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RESEARCH PAPER · Journal of the American Chemical Society · 1999

From Molecules to Frameworks: Variable Dimensionality in the UO2(CH3COO)2·2H2O/HF(aq)/Piperazine System. Syntheses, Structures, and Characterization of Zero-Dimensional (C4N2H12)UO2F4·3H2O, One-Dimensional (C4N2H12)2U2F12·H2O, Two-Dimensional (C4N2H12)2(U2O4F5)4·11H2O, and Three-Dimensional (C4N2H12)U2O4F6

Susan M. Walker, P. Shiv Halasyamani, S. J. Allen, Dermot O’Hare

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From Molecules to Frameworks: Variable Dimensionality in the UO2(CH3COO)2·2H2O/HF(aq)/Piperazine System. Syntheses, Structures, and Characterization of Zero-Dimensional (C4N2H12)UO2F4·3H2O, One-Dimensional (C4N2H12)2U2F12·H2O, Two-Dimensional (C4N2H12)2(U2O4F5)4·11H2O, and Three-Dimensional (C4N2H12)U2O4F6Original17 Scandium, yttrium, the lanthanides, the actinides and the post-actinides2Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster14Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride63Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties67Molecular and electronic structure of AnIVFeII(CN)6·xH2O (An = Th, U, Np) compounds: an X-ray absorption spectroscopy investigation13Synthesis and characterisation of (C4N2H12)(UO2)2(PO3H)2{PO2(OH)H}2: a three dimensionally connected actinide framework46Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]44Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions115Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F3143Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O22Solvent Effects on Uranium(VI) Fluoride and Hydroxide Complexes Studied by EXAFS and Quantum Chemistry146Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)73Crystal structure of new hydroxide fluorides with isolated F− anions: [H3N(CH2)6NH3]2M(F, OH)6(F,OH)·H2O (M = Al, In)18A New Oxoanion: [IO4]3-Containing I(V) with a Stereochemically Active Lone-Pair in the Silver Uranyl Iodate Tetraoxoiodate(V), Ag4(UO2)4(IO3)2(IO4)2O282Hydrothermal synthesis of the first organically templated open-framework uranium phosphate66Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)53Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides8[NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structure102The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O29Structural and NMR studies of the series of related [H3N(CH2)xNH3]·AlF5 (x=6, 8, 10, 12) hybrid compounds12Organically templated uranium(vi) sulfates: understanding phase stability using composition space83Incorporation of uranium( vi ) into metal–organic framework solids, [UO 2 (C 4 H 4 O 4 )]·H 2 O, [UO 2 F(C 5 H 6 O 4 )]·2H 2 O, and [(UO 2 ) 1.5 (C 8 H 4 O 4 ) 2 ] 2 [(CH 3 ) 2 NCOH 2 ]·H 2 O98The Actinides34Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates56The effects of linear diamine chain length in uranium sulfates48[(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework852D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties78Characterisation of Four New Two‐Dimensional Lithium Beryllofluoro‐Layered Compounds20[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates40Tris(2-ethylamino)amine (tren) as template for the elaboration of fluorides: synthesis and crystal structures of [(C2H4NH3)3NH]·[Zr3F16(H2O)], [(C2H4NH3)3N]2·[ZrF6]·[Zr2F12] and [(C2H4NH3)3N]·[TaF7]·F26[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Structural variation in organically templated uranium sulfate fluorides42Uranyl Complexation in Fluorinated Acids (HF, HBF4, HPF6, HTf2N): A Combined Experimental and Theoretical Study38(C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type14Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51Synthesis, Structure and Photoluminescent Studies of Two Novel Layered Uranium Coordination Polymers Constructed from UO(OH) Polyhedra and Pyridinedicarboxylates79[N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)38UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O40Two-dimensional composition diagram of the Al(OH)3-dien-HFaq.-ethanol system: Evidence of a new tetrahedral (Al4F18)6− polyanion16Product evolution in the Np(IV) fluorophosphate system15Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]17Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate75[(CH3)2NH(CH2)2NH(CH3)2][(UO2)2F2(HPO4)2]: a new organically templated layered uranium phosphate fluoride - synthesis, structure, characterization, and ion-exchange reactions9Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides41U(VI)-containing metal-organic frameworks and coordination polymers14[H4tren]3/2·(Al6F24)·3H2O, the most condensed fluoride in the Al(OH)3-tren-HFaq.-ethanol system14Uranyl Coordination in Ionic Liquids: The Competition between Ionic Liquid Anions, Uranyl Counterions, and Cl- Anions Investigated by Extended X-ray Absorption Fine Structure and UV−Visible Spectroscopies and Molecular Dynamics Simulations87One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O2Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families46The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands40Oxo ligand functionalization in the uranyl ion (UO22+)335Time- and Temperature-Dependent Study in the Three-Component Zinc-Triazolate-Oxybis(benzoate) System: Stabilization of New Topologies57Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds45Structural chemistry of organically-templated metal fluorides61Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18[H3tren]3+ and [H4tren]4+ fluoride zirconates or tantalates73-Fold-Interpenetrated Uranium–Organic Frameworks: New Strategy for Rationally Constructing Three-Dimensional Uranyl Organic Materials76The adsorption characteristics of uranium hexafluoride onto activated carbon in vacuum conditions11Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O15From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Changes in the Structural Dimensionality of Selenidostannates in Ionic Liquids: Formation, Structures, Stability, and Photoconductivity50MOFs of Uranium and the Actinides95Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Hydrothermal assembly of various dimensional pure-inorganic copper–molybdenum frameworks6Insight into the Uranyl Oxyfluoride Topologies through the Synthesis, Crystal Structure, and Evidence of a New Oxyfluoride Layer in [(UO2)4F13][Sr3(H2O)8](NO3)·H2O6Formation and distortion of iodidoantimonates(III): the first isolated [SbI6]3−octahedron8Anionic uranyl oxyfluorides as a bifunctional platform for highly selective ion-exchange and photocatalytic degradation of organic dyes13Graphdiyne-actinyl complexes as potential catalytic materials: A DFT perspective from their structural, bonding, electronic and redox properties6Three-dimensional metal-halide open frameworks56Features of Uranium Stereochemistry in Uranyl Oxofluorides6Structural chemistry of fluoride complexes of uranyl8

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  1. 17 Scandium, yttrium, the lanthanides, the actinides and the post-actinides

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  2. Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster

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  3. Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride

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  4. Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties

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  5. Molecular and electronic structure of AnIVFeII(CN)6·xH2O (An = Th, U, Np) compounds: an X-ray absorption spectroscopy investigation

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  6. Synthesis and characterisation of (C4N2H12)(UO2)2(PO3H)2{PO2(OH)H}2: a three dimensionally connected actinide framework

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  7. Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]

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  8. Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions

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  9. Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31

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  10. Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O

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  11. Solvent Effects on Uranium(VI) Fluoride and Hydroxide Complexes Studied by EXAFS and Quantum Chemistry

    Inorganic Chemistry · 2001-06-07

    Valérie Vallet, Ulf Wahlgren, Bernd Schimmelpfennig, Henry Moll, Zoltán Szabó, Ingmar Grenthe

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  12. Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)

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  13. Crystal structure of new hydroxide fluorides with isolated F− anions: [H3N(CH2)6NH3]2M(F, OH)6(F,OH)·H2O (M = Al, In)

    Journal of Fluorine Chemistry · 2001-08-01

    J. Touret, X. Bourdon, M. Leblanc, R. Retoux, Jean Renaudin, V. Maisonneuve

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  14. A New Oxoanion: [IO4]3-Containing I(V) with a Stereochemically Active Lone-Pair in the Silver Uranyl Iodate Tetraoxoiodate(V), Ag4(UO2)4(IO3)2(IO4)2O2

    Journal of the American Chemical Society · 2001-08-15

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  15. Hydrothermal synthesis of the first organically templated open-framework uranium phosphate

    Chemical Communications · 2001-10-31

    Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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  16. Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)

    Journal of Solid State Chemistry · 2001-11-01

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  17. Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides

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  18. [NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structure

    Chemical Communications · 2002-01-01

    M.B. Doran, Alexander J. Norquist, Dermot O’Hare

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  19. The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O

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  20. Structural and NMR studies of the series of related [H3N(CH2)xNH3]·AlF5 (x=6, 8, 10, 12) hybrid compounds

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    Evgeny Goreshnik, M. Leblanc, Etienne Gaudin, Françis Taulelle, V. Maisonneuve

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  21. Organically templated uranium(vi) sulfates: understanding phase stability using composition space

    Journal of Materials Chemistry · 2002-11-12

    Paul M. Thomas, Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  22. Incorporation of uranium( vi ) into metal–organic framework solids, [UO 2 (C 4 H 4 O 4 )]·H 2 O, [UO 2 F(C 5 H 6 O 4 )]·2H 2 O, and [(UO 2 ) 1.5 (C 8 H 4 O 4 ) 2 ] 2 [(CH 3 ) 2 NCOH 2 ]·H 2 O

    Dalton Transactions · 2003-01-01

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  23. The Actinides

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    Carol J. Burns, Mary P. Neu, Hakim Boukhalfa, Keith E. Gutowski, Nicholas J. Bridges, Robin Don Rogers

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  24. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

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  25. Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates

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  26. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

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  27. [(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework

    Journal of the American Chemical Society · 2003-09-26

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  28. 2D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties

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  29. Characterisation of Four New Two‐Dimensional Lithium Beryllofluoro‐Layered Compounds

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  30. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot O’Hare

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  31. Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates

    Journal of Solid State Chemistry · 2004-06-21

    Andrew J. Locock, Peter Carman Burns

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  32. Tris(2-ethylamino)amine (tren) as template for the elaboration of fluorides: synthesis and crystal structures of [(C2H4NH3)3NH]·[Zr3F16(H2O)], [(C2H4NH3)3N]2·[ZrF6]·[Zr2F12] and [(C2H4NH3)3N]·[TaF7]·F

    Journal of Solid State Chemistry · 2004-10-13

    Evgeny Goreshnik, M. Leblanc, V. Maisonneuve

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  33. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

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    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  34. Structural variation in organically templated uranium sulfate fluorides

    Dalton Transactions · 2005-01-01

    M.B. Doran, Ben E. Cockbain, Dermot O’Hare

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  35. Uranyl Complexation in Fluorinated Acids (HF, HBF4, HPF6, HTf2N): A Combined Experimental and Theoretical Study

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    C. Gaillard, Antoine El Azzi, Isabelle Billard, Hélène Bolvin, Christoph Hennig

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  36. (C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type

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  37. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

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    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  38. Synthesis, Structure and Photoluminescent Studies of Two Novel Layered Uranium Coordination Polymers Constructed from UO(OH) Polyhedra and Pyridinedicarboxylates

    European Journal of Inorganic Chemistry · 2005-09-05

    Yan‐Zhen Zheng, Ming‐Liang Tong, Xiao‐Ming Chen

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  39. [N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)

    Journal of Materials Chemistry · 2006-01-01

    Kang Min Ok, M.B. Doran, Dermot O’Hare

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  40. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

    Inorganic Chemistry · 2006-01-27

    Chih-Min Wang, Chia-Hsien Liao, Pei-Lin Chen, Kwang‐Hwa Lii

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  41. General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O

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  42. Two-dimensional composition diagram of the Al(OH)3-dien-HFaq.-ethanol system: Evidence of a new tetrahedral (Al4F18)6− polyanion

    Journal of Fluorine Chemistry · 2006-05-12

    Karim Adil, M. Leblanc, V. Maisonneuve

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  43. Product evolution in the Np(IV) fluorophosphate system

    Journal of Solid State Chemistry · 2006-09-30

    Travis H. Bray, Tyler A. Sullens, Tatiana Y. Shvareva, Richard E. Sykora, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  44. Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]

    Journal of Solid State Chemistry · 2006-11-14

    Kang Min Ok, Dermot O’Hare

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  45. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  46. Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate

    Chemistry of Materials · 2006-12-24

    Tatiana Y. Shvareva, S. Skanthakumar, L. Soderholm, Abraham Clearfield, Thomas E. Albrecht‐Schmitt

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  47. [(CH3)2NH(CH2)2NH(CH3)2][(UO2)2F2(HPO4)2]: a new organically templated layered uranium phosphate fluoride - synthesis, structure, characterization, and ion-exchange reactions

    Dalton Transactions · 2007-01-01

    Kang Min Ok, M.B. Doran, Dermot O’Hare

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  48. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

    Dalton Transactions · 2007-01-01

    Chih-Min Wang, Yi‐Ying Wu, Pei-Lin Chen, Kwang‐Hwa Lii

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  49. The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides

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  50. U(VI)-containing metal-organic frameworks and coordination polymers

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