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RESEARCH PAPER · Chemical Communications · 2001

Direct in situ observation of increasing structural dimensionality during the hydrothermal formation of open-framework zinc phosphates

Richard I. Walton, Alexander J. Norquist, Dermot O’Hare, S. Neeraj, Srinivasan Natarajan, C.N.R. Rao

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Direct in situ observation of increasing structural dimensionality during the hydrothermal formation of open-framework zinc phosphatesOriginalBasic building units, self-assembly and crystallization in the formation of complex inorganic open architectures13A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates50A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates6Synthesis of Open-Framework Iron Phosphates, [C6N2H14][FeIII2F2(HPO4)2(H2PO4)2]·2H2O and [C6N2H14]2[FeIII3(OH)F3(PO4)(HPO4)2]2·H2O, with One- and Three-Dimensional Structures33Novel Inorganic Coordination Polymers Based on Cadmium Oxalates22In‐Situtime‐resolved X‐ray diffraction: The current state of the art11Two polymorphs of a piperazinium zincophosphate with different interrupted SOD-type frameworks11Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-334Hydro/Solvothermal Synthesis and Structures of New Zinc Phosphates of Varying Dimensionality36Synthesis and structure of a zinc oxalate with honeycomb layers and zinc phosphates with one- and three-dimensional structures31Templated inorganic networks: recent developments36Comparison of one-, two-, and three-dimensional iron phosphates containing ethylenediamine20Synthesis of a Single Four-Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single-Crystal and in-Situ MAS NMR Investigation53Two polymorphs of a tetramethylammonium zincophosphate with diamond net-related frameworks containing [H3O4(P)4] hydroxyl nests: solution-mediated and mechanochemical phase transformations and crystal structures14Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates64(NH 4 )Zn 2 (PO 4 )(HPO 4 ): Hydrothermal Synthesis and Reaction with n-Alkylamine Vapours3Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules6The Role of Amine Sulfates in Hydrothermal Uranium Chemistry63Hydrothermal synthesis and structures of two zero-dimensional zinc phosphate polymorphs4Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction57Towards understanding, control and application of layered double hydroxide chemistry582In-situ XRD as a tool to understanding zeolite crystallization105Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction15Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane39Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370Role of Temperature and Time in the Formation of Infinite −M−O−M− Linkages and Isolated Clusters in MOFs: A Few Illustrative Examples163Control of polymorphism in NaNbO 3 by hydrothermal synthesis71Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Nanoscale Chemistry of Uranyl Selenates1In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Steric-Induced Layer Flection in Templated Vanadium Tellurites11Bismuth Tri‐ and Tetraarylcarboxylates: Crystal Structures, In Situ X‐ray Diffraction, Intermediates and Luminescence82Nonaqueous synthesis of molecular zinc amide phosphate4Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction53Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction14Synthesis and crystal-chemical features of two new uranyl chromates with the structures derived from [(UO2)(T6+O4)(H2O) n ]0 (T = Cr6+, S6+, Se6+, n = 0–2)11Organization of Copper Azide Clusters into Two‐Dimensional Structures: Synthesis, Structure, and Magnetic Properties6In Situ Neutron Diffraction Studies of the Flux Crystal Growth of the Reduced Molybdates La 4 Mo 2 O 11 and Ce 4 Mo 2 O 11 : Revealing Unexpected Mixed-Valent Transient Intermediates and Determining the Sequence of Events during Crystal Growth18A kinetic and mechanistic study into the transformation of calcium sulfate hemihydrate to dihydrate40Solvothermal and hydrothermal methods for preparative solid-state chemistry5

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  1. Basic building units, self-assembly and crystallization in the formation of complex inorganic open architectures

    Journal of Chemical Sciences · 2001-10-01

    C. N. R. Rao

    Read original paper ↗ ·

  2. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

    Angewandte Chemie International Edition · 2002-04-02

    Sandip Chakrabarti, Srinivasan Natarajan

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  3. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

    Angewandte Chemie · 2002-04-02

    Sandip Chakrabarti, Srinivasan Natarajan

    Read original paper ↗ ·

  4. Synthesis of Open-Framework Iron Phosphates, [C6N2H14][FeIII2F2(HPO4)2(H2PO4)2]·2H2O and [C6N2H14]2[FeIII3(OH)F3(PO4)(HPO4)2]2·H2O, with One- and Three-Dimensional Structures

    Journal of Solid State Chemistry · 2002-05-01

    S. Mahesh, Mark Green, Srinivasan Natarajan

    Read original paper ↗ ·

  5. Novel Inorganic Coordination Polymers Based on Cadmium Oxalates

    Journal of Solid State Chemistry · 2002-06-01

    P.A. Prasad, S. Neeraj, Ramanathan Vaidhyanathan, Srinivasan Natarajan

    Read original paper ↗ ·

  6. In‐Situtime‐resolved X‐ray diffraction: The current state of the art

    Synchrotron Radiation News · 2002-07-01

    Ann E. Terry, G. Vaughan, Åke Kvick, Richard I. Walton, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  7. Two polymorphs of a piperazinium zincophosphate with different interrupted SOD-type frameworks

    Microporous and Mesoporous Materials · 2002-07-01

    Michael Wiebcke

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  8. Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-3

    Chemistry of Materials · 2002-09-14

    Franck Millange, Richard I. Walton, Nathalie Guillou, Thierry Loiseau, Dermot O’Hare, Gérard Férey

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  9. Hydro/Solvothermal Synthesis and Structures of New Zinc Phosphates of Varying Dimensionality

    Inorganic Chemistry · 2002-09-21

    Srinivasan Natarajan

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  10. Synthesis and structure of a zinc oxalate with honeycomb layers and zinc phosphates with one- and three-dimensional structures

    Solid State Sciences · 2002-10-01

    Srinivasan Natarajan

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  11. Templated inorganic networks: recent developments

    Current Opinion in Solid State and Materials Science · 2002-10-01

    William T. A. Harrison

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  12. Comparison of one-, two-, and three-dimensional iron phosphates containing ethylenediamine

    Journal of Solid State Chemistry · 2003-06-30

    Yanning Song, Peter Y. Zavalij, Natasha A. Chernova, Masatsugu Suzuki, M. Stanley Whittingham

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  13. Synthesis of a Single Four-Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single-Crystal and in-Situ MAS NMR Investigation

    Inorganic Chemistry · 2003-09-06

    Srinivasan Natarajan, Leo van Wüllen, Wilhelm Klein, Martin Jansen

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  14. Two polymorphs of a tetramethylammonium zincophosphate with diamond net-related frameworks containing [H3O4(P)4] hydroxyl nests: solution-mediated and mechanochemical phase transformations and crystal structures

    Solid State Sciences · 2004-02-01

    Michael Wiebcke, Bernd Marler

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  15. Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates

    Journal of the American Chemical Society · 2004-05-08

    Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  16. (NH 4 )Zn 2 (PO 4 )(HPO 4 ): Hydrothermal Synthesis and Reaction with n-Alkylamine Vapours

    Journal of Inclusion Phenomena and Macrocyclic Chemistry · 2004-08-01

    Beatriz Ramajo, Aránzazu Espina, Sergei A. Khainakov, José R. Garcı́a

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  17. Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)

    The Journal of Physical Chemistry B · 2004-11-24

    Thierry Loiseau, L. Beitone, Franck Millange, Françis Taulelle, Dermot O’Hare, Gérard Férey

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  18. Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules

    Journal of Solid State Chemistry · 2005-02-15

    Michael Wiebcke, Clemens Kühn, Gerhard Wildermuth

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  19. The Role of Amine Sulfates in Hydrothermal Uranium Chemistry

    Inorganic Chemistry · 2005-05-01

    Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  20. Hydrothermal synthesis and structures of two zero-dimensional zinc phosphate polymorphs

    Solid State Sciences · 2005-10-25

    Srinivasan Natarajan

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  21. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction

    Structure and bonding · 2005-11-08

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  22. Towards understanding, control and application of layered double hydroxide chemistry

    Journal of Materials Chemistry · 2006-01-01

    Gareth R. Williams, Dermot O’Hare

    Read original paper ↗ ·

  23. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

    Read original paper ↗ ·

  24. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction

    ChemInform · 2006-05-23

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

    Read original paper ↗ ·

  25. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

    Chemistry of Materials · 2006-07-18

    Gareth R. Williams, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  26. Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane

    New Journal of Chemistry · 2006-11-24

    R. Atencio, Alexander Briceño, Pedro J. Silva, José A. Rodríguez, Jonathan C. Hanson

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  27. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  28. Role of Temperature and Time in the Formation of Infinite −M−O−M− Linkages and Isolated Clusters in MOFs: A Few Illustrative Examples

    Inorganic Chemistry · 2008-09-29

    Partha Mahata, N. Manikanda Prabu, Srinivasan Natarajan

    Read original paper ↗ ·

  29. Control of polymorphism in NaNbO 3 by hydrothermal synthesis

    Chemical Communications · 2008-11-12

    Deena R. Modeshia, Richard J. Darton, Sharon Elizabeth Ashbrook, Richard I. Walton

    Read original paper ↗ ·

  30. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  31. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  32. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  33. Copyright Page

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  34. Dedication

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  35. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  36. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  37. Preface

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  38. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  39. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  40. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

    Read original paper ↗ ·

  41. Nanoscale Chemistry of Uranyl Selenates

    Springer eBooks · 2011-01-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  42. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

    Read original paper ↗ ·

  43. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

    Angewandte Chemie · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

    Read original paper ↗ ·

  44. Steric-Induced Layer Flection in Templated Vanadium Tellurites

    Crystal Growth & Design · 2013-04-02

    Kelvin B. Chang, Matthew D. Smith, Samuel M. Blau, Ethan C. Glor, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

    Read original paper ↗ ·

  45. Bismuth Tri‐ and Tetraarylcarboxylates: Crystal Structures, In Situ X‐ray Diffraction, Intermediates and Luminescence

    Chemistry - A European Journal · 2013-07-29

    Mark Feyand, Milan Köppen, Gernot Friedrichs, Norbert Stock

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  46. Nonaqueous synthesis of molecular zinc amide phosphate

    Journal of Organometallic Chemistry · 2013-10-09

    Jan Chyba, Z. Moravec, Marek Nečas, Sanjay Mathur, Jiří Pinkas

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  47. Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

    Angewandte Chemie International Edition · 2016-03-09

    Yue Wu, Matthew I. Breeze, Guy J. Clarkson, Franck Millange, Dermot O’Hare, Richard I. Walton

    Read original paper ↗ ·

  48. Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

    Angewandte Chemie · 2016-03-09

    Yue Wu, Matthew I. Breeze, Guy J. Clarkson, Franck Millange, Dermot O’Hare, Richard I. Walton

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  49. Synthesis and crystal-chemical features of two new uranyl chromates with the structures derived from [(UO2)(T6+O4)(H2O) n ]0 (T = Cr6+, S6+, Se6+, n = 0–2)

    Radiochemistry · 2016-11-01

    Еvgeny V. Nazarchuk, Oleg I. Siidra, Roman A. Kayukov

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  50. Organization of Copper Azide Clusters into Two‐Dimensional Structures: Synthesis, Structure, and Magnetic Properties

    European Journal of Inorganic Chemistry · 2017-02-06

    Subhradeep Mistry, Subramanian Yashonath, Srinivasan Natarajan

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