon, Sang‐Hwan Kim, Sau Doan Nguyen, Hana Lee, P. Shiv Halasyamani

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  31. New Hybrid Layered Molybdates Based on 2/∞[MonO3n+1]2– Units (n = 7, 9) with Systematic Organic–Inorganic Interfaces

    Inorganic Chemistry · 2011-12-15

    Martine Bujoli‐Doeuff, Rémi Dessapt, Philippe Deniard, Stéphane Jobic

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  32. Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)

    Inorganic Chemistry · 2012-02-01

    Jeongho Yeon, Sang‐Hwan Kim, Sau Doan Nguyen, Hana Lee, P. Shiv Halasyamani

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  33. Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks

    Journal of Solid State Chemistry · 2012-02-21

    Matthew D. Smith, Samuel M. Blau, Kelvin B. Chang, T. Thao Tran, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

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  34. Small non-polar complexes exhibiting significant piezoelectric properties: Solvothermal synthesis and crystal structures of MO5V(tren)·H2O (M=Mo and W; tren=tris(2-aminoethyl)amine)

    Journal of Solid State Chemistry · 2012-02-24

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  35. Syntheses and structural characterization of four new organic–inorganic hybrid compounds based on bicapped Keggin polyoxometalate {PMo12Sb2O40}

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    Li‐Na Xiao, Yu-Jiao qin, Shu-Yun Shi, Jianing Xu, Yan Wang, Yu Peng, La-Mei Wang, Yang‐Yang Hu, Tie‐Gang Wang, Zhong‐Min Gao, Dafang Zheng, Xiao‐Bing Cui, Ji‐Qing Xu

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  36. Noncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)

    Journal of Coordination Chemistry · 2012-03-13

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  37. Salt-flux synthesis of complex oxides: Cs0.33MoO3, CsFe(MoO4)2, and the inverse salt-inclusion phase Cs2Mo0.65O0.21Cl5.44

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  38. Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks

    Inorganic Chemistry · 2012-09-24

    Jacob H. Olshansky, T. Thao Tran, Kristen J. Hernandez, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

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  39. Preservation of Chirality and Polarity between Chiral and Polar Building Units in the Solid State

    Inorganic Chemistry · 2012-09-27

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  40. Chiral polyoxometalate-based materials: From design syntheses to functional applications

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    Dong‐Ying Du, Li‐Kai Yan, Zhong‐Min Su, Shun‐Li Li, Ya‐Qian Lan, Enbo Wang

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  41. From Racemic Units to Polar Materials

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  42. Chemistry of Polar Transition-Metal Oxides

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  43. Nonlinear Optical Properties of Coordination and Organometallic Complexes

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  44. New compounds constructed from bi-antimony capped Keggin polyoxoanions and different coordination fragments

    Inorganica Chimica Acta · 2013-02-08

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  45. Steric-Induced Layer Flection in Templated Vanadium Tellurites

    Crystal Growth & Design · 2013-04-02

    Kelvin B. Chang, Matthew D. Smith, Samuel M. Blau, Ethan C. Glor, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  46. New compounds based on polyoxometalates and transition metal complexes with a lower positive charge

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  47. The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior

    Phase Transitions · 2013-05-23

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  48. Formation Principles for Templated Vanadium Selenite Oxalates

    Crystal Growth & Design · 2013-08-08

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  49. Two novel organic–inorganic hybrid molybdenum( v ) cobalt/nickel phosphate compounds based on isolated nanosized Mo/Co(Ni)/P cluster wheels

    Journal of Materials Chemistry C · 2014-01-01

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  50. Formation Principles for Vanadium Selenites: The Role of pH on Product Composition

    Inorganic Chemistry · 2014-11-03

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