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RESEARCH PAPER · Dalton Transactions · 2007

The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides

David W. Aldous, Nicholas F. Stephens, Philip Lightfoot

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The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluoridesOriginalAn unusual hybrid fluoride featuring a [V7F27]6− chain motif based on a pyrochlore-like building unit14Crystallisation of some mixed Na/V and K/V fluorides by solvothermal methods36Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions21Controllable solvothermal synthesis and photocatalytic properties of complex (oxy)fluorides K2TiOF4, K3TiOF5, K7Ti4O4F7 and K2TiF620Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers2Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides21Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases15Increasing the dimensionality of hybrid vanadium oxyfluorides using ionothermal synthesis31Structural chemistry of organically-templated metal fluorides61Syntheses and Physicochemical Properties of Low‐Melting Salts Based on VOF4– and MoOF5–, and the Molecular Geometries of the Dimeric (VOF4–)2 and Mo2O4F62– Anions24Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)15A new chain structure:catena-poly[4,4′-(ethane-1,2-diyl)dipyridinium bis[[aquadifluoridooxidovanadate]-μ-fluorido]]0Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides31Solvothermal and hydrothermal processes: the main physico-chemical factors involved and new trends66An ionothermally prepared S = 1/2 vanadium oxyfluoride kagome lattice164Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations9Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )4AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids59New structural units in molybdenum oxyfluoride chemistry14Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)16The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit18Syntheses, structures, sorption and magnetic properties of copper(II) frameworks with varied topologies14AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties22Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block27Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components13A hybrid vanadium fluoride with structurally isolated S = 1 kagome layers11Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride9Syntheses of Two Vanadium Oxide–Fluoride Materials That Differ in Phase Matchability46A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties2Structural complexity in indium selenides prepared using bicyclic amines as structure-directing agents10Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Polymorphism of NaVO2F2: aP21/csuperstructure with pseudosymmetry ofP21/min the subcell2Extending the Family of V4+S= Kagome Antiferromagnets17Extending the Family of V4+S=${{ 1/2 }}$ Kagome Antiferromagnets4Synthesis, Bonding, and Reactivity of Vanadium(IV) Oxido–Fluorido Compounds with Neutral Chelate Ligands of the General Formula cis-[VIV(═O)(F)(LN–N)2]+7Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials2Reactivity of VOF3 with N-Heterocyclic Carbene and Imidazolium Fluoride: Analysis of Ligand–VOF3 Bonding with Evidence of a Minute π Back-Donation of Fluoride16Conversion hydrothermale d'oxalates d'actinides tétravalents : de la synthèse au frittage des poudres d'oxydes0Coordination of a Neutral Ligand to a Metal Center of Oxohalido Anions: Fact or Fiction?3Layered Hybrid iron Fluorides2

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  1. An unusual hybrid fluoride featuring a [V7F27]6− chain motif based on a pyrochlore-like building unit

    Journal of Solid State Chemistry · 2008-08-15

    David W. Aldous, Alexandra M. Z. Slawin, Philip Lightfoot

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  2. Crystallisation of some mixed Na/V and K/V fluorides by solvothermal methods

    Solid State Sciences · 2008-10-01

    David W. Aldous, Philip Lightfoot

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  3. Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions

    Dalton Transactions · 2009-01-01

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  4. Controllable solvothermal synthesis and photocatalytic properties of complex (oxy)fluorides K2TiOF4, K3TiOF5, K7Ti4O4F7 and K2TiF6

    Journal of Hazardous Materials · 2009-06-09

    Jie Sheng, Kaibin Tang, Wei Cheng, Junli Wang, Nie Yanxiang, Qing Yang

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  5. Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers

    Journal of Solid State Chemistry · 2009-09-10

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

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  6. Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides

    Inorganica Chimica Acta · 2009-10-15

    P. DeBurgomaster, W. Ouellette, Hongxue Liu, Charles J. O’Connor, G.T. Yee, Jon A. Zubieta

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  7. Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases

    Inorganica Chimica Acta · 2009-10-30

    P. DeBurgomaster, Hongxue Liu, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  8. Increasing the dimensionality of hybrid vanadium oxyfluorides using ionothermal synthesis

    Dalton Transactions · 2010-01-01

    Farida Himeur, Phoebe K. Allan, Simon J. Teat, Richard J. Goff, Russell E. Morris, Philip Lightfoot

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  9. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  10. Syntheses and Physicochemical Properties of Low‐Melting Salts Based on VOF4– and MoOF5–, and the Molecular Geometries of the Dimeric (VOF4–)2 and Mo2O4F62– Anions

    European Journal of Inorganic Chemistry · 2010-01-19

    Takatsugu Kanatani, Kazuhiko Matsumoto, Rika Hagiwara

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  11. Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)

    Inorganic Chemistry Communications · 2010-02-05

    Stephanie Jones, Hongxue Liu, W. Ouellette, Katherine Schmidtke, Charles J. O’Connor, Jon A. Zubieta

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  12. A new chain structure:catena-poly[4,4′-(ethane-1,2-diyl)dipyridinium bis[[aquadifluoridooxidovanadate]-μ-fluorido]]

    Acta Crystallographica Section C Crystal Structure Communications · 2010-04-13

    David W. Aldous, Alexandra M. Z. Slawin, Philip Lightfoot

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  13. Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides

    Dalton Transactions · 2011-01-01

    Farida H. Aidoudi, P.J. Byrne, Pheobe K. Allan, Simon J. Teat, Philip Lightfoot, Russell E. Morris

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  14. Solvothermal and hydrothermal processes: the main physico-chemical factors involved and new trends

    Research on Chemical Intermediates · 2011-02-10

    Gérard Demazeau

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  15. An ionothermally prepared S = 1/2 vanadium oxyfluoride kagome lattice

    Nature Chemistry · 2011-08-26

    Farida H. Aidoudi, David W. Aldous, Richard J. Goff, Alexandra M. Z. Slawin, John Paul Attfield, Russell E. Morris, Philip Lightfoot

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  16. Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations

    Inorganica Chimica Acta · 2011-09-10

    Tiffany M. Smith, Michael Tichenor, Jose Marcelo Vargas, Charles J. O’Connor, Jon A. Zubieta

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  17. Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-20

    Matic Lozinšek, Evgeny Goreshnik, Boris Žemva

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  18. AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids

    Inorganic Chemistry · 2012-07-25

    Ganna A. Senchyk, Valerii Bukhanko, A.B. Lysenko, Harald Krautscheid, Eduard B. Rusanov, A.N. Chernega, Mirosław Karbowiak, K.V. Domasevitch

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  19. New structural units in molybdenum oxyfluoride chemistry

    Journal of Fluorine Chemistry · 2012-08-09

    David W. Aldous, Philip Lightfoot

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  20. Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)

    Inorganica Chimica Acta · 2012-11-02

    Stephanie Jones, Jose Marcelo Vargas, Steven Pellizzeri, Charles J. O’Connor, Jon A. Zubieta

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  21. The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit

    Journal of Solid State Chemistry · 2013-01-26

    Hongcheng Lu, Romain Gautier, Zuo-Xi Li, Wanqi Jie, Zheng‐Tang Liu, Kenneth Reinhard Poeppelmeier

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  22. Syntheses, structures, sorption and magnetic properties of copper(II) frameworks with varied topologies

    Microporous and Mesoporous Materials · 2013-03-28

    Peng Wang, Li Luo, Jian Fan, Gao‐Chao Lv, You Song, Wei‐Yin Sun

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  23. AgNa(VO2F2)2: A Trioxovanadium Fluoride with Unconventional Electrochemical Properties

    Journal of the American Chemical Society · 2013-06-24

    Martin D. Donakowski, Arno L. Görne, John T. Vaughey, Kenneth Reinhard Poeppelmeier

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  24. Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block

    Dalton Transactions · 2013-10-07

    Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

    Read original paper ↗ ·

  25. Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components

    Inorganica Chimica Acta · 2013-11-28

    Tiffany M. Smith, Luke Strauskulage, Kathryn Perrin, Diona Symester, Steve R. Freund, Jose Marcelo Vargas, Leonard Spînu, Jon A. Zubieta

    Read original paper ↗ ·

  26. A hybrid vanadium fluoride with structurally isolated S = 1 kagome layers

    Dalton Transactions · 2014-01-01

    Farida H. Aidoudi, Lewis J. Downie, Russell E. Morris, Mark A. de Vries, Philip Lightfoot

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  27. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  28. Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride

    Journal of Cluster Science · 2014-08-14

    Issam Omri, Mohsen Graia, Tahar Mhiri

    Read original paper ↗ ·

  29. Syntheses of Two Vanadium Oxide–Fluoride Materials That Differ in Phase Matchability

    Inorganic Chemistry · 2014-08-19

    Martin D. Donakowski, Romain Gautier, Hongcheng Lu, T. Thao Tran, Jacqueline Cantwell, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  30. A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties

    Journal of Cluster Science · 2014-11-08

    Issam Omri, Tahar Mhiri, Mohsen Graia

    Read original paper ↗ ·

  31. Structural complexity in indium selenides prepared using bicyclic amines as structure-directing agents

    Dalton Transactions · 2014-11-19

    Sarah J. Ewing, Paz Vaqueiro

    Read original paper ↗ ·

  32. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  33. Polymorphism of NaVO2F2: aP21/csuperstructure with pseudosymmetry ofP21/min the subcell

    Acta Crystallographica Section C Structural Chemistry · 2015-05-07

    Zi-Qun Yu, Jingquan Wang, Ya‐Xi Huang, Sanda M. Botis, Yuanming Pan, Jin‐Xiao Mi

    Read original paper ↗ ·

  34. Extending the Family of V4+S= Kagome Antiferromagnets

    Angewandte Chemie International Edition · 2015-10-30

    Lucy Clark, Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

    Read original paper ↗ ·

  35. Extending the Family of V4+S=${{ 1/2 }}$ Kagome Antiferromagnets

    Angewandte Chemie · 2015-10-30

    Lucy Clark, Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

    Read original paper ↗ ·

  36. Synthesis, Bonding, and Reactivity of Vanadium(IV) Oxido–Fluorido Compounds with Neutral Chelate Ligands of the General Formula cis-[VIV(═O)(F)(LN–N)2]+

    Inorganic Chemistry · 2016-01-21

    Stamatis S. Passadis, Constantinos G. Tsiafoulis, Chryssoula Drouza, Athanassios C. Tsipis, Haralampos N. Miras, Anastasios D. Keramidas, Themistoklis A. Kabanos

    Read original paper ↗ ·

  37. Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials

    The Philosophical Magazine A Journal of Theoretical Experimental and Applied Physics · 2016-08-31

    A.H. Reshak

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  38. Reactivity of VOF3 with N-Heterocyclic Carbene and Imidazolium Fluoride: Analysis of Ligand–VOF3 Bonding with Evidence of a Minute π Back-Donation of Fluoride

    Inorganic Chemistry · 2018-10-24

    Žiga Zupanek, Melita Tramšek, Anton Kokalj, Gašper Tavčar

    Read original paper ↗ ·

  39. Conversion hydrothermale d'oxalates d'actinides tétravalents : de la synthèse au frittage des poudres d'oxydes

    Unknown journal · 2020-11-10

    Jérémie Manaud

    Read original paper ↗ ·

  40. Coordination of a Neutral Ligand to a Metal Center of Oxohalido Anions: Fact or Fiction?

    Inorganic Chemistry · 2021-08-05

    Anton Kokalj, Žiga Zupanek, Melita Tramšek, Gašper Tavčar

    Read original paper ↗ ·

  41. Layered Hybrid iron Fluorides

    Crystals · 2022-10-13

    Teng Li, Philip Lightfoot

    Read original paper ↗ ·
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