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RESEARCH PAPER · Journal of Solid State Chemistry · 2004

Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates

Andrew J. Locock, Peter Carman Burns

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Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenatesOriginalSyntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs4[(UO2)2(GaOH)2(PO4)4]·H2O and Cs[UO2Ga(PO4)2]6820 New compounds and structures in the solid state5Structural study of trivalent lanthanide and actinide complexes formed upon solvent extraction82Raman spectroscopy study of selected uranophanes22General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O40Raman spectroscopic study of the uranyl oxyhydroxide hydrates: becquerelite, billietite, curite, schoepite and vandendriesscheite122Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Three-dimensional framework of uranium-centered polyhedra with non-intersecting channels in the uranyl oxy-vanadates A2(UO2)3(VO4)2O (A=Li, Na)35Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O2The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate12Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370[H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl17New open-framework in the uranyl vanadates A3(UO2)7(VO4)5O (A=Li, Ag) with intergrowth structure between A(UO2)4(VO4)3 and A2(UO2)3(VO4)2O23Raman spectroscopic study of the uranyl mineral natrouranospinite (Na2,Ca)[(UO2)(AsO4)]2· 5H2O8[Hg5O2(OH)4][(UO2)2(AsO4)2]: A complex mercury(II) uranyl arsenate6A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks79Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers6Raman spectroscopic study of the uranyl titanate mineral brannerite (U,Ca,Y,Ce)2(Ti,Fe)2O6:effect of metamictisation14Raman spectroscopic study of the uranyl titanate mineral betafite (Ca,U)2(Ti,Nb)2O6(OH): effect of metamictization5New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]15Raman spectroscopic study of the uranyl titanate mineral euxenite (Y,Ca,U,Ce,Th) (Nb,Ta,Ti)2O69Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy109Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds72Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine10In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions1Ionothermal synthesis of uranyl compounds that incorporate imidazole derivatives14Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3Synthesis, Characterization, and Solid-State Structural Chemistry of Uranium(IV) Aliphatic Dicarboxylates7Chemical stability of rare-earth elements’ uranyl arsenates with general formula MIII(AsUO6)3·16H2O (MIII–La–Lu) in aqueous solution3Mild hydrothermal synthesis of potassium uranyl phosphates with layered and framework structures2Solubility and Thermodynamic Investigation of Meta-Autunite Group Uranyl Arsenate Solids with Monovalent Cations Na and K7Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3Mild Hydrothermal Crystal Growth of Two Luminescing Uranyl Phosphates Exhibiting an Autunite-Type Sheet Structure3

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  1. Syntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs4[(UO2)2(GaOH)2(PO4)4]·H2O and Cs[UO2Ga(PO4)2]

    Inorganic Chemistry · 2004-12-24

    Tatiana Y. Shvareva, Tyler A. Sullens, Thomas C. Shehee, Thomas E. Albrecht‐Schmitt

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  2. 20 New compounds and structures in the solid state

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  3. Structural study of trivalent lanthanide and actinide complexes formed upon solvent extraction

    Dalton Transactions · 2006-01-01

    Benoît Gannaz, Mark R. Antonio, Renato Chiarizia, Cl ment Hill, Gérard Cote

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  4. Raman spectroscopy study of selected uranophanes

    Journal of Molecular Structure · 2006-01-05

    Ray L. Frost, Jiřı́ Čejka, Matt L. Weier, Wayde N. Martens

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  5. General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O

    Inorganic Chemistry · 2006-02-03

    Tatiana Y. Shvareva, Thomas E. Albrecht‐Schmitt

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  6. Raman spectroscopic study of the uranyl oxyhydroxide hydrates: becquerelite, billietite, curite, schoepite and vandendriesscheite

    Journal of Raman Spectroscopy · 2006-12-07

    Ray L. Frost, Jiří Čejka, Matt L. Weier

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  7. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  8. Three-dimensional framework of uranium-centered polyhedra with non-intersecting channels in the uranyl oxy-vanadates A2(UO2)3(VO4)2O (A=Li, Na)

    Journal of Solid State Chemistry · 2006-12-28

    S. Obbade, L. Duvieubourg, C. Dion, F. Abraham

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  9. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

    Inorganic Chemistry · 2007-08-24

    Sukhendu Bikas Mandal, Manabendra Chandra, Srinivasan Natarajan

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  10. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  11. Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O

    Solid State Sciences · 2007-12-04

    Yaqin Yu, Thomas E. Albrecht‐Schmitt

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  12. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  13. Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate

    Journal of Solid State Chemistry · 2008-05-17

    Travis H. Bray, John D. Gorden, Thomas E. Albrecht‐Schmitt

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  14. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  15. [H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl

    Inorganic Chemistry · 2008-08-23

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  16. New open-framework in the uranyl vanadates A3(UO2)7(VO4)5O (A=Li, Ag) with intergrowth structure between A(UO2)4(VO4)3 and A2(UO2)3(VO4)2O

    Journal of Solid State Chemistry · 2008-10-30

    S. Obbade, Catherine Renard, F. Abraham

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  17. Raman spectroscopic study of the uranyl mineral natrouranospinite (Na2,Ca)[(UO2)(AsO4)]2· 5H2O

    Journal of Raman Spectroscopy · 2009-03-03

    Jiří Čejka, Jiří Sejkora, Ray L. Frost, Eloise C. Keeffe

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  18. [Hg5O2(OH)4][(UO2)2(AsO4)2]: A complex mercury(II) uranyl arsenate

    Journal of Solid State Chemistry · 2009-04-09

    Yaqin Yu, Kai Jiang, Thomas E. Albrecht‐Schmitt

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  19. A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems

    Journal of Solid State Chemistry · 2009-11-01

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

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  20. Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks

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    P. Thuéry, B. Masci

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  21. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

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    Vandavasi Koteswara Rao, K. Bharathi, Ramanath Prabhu, Manabendra Chandra, Srinivasan Natarajan

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  22. U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers

    IOP Conference Series Materials Science and Engineering · 2010-03-01

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  23. Raman spectroscopic study of the uranyl titanate mineral brannerite (U,Ca,Y,Ce)2(Ti,Fe)2O6:effect of metamictisation

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    Ray L. Frost, B. Jagannadha Reddy

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  24. Raman spectroscopic study of the uranyl titanate mineral betafite (Ca,U)2(Ti,Nb)2O6(OH): effect of metamictization

    Radiation effects and defects in solids · 2010-07-20

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  25. New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates

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  26. Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]

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  27. Raman spectroscopic study of the uranyl titanate mineral euxenite (Y,Ca,U,Ce,Th) (Nb,Ta,Ti)2O6

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  28. Probing the local coordination environment and nuclearity of uranyl(vi) complexes in non-aqueous media by emission spectroscopy

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  29. Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds

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  30. Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine

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  31. In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions

    MRS Proceedings · 2012-01-01

    Brendan T. McGrail, Laurent J. Jouffret, Eric M. Villa, Peter Carman Burns

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  32. Ionothermal synthesis of uranyl compounds that incorporate imidazole derivatives

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  33. Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine

    Journal of Solid State Chemistry · 2012-09-05

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  34. Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]

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  35. Synthesis, Characterization, and Solid-State Structural Chemistry of Uranium(IV) Aliphatic Dicarboxylates

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  36. Chemical stability of rare-earth elements’ uranyl arsenates with general formula MIII(AsUO6)3·16H2O (MIII–La–Lu) in aqueous solution

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  37. Mild hydrothermal synthesis of potassium uranyl phosphates with layered and framework structures

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  38. Solubility and Thermodynamic Investigation of Meta-Autunite Group Uranyl Arsenate Solids with Monovalent Cations Na and K

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  39. Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University

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  40. Mild Hydrothermal Crystal Growth of Two Luminescing Uranyl Phosphates Exhibiting an Autunite-Type Sheet Structure

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