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RESEARCH PAPER · Chemical Communications · 2002

[NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structure

M.B. Doran, Alexander J. Norquist, Dermot O’Hare

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[NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structureOriginal22 New compounds and structures in the solid state217 Scandium, yttrium, the lanthanides and the actinides321 New compounds and structures in the solid state1The Actinides34[NC4H12]2 [(UO2)6(H2O)2 (SO4)7]: The First Organically Templated Actinide Sulfate with a Three‐Dimensional Framework Structure.0Reactant-Mediated Diversity in Uranyl Phosphonates58The effects of linear diamine chain length in uranium sulfates48Synthesis and structure of organically templated lanthanum sulfate [C4N3H16][La(SO4)3]·H2O57The first organically templated linear metal selenate50The First Sodium Uranyl Chromate, Na4[(UO2)(CrO4)3]: Synthesis and Crystal Structure Determination39Exploration of Composition Space in Templated Uranium Sulfates8918 Scandium, yttrium, the lanthanides and the actinides11[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Synthesis, Structure, and the Unusual Magnetic Properties of an Amine-Templated Iron(II) Sulfate Possessing the Kagomé Lattice102Synthesis, Structure, and Magnetic Properties of Amine-Templated Open-Framework Nickel(II) Sulfates61Synthesis and crystal structure of a new neodymium(III) selenate-selenite: Nd2(SeO4)(SeO3)2(H2O)217Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)53Chiral open-framework uranyl molybdates. 2. Flexibility of the U:Mo=6:7 frameworks: syntheses and crystal structures of (UO2)0.82[C8H20N]0.36[(UO2)6(MoO4)7(H2O)2](H2O)n and [C6H14N2][(UO2)6(MoO4)7(H2O)2](H2O)m38Structural variation in organically templated uranium sulfate fluorides42[C2N2H10]1.5[Nd(SO4)3(H2O)]·2H2O: The first organically templated neodymium sulfate with a layer structure21[H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates38Synthesis, Crystal Structure, and Magnetic Properties of a Three‐Dimensional Hydroxide Sulfate: Mn5(OH)8SO412Low‐Dimensional Structural Units in Amine‐Templated Uranyl Oxoselenates(VI): Synthesis and Crystal Structures of [C3H12N2][(UO2)(SeO4)2(H2O)2](H2O), [C5H16N2]2[(UO2)(SeO4)2(H2O)](NO3)2, [C4H12N][(UO2)(SeO4)(NO3)], and [C4H14N2][(UO2)(SeO4)2(H2O)]40Organically‐Templated Zinc and Thorium Sulfates with Chain and Layered Structures17[N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)38Organically-templated metal sulfates, selenites and selenates194Two new 3D organically templated cerium sulfates, hydrothermal synthesis and structural characterization7General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O40Hydrothermal synthesis and crystal structure of a new inorganic/organic hybrid of scandium sulfate: (H2en)Sc2(SO4)4·(H2O)0.727Synthesis and structure of the first organic–inorganic hybrid tin (II) chlorosulfate: [C6N2H14][SnCl2SO4]2Supramolecular networks of transition metal sulfates templated by piperazine49Organically Directed Iron Sulfate Chains: Structural Diversity Based on Hydrogen Bonding Interactions31Hydrothermal Synthesis and Crystal Structure of a Novel 3-D Porous Lanthanum Sulfate21Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26Organic–inorganic hybrid materials constructed from inorganic lanthanide sulfate skeletons and organic 4,5-imidazoledicarboxylic acid115Synthesis, crystal structures, phase transition characterization and thermal decomposition of a new dabcodiium hexaaquairon(II) bis(sulfate): (C6H14N2)[Fe(H2O)6](SO4)260A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds90A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds11Solvothermal Synthesis, Crystal Structure and Properties of a New Organic Templated Lanthanum Sulfate [C4N3H16][La(SO4)3(H2O)]25(2,2′-bipy)[In2(OH)2(H2O)](SO4)2: The first indium sulfate with a layer structure8An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids42Synthesis and Structural Characterization of Open-Framework Copper (II) Sulfates22New transition metal sulfates templated by 1,4-butanediamine, (C4H14N2)[MII(H2O)6](SO4)2·4H2O (MII: Co, Ni): Structure, reactivity and thermal decomposition23Solvothermal synthesis, crystal structure and luminescence of the first organic amine templated europium sulfate21Solvothermal Synthesis, Crystal Structure and Properties of the First Organic‐templated Holmium Sulfate [C2N2H10]3[Ho2(SO4)6·2H2O]24Solvothermal synthesis, crystal structure and properties of a novel 1-D organic amine templated holmium sulfate19Synthesis, structural characterisation and thermal decomposition of a new organic–inorganic hybrid material (C5H14N2)[Cu(SO4)2(H2O)4]·H2O16Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism35(C 2 H 8 N) 9 [Eu 5 (SO 4 ) 12 ]·2H 2 O: the first europium sulfate open-framework containing two kinds of intersecting extra-large 20-membered ring channels32A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Crystal structure, phase transition and thermal decomposition of a copper (II) sulfate dihydrate containing a chiral organic ammonium cation23Amine templated two- and three-dimensional uranyl sulfates24Solvothermal syntheses, crystal structures and luminescence properties of three new lanthanide sulfate fluorides33Solvothermal Synthesis, Crystal Structure, and Properties of a New Organic‐Templated Holmium Sulfate with 1D Single Ladder Chains14Hydrothermal synthesis and structure of three novel open-framework lanthanide sulfate–oxalates13Solvothermal Synthesis, Crystal Structures, and Magnetic Properties of Two Organically Templated Iron Sulfates with Chain Structures3New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates8Hydrothermal synthesis and characterization of a Na+ templated new 3-D lanthanum sulfate Na[C6H14N2][La3(SO4)6(H2O)3] constructed from La–O–S tubes and cubic cages12Second structural directing agent induces the formation of 1D organic templated terbium sulfate17Dy2(SO3)2(SO4)(H2O)2: the first lanthanide mixed sulfate–sulfite inorganic compound3Synthesis, structure and properties of the first organic-templated inorganic-framework Ba(II) perchlorate6Structural systematic design of organic templated samarium sulfates and their luminescence property14Solvothermal synthesis, crystal structure and properties of three new 1D and 3D organically templated lanthanide sulfates7Synthesis, crystal structures and thermal behaviour of organic–inorganic hybrids incorporating a chiral diamine19Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21A series of new rare earth sulfates based on lanthanide contraction and dual organic-amine templating effects12Solvothermal synthesis, structure and characterization of 1D chain and 2D layered rare earth sulfates in the presence of cyclic diamines4Isopropylammonium Layered Uranyl Chromates: Syntheses and Crystal Structures of [(CH3)2CHNH3]3[(UO2)3(CrO4)2O(OH)3] and[(CH3)2CHNH3]2[(UO2)2(CrO4)3(H2O)]30Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system24Syntheses, structures and luminescent properties of two one-dimensional uranium oxyfluorides12Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418l - and d -[Ln(HCO2)(SO4)(H2O)]n (Ln = La, Ce, Pr, Nd, and Eu): Chiral Enantiomerically 3D Architectures Constructed by Double −[Ln–O]n– Helices29Crystal Chemistry of Uranium Oxides and Minerals27Two new piperazine templated lanthanide sulfates with 2D corrugated layered crystal structures5(C4N2H12)3[Ln3(OH)(SO4)7] (Ln = Sm, Eu, and Tb): A Series of Honeycomb-like Open-Framework Lanthanide Sulfates with Extra-Large Channels Containing 24-Membered Rings31Synthesis, structure and photoluminescence properties of amine-templated open-framework bismuth sulfates9Synthesis and characterization of robust three-dimensional chiral metal sulfates93-D Hydrogen bonded networks of three organically templated cadmium sulfates. Dehydration reactions and crystallization behavior5Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Synthesis, structural characterization, electronic spectroscopy, and microfluidic detection of Cu +2 and UO 2 +2 [di- tert -butyl-salphenazine] complexes7Coherent Fusion of Water Array and Protonated Amine in a Metal–Sulfate-Based Coordination Polymer for Proton Conduction18Effect of the partial substitution of sulfur by selenium on the atomic arrangement in sulfate- and selenate-based compounds3Microporous uranyl chromates successively formed by evaporation from acidic solution9NCI calculations for understanding a physical phase transition in (C 6 H 14 N 2 )[Mn(H 2 O) 6 ](SeO 4 ) 26Luminescent mixed-crystal Ln-MOF thin film for the recognition and detection of pharmaceuticals107Synthesis and Study of the First Zeolitic Uranium Borate22Complex Inorganic Actinide Materials1Structural unit charge density and molecular cation templating effects on orientational geometric isomerism and interlayer spacing in 2-D uranyl sulfates11Ligand Mediated Morphology of the Two‐Dimensional Uranyl Aqua Sulfates [UO2(X)(SO4)(H2O)] [X = Cl– or (CH3)3NCH2COO]6A new mixed halide 2D hybrid perovskite: Structural, thermal, optic and magnetic properties34Two‐Dimensional Uranyl Borates: From Conventional to Extreme Synthetic Conditions13Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3Hydrogen bond network and bond valence analysis on uranyl sulfate compounds with organic-based interstitial cations5Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis10Organically Templated Uranyl Sulfates and Selenates: Structural Complexity and Crystal Chemical Restrictions for Isotypic Compounds Formation7Crystal Growth, Optical, Mechanical and Dielectric Analysis of Semiorganic Glycine Manganese Sulphate Single Crystal for Opto‐Electronic Device Application0Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3Lanthanide salts in sustainable corrosion protection: Chemistry, progress, mechanism, challenges and opportunities6

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  1. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

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  2. 17 Scandium, yttrium, the lanthanides and the actinides

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  3. 21 New compounds and structures in the solid state

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  4. The Actinides

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    Carol J. Burns, Mary P. Neu, Hakim Boukhalfa, Keith E. Gutowski, Nicholas J. Bridges, Robin Don Rogers

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  5. [NC4H12]2 [(UO2)6(H2O)2 (SO4)7]: The First Organically Templated Actinide Sulfate with a Three‐Dimensional Framework Structure.

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  6. Reactant-Mediated Diversity in Uranyl Phosphonates

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  7. The effects of linear diamine chain length in uranium sulfates

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  8. Synthesis and structure of organically templated lanthanum sulfate [C4N3H16][La(SO4)3]·H2O

    Journal of Solid State Chemistry · 2003-07-22

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  9. The first organically templated linear metal selenate

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  10. The First Sodium Uranyl Chromate, Na4[(UO2)(CrO4)3]: Synthesis and Crystal Structure Determination

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  11. Exploration of Composition Space in Templated Uranium Sulfates

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  12. 18 Scandium, yttrium, the lanthanides and the actinides

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  13. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

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  14. Synthesis, Structure, and the Unusual Magnetic Properties of an Amine-Templated Iron(II) Sulfate Possessing the Kagomé Lattice

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  15. Synthesis, Structure, and Magnetic Properties of Amine-Templated Open-Framework Nickel(II) Sulfates

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  16. Synthesis and crystal structure of a new neodymium(III) selenate-selenite: Nd2(SeO4)(SeO3)2(H2O)2

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  17. Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)

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  18. Chiral open-framework uranyl molybdates. 2. Flexibility of the U:Mo=6:7 frameworks: syntheses and crystal structures of (UO2)0.82[C8H20N]0.36[(UO2)6(MoO4)7(H2O)2](H2O)n and [C6H14N2][(UO2)6(MoO4)7(H2O)2](H2O)m

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  19. Structural variation in organically templated uranium sulfate fluorides

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  20. [C2N2H10]1.5[Nd(SO4)3(H2O)]·2H2O: The first organically templated neodymium sulfate with a layer structure

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  21. [H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates

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  22. Synthesis, Crystal Structure, and Magnetic Properties of a Three‐Dimensional Hydroxide Sulfate: Mn5(OH)8SO4

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  23. Low‐Dimensional Structural Units in Amine‐Templated Uranyl Oxoselenates(VI): Synthesis and Crystal Structures of [C3H12N2][(UO2)(SeO4)2(H2O)2](H2O), [C5H16N2]2[(UO2)(SeO4)2(H2O)](NO3)2, [C4H12N][(UO2)(SeO4)(NO3)], and [C4H14N2][(UO2)(SeO4)2(H2O)]

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  24. Organically‐Templated Zinc and Thorium Sulfates with Chain and Layered Structures

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  25. [N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)

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  26. Organically-templated metal sulfates, selenites and selenates

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  27. Two new 3D organically templated cerium sulfates, hydrothermal synthesis and structural characterization

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  28. General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O

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  29. Hydrothermal synthesis and crystal structure of a new inorganic/organic hybrid of scandium sulfate: (H2en)Sc2(SO4)4·(H2O)0.72

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  30. Synthesis and structure of the first organic–inorganic hybrid tin (II) chlorosulfate: [C6N2H14][SnCl2SO4]

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  31. Supramolecular networks of transition metal sulfates templated by piperazine

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  32. Organically Directed Iron Sulfate Chains: Structural Diversity Based on Hydrogen Bonding Interactions

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  33. Hydrothermal Synthesis and Crystal Structure of a Novel 3-D Porous Lanthanum Sulfate

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  34. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

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  35. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

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  36. Organic–inorganic hybrid materials constructed from inorganic lanthanide sulfate skeletons and organic 4,5-imidazoledicarboxylic acid

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  37. Synthesis, crystal structures, phase transition characterization and thermal decomposition of a new dabcodiium hexaaquairon(II) bis(sulfate): (C6H14N2)[Fe(H2O)6](SO4)2

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  38. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

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  39. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

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  40. Solvothermal Synthesis, Crystal Structure and Properties of a New Organic Templated Lanthanum Sulfate [C4N3H16][La(SO4)3(H2O)]

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  41. (2,2′-bipy)[In2(OH)2(H2O)](SO4)2: The first indium sulfate with a layer structure

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  42. An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids

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  43. Synthesis and Structural Characterization of Open-Framework Copper (II) Sulfates

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  44. New transition metal sulfates templated by 1,4-butanediamine, (C4H14N2)[MII(H2O)6](SO4)2·4H2O (MII: Co, Ni): Structure, reactivity and thermal decomposition

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  45. Solvothermal synthesis, crystal structure and luminescence of the first organic amine templated europium sulfate

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  46. Solvothermal Synthesis, Crystal Structure and Properties of the First Organic‐templated Holmium Sulfate [C2N2H10]3[Ho2(SO4)6·2H2O]

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  47. Solvothermal synthesis, crystal structure and properties of a novel 1-D organic amine templated holmium sulfate

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  48. Synthesis, structural characterisation and thermal decomposition of a new organic–inorganic hybrid material (C5H14N2)[Cu(SO4)2(H2O)4]·H2O

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  49. Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships

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    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  50. Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism

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