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RESEARCH PAPER · Inorganic Chemistry · 2003

Synthesis of a Single Four-Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single-Crystal and in-Situ MAS NMR Investigation

Srinivasan Natarajan, Leo van Wüllen, Wilhelm Klein, Martin Jansen

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Synthesis of a Single Four-Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single-Crystal and in-Situ MAS NMR InvestigationOriginalSynthesis of a Single Four‐Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single‐Crystal and in situ MAS NMR Investigation.122 New compounds and structures in the solid state2Synthesis, structure and luminescent properties of yttrium benzene dicarboxylates with one- and three-dimensional structure151Synthesis and Characterization of a Molecular Zinc Phosphate Ni(2, 2'‐bipy)3·[ZnCl(H2PO4)3]420 New compounds and structures in the solid state5A two-dimensional cationic lattice built from [Zn6(HPO4)2(PO4)2]2+ clusters57New Zinc Phosphates Decorated by Imidazole-Containing Ligands95Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules6Five New Zinc Phosphite Structures: Tertiary Building Blocks in the Construction of Hybrid Materials75[Zn(H2PO4)4]2− clusters and ∞[Zn2(HPO4)3(H2PO4)2]4− layers in two new zinc phosphates templated by [H2(4-amino-2.2.6.6-tetramethylpiperidine)]2+ cations7Hydrothermal Synthesis, Crystal Structure, and Characterization of a Two-Dimensional Open-Framework Zinc Phosphate Templated by Hexylamine: [C6H16N]·[Zn(HPO4)Cl]0Novel Zinc Phosphate Topologies Defined by Organic Ligands95{Zn3(Et2O)2[(EtO)PO2(C6H5NH)]6·2THF}: A Trinuclear Zinc Amidophosphate with an Hourglass Structure6Hydrothermal synthesis and structures of two zero-dimensional zinc phosphate polymorphs4Hydrothermal synthesis and characterization of a new three-dimensional hybrid zinc phosphate [Zn2(HPO4)2(4,4′-bipy)]·3H2O with neutral porous framework15A tetranuclear zinc cluster, (bipy)4Zn4(HPO3)4, that stabilizes a hydrogen bonded chain of water molecules: Transformation of a zinc phosphite 4-ring to a cluster16Polymorphism of [Zn(2,2′‐bipy)(H2PO4)2]26Hydrothermal synthesis, structure and magnetic properties of a new three-dimensional iron arsenate [C6N4H21][FeIII3(HAsO4)6]4Synthesis of open-framework zinc phosphite structures of varying dimensionality17A trinuclear cobalt(III) phosphate complex with a novel molecular structure: Synthesis and crystal structure of {[Co(en)2]3(PO4)(HPO4)}2(H2PO4)Cl7· 6H2O8Amine‐Intercalated Layered SnII Phosphates with Open‐Framework Structures7(C5H14N2)[Zn3(HPO4)4], a New 3D Open‐framework Zincophosphate Synthesized by Hydrothermal Reversible Transformation of (C5H14N2)[Zn2(HPO4)3]·H2O3Hydrothermal synthesis and characterization of a new organic templated metallophosphate [Zn(H2PO4)2(HPO4)][C7H17N2]6Human neutrophil elastase and collagenase sequestration with phosphorylated cotton wound dressings45Oxyfluorotitanophosphate Cluster [Ti10P4O16F44]16−: Synthesis and Characterization of K16[Ti10P4O16F44]21Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370Role of Temperature and Time in the Formation of Infinite −M−O−M− Linkages and Isolated Clusters in MOFs: A Few Illustrative Examples163On the Sn(II) and Sn(IV) incorporation into the AFI-structured AlPO4-based framework: the first significantly acidic SnAPO-530Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Time- and Temperature-Dependent Study in the Three-Component Zinc-Triazolate-Oxybis(benzoate) System: Stabilization of New Topologies57Synthesis, characterization, and catalytic behavior of two open-framework zinc phosphites with 2D and 3D structures5Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques39[Zn5(PO4)(HPO4)4(Hbpy)2(bpy)][H2PO4]·H2O: a novel inorganic–organic metal-phosphate framework showing an unprecedented (3,4)-connected (4·62)6(4·62·103)2(64·102)2 topology and the coexistence of various phosphates10Solid State and Solution Mediated Multistep Sequential Transformations in Metal–Organic Coordination Networks32Syntheses, crystal structures of a series of novel alkali metal or alkaline earth metal phosphites21Nonaqueous synthesis of molecular zinc amide phosphate4Recent NMR developments applied to organic–inorganic materials89Outlining the mechanism of flame retardancy in polyamide 66 blended with melamine-poly(zinc phosphate)39Is Single-4-Ring the Most Basic but Elusive Secondary Building Unit That Transforms to Larger Structures in Zinc Phosphate Chemistry?24Octanuclear Zinc Phosphates with Hitherto Unknown Cluster Architectures: Ancillary Ligand and Solvent Assisted Structural Transformations Thereof33Synthesis, physico-chemical studies and Hirshfeld surface analysis of a first 0-D Chlorozincophosphate, (H2N(CH2)4NH(CH2)2NH3Cl)ZnCl2(HPO4)3Crystal structure, physico-chemical characterization and Hirshfeld surface analysis of a new 0D pyridinium dichlorido(dihydrogenphosphato-O,O′)zinc(II)1Molecular di- and tetra-nuclear zinc(II) phosphates with sterically hindered aryl phosphate mono esters ligands2Synthesis, crystal structure, vibrational studies, optical properties and DFT calculation of a new Bi(III) halide complex: (C9H14N3)4[Bi2Cl11][BiCl6].4H2O3

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  1. Synthesis of a Single Four‐Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single‐Crystal and in situ MAS NMR Investigation.

    ChemInform · 2003-11-26

    Srinivasan Natarajan, Leo van Wuellen, Wilhelm Klein, Martin Jansen

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  2. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2004-01-01

    Gary B. Hix

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  3. Synthesis, structure and luminescent properties of yttrium benzene dicarboxylates with one- and three-dimensional structure

    Dalton Transactions · 2004-01-01

    A. Thirumurugan, Srinivasan Natarajan

    Read original paper ↗ ·

  4. Synthesis and Characterization of a Molecular Zinc Phosphate Ni(2, 2'‐bipy)3·[ZnCl(H2PO4)3]

    Zeitschrift für anorganische und allgemeine Chemie · 2004-12-17

    Zhien Lin, Jie Zhang, Shou‐Tian Zheng, Guo‐Yu Yang

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  5. 20 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2005-01-01

    Gary B. Hix

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  6. A two-dimensional cationic lattice built from [Zn6(HPO4)2(PO4)2]2+ clusters

    Chemical Communications · 2005-01-01

    Jian Fan, Brian E. Hanson

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  7. New Zinc Phosphates Decorated by Imidazole-Containing Ligands

    Inorganic Chemistry · 2005-01-13

    Jian Fan, Carla Slebodnick, Ross John Angel, Brian E. Hanson

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  8. Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules

    Journal of Solid State Chemistry · 2005-02-15

    Michael Wiebcke, Clemens Kühn, Gerhard Wildermuth

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  9. Five New Zinc Phosphite Structures: Tertiary Building Blocks in the Construction of Hybrid Materials

    Inorganic Chemistry · 2005-03-23

    Jian Fan, Carla Slebodnick, Diego Troya, Ross John Angel, Brian E. Hanson

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  10. [Zn(H2PO4)4]2− clusters and ∞[Zn2(HPO4)3(H2PO4)2]4− layers in two new zinc phosphates templated by [H2(4-amino-2.2.6.6-tetramethylpiperidine)]2+ cations

    Journal of Solid State Chemistry · 2005-04-24

    A. Dakhlaoui, V. Maisonneuve, M. Leblanc, Leila Samia Smiri

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  11. Hydrothermal Synthesis, Crystal Structure, and Characterization of a Two-Dimensional Open-Framework Zinc Phosphate Templated by Hexylamine: [C6H16N]·[Zn(HPO4)Cl]

    Phosphorus, sulfur, and silicon and the related elements · 2005-08-01

    A. Dakhlaoui, Leila Samia Smiri, Ahmed Driss

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  12. Novel Zinc Phosphate Topologies Defined by Organic Ligands

    Inorganic Chemistry · 2005-09-10

    Jian Fan, Brian E. Hanson

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  13. {Zn3(Et2O)2[(EtO)PO2(C6H5NH)]6·2THF}: A Trinuclear Zinc Amidophosphate with an Hourglass Structure

    Inorganic Chemistry · 2005-09-21

    Zhiyong Fu, T. Chivers

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  14. Hydrothermal synthesis and structures of two zero-dimensional zinc phosphate polymorphs

    Solid State Sciences · 2005-10-25

    Srinivasan Natarajan

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  15. Hydrothermal synthesis and characterization of a new three-dimensional hybrid zinc phosphate [Zn2(HPO4)2(4,4′-bipy)]·3H2O with neutral porous framework

    Journal of Solid State Chemistry · 2005-11-12

    Lei Wang, Ming Yang, Guanghua Li, Zhan Shi, Shouhua Feng

    Read original paper ↗ ·

  16. A tetranuclear zinc cluster, (bipy)4Zn4(HPO3)4, that stabilizes a hydrogen bonded chain of water molecules: Transformation of a zinc phosphite 4-ring to a cluster

    Inorganic Chemistry Communications · 2005-12-01

    Jian Fan, Carla Slebodnick, Brian E. Hanson

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  17. Polymorphism of [Zn(2,2′‐bipy)(H2PO4)2]2

    Zeitschrift für anorganische und allgemeine Chemie · 2005-12-09

    Srinivasan Natarajan, Yurii M. Prots', Bastian Ewald, Rainer Niewa, Rüdiger Kniep

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  18. Hydrothermal synthesis, structure and magnetic properties of a new three-dimensional iron arsenate [C6N4H21][FeIII3(HAsO4)6]

    Materials Research Bulletin · 2006-03-01

    Vandavasi Koteswara Rao, Srinivasan Natarajan

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  19. Synthesis of open-framework zinc phosphite structures of varying dimensionality

    Solid State Sciences · 2006-03-01

    Sukhendu Bikas Mandal, Srinivasan Natarajan

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  20. A trinuclear cobalt(III) phosphate complex with a novel molecular structure: Synthesis and crystal structure of {[Co(en)2]3(PO4)(HPO4)}2(H2PO4)Cl7· 6H2O

    Inorganic Chemistry Communications · 2006-04-23

    R.P. Sharma, R.P. Sharma, R.P. Sharma, R.P. Sharma, Ritu Bala, M. Quirós, Juan Manuel Salas

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  21. Amine‐Intercalated Layered SnII Phosphates with Open‐Framework Structures

    European Journal of Inorganic Chemistry · 2006-07-11

    Padmini Ramaswamy, Srinivasan Natarajan

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  22. (C5H14N2)[Zn3(HPO4)4], a New 3D Open‐framework Zincophosphate Synthesized by Hydrothermal Reversible Transformation of (C5H14N2)[Zn2(HPO4)3]·H2O

    Zeitschrift für anorganische und allgemeine Chemie · 2006-12-11

    Michael Wiebcke

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  23. Hydrothermal synthesis and characterization of a new organic templated metallophosphate [Zn(H2PO4)2(HPO4)][C7H17N2]

    Polyhedron · 2006-12-14

    R. Kefi, Chérif Ben Nasr, Frédéric Lefebvre, M. Rzaigui

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  24. Human neutrophil elastase and collagenase sequestration with phosphorylated cotton wound dressings

    Journal of Biomedical Materials Research Part A · 2007-05-03

    Judson Vincent Edwards, Phyllis S. Howley

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  25. Oxyfluorotitanophosphate Cluster [Ti10P4O16F44]16−: Synthesis and Characterization of K16[Ti10P4O16F44]

    Inorganic Chemistry · 2008-02-01

    Sihai Yang⧫, Guobao Li, Alexander J. Blake, Junliang Sun, Ming Xiong, Fuhui Liao, Jianhua Lin

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  26. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  27. Role of Temperature and Time in the Formation of Infinite −M−O−M− Linkages and Isolated Clusters in MOFs: A Few Illustrative Examples

    Inorganic Chemistry · 2008-09-29

    Partha Mahata, N. Manikanda Prabu, Srinivasan Natarajan

    Read original paper ↗ ·

  28. On the Sn(II) and Sn(IV) incorporation into the AFI-structured AlPO4-based framework: the first significantly acidic SnAPO-5

    Journal of Materials Chemistry · 2009-01-01

    Manuel Sánchez‐Sánchez, Rafael van Grieken, David Pedro Serrano, Juan Antonio Melero

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  29. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  30. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  31. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  32. Copyright Page

    Unknown journal · 2009-01-22

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  33. Dedication

    Unknown journal · 2009-01-22

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  34. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  35. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  36. Preface

    Unknown journal · 2009-01-22

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  37. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  38. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  39. Time- and Temperature-Dependent Study in the Three-Component Zinc-Triazolate-Oxybis(benzoate) System: Stabilization of New Topologies

    Crystal Growth & Design · 2009-06-23

    Partha Mahata, N. Manikanda Prabu, Srinivasan Natarajan

    Read original paper ↗ ·

  40. Synthesis, characterization, and catalytic behavior of two open-framework zinc phosphites with 2D and 3D structures

    Inorganic Chemistry Communications · 2010-10-17

    Desheng Song, Dongpo Su, Zhiyong Fu, Shijun Liao

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  41. Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques

    The Journal of Physical Chemistry C · 2011-03-07

    Andrew Michael Beale, Matthew G. O’Brien, Marta Kasunič, Amalija Golobič, Manuel Sánchez‐Sánchez, Alan J. W. Lobo, Dewi W. Lewis, David Stephen Wragg, Sergey Nikitenko, Wim Bras, Bert Marc Weckhuysen

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  42. [Zn5(PO4)(HPO4)4(Hbpy)2(bpy)][H2PO4]·H2O: a novel inorganic–organic metal-phosphate framework showing an unprecedented (3,4)-connected (4·62)6(4·62·103)2(64·102)2 topology and the coexistence of various phosphates

    CrystEngComm · 2012-01-01

    Wenyuan Xu, Xiao-Zhao Tian, Gong‐Ming Sun, Yu‐Mei Song, Hai-xiao Huang, Yan Zhu, Zi-Zun Yuan, Xue-feng Feng, Mingbiao Luo, Shujuan Liu, Feng Luo

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  43. Solid State and Solution Mediated Multistep Sequential Transformations in Metal–Organic Coordination Networks

    Crystal Growth & Design · 2012-12-05

    Partha Mahata, Caroline-Mellot Draznieks, Partha Sarathi Roy, Srinivasan Natarajan

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  44. Syntheses, crystal structures of a series of novel alkali metal or alkaline earth metal phosphites

    CrystEngComm · 2013-01-01

    Xi-Jia Wang, Jian‐Han Zhang, Jun‐Ling Song, Fang Kong, Jiang‐Gao Mao

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  45. Nonaqueous synthesis of molecular zinc amide phosphate

    Journal of Organometallic Chemistry · 2013-10-09

    Jan Chyba, Z. Moravec, Marek Nečas, Sanjay Mathur, Jiří Pinkas

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  46. Recent NMR developments applied to organic–inorganic materials

    Progress in Nuclear Magnetic Resonance Spectroscopy · 2013-10-26

    Christian Bonhomme, Christel Gervais, Danielle Laurencin

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  47. Outlining the mechanism of flame retardancy in polyamide 66 blended with melamine-poly(zinc phosphate)

    Fire Safety Journal · 2014-10-11

    Anil Damodar Naik, Gaëlle Fontaine, Fabienne Samyn, Xavier Delva, Jérémie Louisy, Séverine Bellayer, Yann Bourgeois, Serge Bourbigot

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  48. Is Single-4-Ring the Most Basic but Elusive Secondary Building Unit That Transforms to Larger Structures in Zinc Phosphate Chemistry?

    Inorganic Chemistry · 2015-05-04

    Aijaz Ahmad Dar, Sunil K. Sharma, Ramaswamy Murugavel

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  49. Octanuclear Zinc Phosphates with Hitherto Unknown Cluster Architectures: Ancillary Ligand and Solvent Assisted Structural Transformations Thereof

    Inorganic Chemistry · 2015-09-14

    Aijaz A. Dar, Saumik Sen, Sandeep K. Gupta, G. Naresh Patwari, Ramaswamy Murugavel

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  50. Synthesis, physico-chemical studies and Hirshfeld surface analysis of a first 0-D Chlorozincophosphate, (H2N(CH2)4NH(CH2)2NH3Cl)ZnCl2(HPO4)

    Journal of Materials Science Materials in Electronics · 2018-06-15

    Ali Rayes, Sofian Gatfaoui, Chérif Ben Nasr, Brahim Ayed, Mohamed Rzaigui A

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