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RESEARCH PAPER · Angewandte Chemie International Edition · 2002

A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

Sandip Chakrabarti, Srinivasan Natarajan

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A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron ArsenatesOriginal22 New compounds and structures in the solid state2Hydrothermal synthesis and structure of a zinc arsenate–oxalate, [NH3(CH2)3NH2(CH2)3NH3][Zn3(AsO4)(HAsO4)2(C2O4)], and a zinc arsenate, [{NH3(CH3)2NH2(CH3)3NH3}2][Zn6(AsO4)4(HAsO4)3]·H2O, with three-dimensional structures16ChemInform Abstract: A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One‐Dimensional Iron Arsenate Oxalate and Its Transformation into Two‐ and Three‐Dimensional Iron Arsenates.021 New compounds and structures in the solid state1Synthesis and structure of a new three-dimensional indium phosphate with 16-membered one-dimensional channelsElectronic supplementary information (ESI) available: TGA analysis and 1H decoupled 31P MAS NMR spectrum for I. See http://www.rsc.org/suppdata/dt/b3/b303998f/34Organically Templated Linear and Layered Iron Sulfates103Synthesis, Structure and Magnetic Properties of a New Iron Arsenate, [C10N4H28][{FeF(OH)(HAsO4)}4], with a Layer Structure24Metal Carboxylates with Open Architectures1935Offene Metallcarboxylat‐Architekturen179Hydrothermal Synthesis, Structure and Magnetic Properties of a One‐Dimensional Iron Arsenate, 1∞[NH3(CH2)2NH(CH2)2NH3][Fe2F4(HAsO4)2]21The First One-Dimensional Iron Phosphite−Phosphate, [FeIII(2,2‘-bipyridine)(HPO3)(H2PO4)]: Synthesis, Structure, and Magnetic Properties43Iron: Inorganic & Coordination ChemistryBased in part on the article Iron: Inorganic & Coordination Chemistry by Pelham N. Hawker & Martyn V. Twigg which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .9Iron: Inorganic & Coordination ChemistryBased in part on the article Iron: Inorganic & Coordination Chemistry by Pelham N. Hawker & Martyn V. Twigg which appeared in theEncyclopedia of Inorganic Chemistry, First Edition.2Organically-templated metal sulfates, selenites and selenates194Hydrothermal synthesis, structure and magnetic properties of a new three-dimensional iron arsenate [C6N4H21][FeIII3(HAsO4)6]4Fe2(AsO4)F: A new three-dimensional condensed fluoro-arsenate iron(II) compound with antiferromagnetic interactions14Inorganic–organic hybrid structures: Synthesis, structure and magnetic properties of a new iron oxalatoarsenate, [NH3(CH2)CH(NH3)CH3]3[Fe6(AsO4)2(HAsO4)6(C2O4)3]8A New Organically Templated Zinc Phosphite Synthesized in Phosphorous Acid Flux and Its Hydrothermal Analogue22Inorganic–Organic Hybrid Structures: Open‐Framework Iron Phosphite–Oxalates of Varying Dimensionality44Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane39Inter-relationship between the structures of metal-organic frameworks: is there a role for an intermediate?0Iron arsenate frameworks8Synthesis, Structure, and Magnetic Properties of a Novel Pillared Layered Iron(III) Arsenate, [4,4‘-bpyH2]3[Fe9(H2O)6F3(HAsO4)12(AsO4)2]·2H2O9Amine-Templated Open-Framework Zinc Arsenates of Varying Dimensionalities: Synthesis, Structure, Polymorphism, and Transformation Reactions34Preparation and structure of [Cr2IIIF3(TPyA)2](BF4)3 [TPyA = tris(2-pyridylmethyl)amine] possessing terminal and bridging fluorides14Offene Gerüststrukturen von Übergangsmetallen24Open‐Framework Structures of Transition‐Metal Compounds380New indium selenite-oxalate and indium oxalate with two- and three-dimensional structures11A family of 3D lanthanide oxalatosuccinate with rare structures: 3D host framework incorporating a 3D alkali metal guest lattice15Mild hydrothermal synthesis, crystal structure, thermal behavior, spectroscopic and magnetic properties of the (NH4)[Fe(AsO4)1−x(PO4)xF] (x=0.3, 0.6, 0.8) series. Thermal transformation of (NH4)[Fe(AsO4)0.7(PO4)0.3F] into the textural porous orthorhombic Fe(AsO4)0.7(PO4)0.34Formation of a 3D Porous Ferric Arsenate Containing Novel Cubane-like Fe4F4 Building Units3Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium36Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18Hierarchy of structures in the family of amine templated open-framework gallium arsenates2Two novel organic amine templated lanthanide sulfates: Layer H3DETA · [Nd(H2O)(SO4)3] and chain-like H3DETA · [Ho(H2O)2(SO4)3]1Lanthanide Sulfate Frameworks: Synthesis, Structure, and Optical Properties31Organic‐inorganic Hybrid Lanthanide‐Silver Heterometallic Coordination Frameworks Constructed from Oxalate and Sulfate Anion: Syntheses, Structures, and Photoluminescent Properties10Mild hydrothermal synthesis, crystal structure, thermal behaviour, spectroscopic and magnetic properties of (NH4)0.80Li0.20[Fe(AsO4)F]1Syntheses, Characterization, and Magnetic Studies of Copper(II) Complexes with the Ligand N,N,N′,N′-Tetrakis(2-pyridylmethyl)-1,3-benzenediamine (1,3-tpbd) and its Phenol Derivative 2,6-Bis[bis(2-pyridylmethyl)amino]-p-cresol] (2,6-Htpcd)10A series of boroselenite-based open frameworks mediated by the cationic sizes of the alkali metals25Solvothermal synthesis, structure and characterization of 1D chain and 2D layered rare earth sulfates in the presence of cyclic diamines4The synthesis, structure and magnetism studies of two manganese sulfates with a 3D zeolite GIS framework and 1D chain structure8Unprecedented Trapping of Difluorooctamolybdate Anions within an α-Polonium Type Coordination Network13Materials1The Lead Coordination Polymers Containing Pyrazine-2,3-Dicarboxylic Acid: Rapid Structural Transformations and Cation Exchange25Three rare Ln–Na heterometallic 3D polymers based on sulfate anion: Syntheses, structures, and luminescence properties13Fluorescent Metal–Organic Frameworks for Selective Sensing of Toxic Cations (Tl3+, Hg2+) and Highly Oxidizing Anions ((CrO4)2−, (Cr2O7)2−, (MnO4)−)78Extra-large-pore metal sulfate-oxalates with diamondoid and zeolitic frameworks6Lead–Organic Frameworks Containing Trimesic Acid: Facile Dissolution–Crystallization and Near-White Light Emission15Piperazine-1,4-diol (PipzDiol): synthesis, stereodynamics and assembly of supramolecular hydrogen-bonded 2D networks6

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  1. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

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  2. Hydrothermal synthesis and structure of a zinc arsenate–oxalate, [NH3(CH2)3NH2(CH2)3NH3][Zn3(AsO4)(HAsO4)2(C2O4)], and a zinc arsenate, [{NH3(CH3)2NH2(CH3)3NH3}2][Zn6(AsO4)4(HAsO4)3]·H2O, with three-dimensional structures

    Journal of the Chemical Society Dalton Transactions · 2002-01-01

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  3. ChemInform Abstract: A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One‐Dimensional Iron Arsenate Oxalate and Its Transformation into Two‐ and Three‐Dimensional Iron Arsenates.

    ChemInform · 2002-07-02

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  4. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2003-01-01

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  5. Synthesis and structure of a new three-dimensional indium phosphate with 16-membered one-dimensional channelsElectronic supplementary information (ESI) available: TGA analysis and 1H decoupled 31P MAS NMR spectrum for I. See http://www.rsc.org/suppdata/dt/b3/b303998f/

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  6. Organically Templated Linear and Layered Iron Sulfates

    Chemistry of Materials · 2003-02-15

    Geo Paul, Amitava Choudhury, C.N.R. Rao

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  7. Synthesis, Structure and Magnetic Properties of a New Iron Arsenate, [C10N4H28][{FeF(OH)(HAsO4)}4], with a Layer Structure

    European Journal of Inorganic Chemistry · 2003-10-01

    Sandip Chakrabarti, Swapan Kumar Pati, Mark Green, Srinivasan Natarajan

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  8. Metal Carboxylates with Open Architectures

    Angewandte Chemie International Edition · 2004-03-09

    C. N. R. Rao, Srinivasan Natarajan, Ramanathan Vaidhyanathan

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  9. Offene Metallcarboxylat‐Architekturen

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    C. N. R. Rao, Srinivasan Natarajan, R. Vaidhyanathan

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  10. Hydrothermal Synthesis, Structure and Magnetic Properties of a One‐Dimensional Iron Arsenate, 1∞[NH3(CH2)2NH(CH2)2NH3][Fe2F4(HAsO4)2]

    European Journal of Inorganic Chemistry · 2004-07-27

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  11. The First One-Dimensional Iron Phosphite−Phosphate, [FeIII(2,2‘-bipyridine)(HPO3)(H2PO4)]: Synthesis, Structure, and Magnetic Properties

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    Sukhendu Bikas Mandal, Swapan Kumar Pati, Mark Green, Srinivasan Natarajan

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  12. Iron: Inorganic & Coordination ChemistryBased in part on the article Iron: Inorganic & Coordination Chemistry by Pelham N. Hawker & Martyn V. Twigg which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .

    Encyclopedia of Inorganic Chemistry · 2005-09-07

    John R. Burgess, MARTYN V. TWIGG

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  13. Iron: Inorganic & Coordination ChemistryBased in part on the article Iron: Inorganic & Coordination Chemistry by Pelham N. Hawker & Martyn V. Twigg which appeared in theEncyclopedia of Inorganic Chemistry, First Edition.

    Encyclopedia of Inorganic and Bioinorganic Chemistry · 2005-09-07

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  14. Organically-templated metal sulfates, selenites and selenates

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  15. Hydrothermal synthesis, structure and magnetic properties of a new three-dimensional iron arsenate [C6N4H21][FeIII3(HAsO4)6]

    Materials Research Bulletin · 2006-03-01

    Vandavasi Koteswara Rao, Srinivasan Natarajan

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  16. Fe2(AsO4)F: A new three-dimensional condensed fluoro-arsenate iron(II) compound with antiferromagnetic interactions

    Journal of Solid State Chemistry · 2006-03-03

    Teresa Berrocal, Jose Luis Mesa, José Luis Pizarro, M. Karmele Urtiaga, María Isabel Arriortua, Teófilo Rojo

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  17. Inorganic–organic hybrid structures: Synthesis, structure and magnetic properties of a new iron oxalatoarsenate, [NH3(CH2)CH(NH3)CH3]3[Fe6(AsO4)2(HAsO4)6(C2O4)3]

    Solid State Sciences · 2006-04-05

    Vandavasi Koteswara Rao, Kinson C. Kam, Anthony Kevin Cheetham, Srinivasan Natarajan

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  18. A New Organically Templated Zinc Phosphite Synthesized in Phosphorous Acid Flux and Its Hydrothermal Analogue

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    Zhien Lin, Wei Fan, Feifei Gao, Naotaka Chino, Toshiyuki Yokoi, Tatsuya Okubo

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  19. Inorganic–Organic Hybrid Structures: Open‐Framework Iron Phosphite–Oxalates of Varying Dimensionality

    Chemistry - A European Journal · 2006-10-25

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  20. Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane

    New Journal of Chemistry · 2006-11-24

    R. Atencio, Alexander Briceño, Pedro J. Silva, José A. Rodríguez, Jonathan C. Hanson

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  21. Inter-relationship between the structures of metal-organic frameworks: is there a role for an intermediate?

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  22. Iron arsenate frameworks

    Dalton Transactions · 2007-01-01

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  23. Synthesis, Structure, and Magnetic Properties of a Novel Pillared Layered Iron(III) Arsenate, [4,4‘-bpyH2]3[Fe9(H2O)6F3(HAsO4)12(AsO4)2]·2H2O

    The Journal of Physical Chemistry B · 2007-10-17

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  24. Amine-Templated Open-Framework Zinc Arsenates of Varying Dimensionalities: Synthesis, Structure, Polymorphism, and Transformation Reactions

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  25. Preparation and structure of [Cr2IIIF3(TPyA)2](BF4)3 [TPyA = tris(2-pyridylmethyl)amine] possessing terminal and bridging fluorides

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  26. Offene Gerüststrukturen von Übergangsmetallen

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  27. Open‐Framework Structures of Transition‐Metal Compounds

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  28. New indium selenite-oxalate and indium oxalate with two- and three-dimensional structures

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  29. A family of 3D lanthanide oxalatosuccinate with rare structures: 3D host framework incorporating a 3D alkali metal guest lattice

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  30. Mild hydrothermal synthesis, crystal structure, thermal behavior, spectroscopic and magnetic properties of the (NH4)[Fe(AsO4)1−x(PO4)xF] (x=0.3, 0.6, 0.8) series. Thermal transformation of (NH4)[Fe(AsO4)0.7(PO4)0.3F] into the textural porous orthorhombic Fe(AsO4)0.7(PO4)0.3

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  31. Formation of a 3D Porous Ferric Arsenate Containing Novel Cubane-like Fe4F4 Building Units

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  32. Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium

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  33. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

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  34. Hierarchy of structures in the family of amine templated open-framework gallium arsenates

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  35. Two novel organic amine templated lanthanide sulfates: Layer H3DETA · [Nd(H2O)(SO4)3] and chain-like H3DETA · [Ho(H2O)2(SO4)3]

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  36. Lanthanide Sulfate Frameworks: Synthesis, Structure, and Optical Properties

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  37. Organic‐inorganic Hybrid Lanthanide‐Silver Heterometallic Coordination Frameworks Constructed from Oxalate and Sulfate Anion: Syntheses, Structures, and Photoluminescent Properties

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  38. Mild hydrothermal synthesis, crystal structure, thermal behaviour, spectroscopic and magnetic properties of (NH4)0.80Li0.20[Fe(AsO4)F]

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  39. Syntheses, Characterization, and Magnetic Studies of Copper(II) Complexes with the Ligand N,N,N′,N′-Tetrakis(2-pyridylmethyl)-1,3-benzenediamine (1,3-tpbd) and its Phenol Derivative 2,6-Bis[bis(2-pyridylmethyl)amino]-p-cresol] (2,6-Htpcd)

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  40. A series of boroselenite-based open frameworks mediated by the cationic sizes of the alkali metals

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  42. The synthesis, structure and magnetism studies of two manganese sulfates with a 3D zeolite GIS framework and 1D chain structure

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  43. Unprecedented Trapping of Difluorooctamolybdate Anions within an α-Polonium Type Coordination Network

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  44. Materials

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  46. Three rare Ln–Na heterometallic 3D polymers based on sulfate anion: Syntheses, structures, and luminescence properties

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  47. Fluorescent Metal–Organic Frameworks for Selective Sensing of Toxic Cations (Tl3+, Hg2+) and Highly Oxidizing Anions ((CrO4)2−, (Cr2O7)2−, (MnO4)−)

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  49. Lead–Organic Frameworks Containing Trimesic Acid: Facile Dissolution–Crystallization and Near-White Light Emission

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