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RESEARCH PAPER · Angewandte Chemie · 2016

Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

Yue Wu, Matthew I. Breeze, Guy J. Clarkson, Franck Millange, Dermot M. O'Hare, Richard I. Walton

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Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray DiffractionOriginalTime‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation38Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation10From a Metastable Layer to a Stable Ring: A Kinetic Study for Transformation Reactions of Li2Mo3TeO12 to Polyoxometalates12Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes41Atomic Force Microscopy Study of the Influence of the Synthesis Conditions on the Single‐Crystal Surface of Interdigitated Metal‐Organic Frameworks9Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20In-situ IR monitoring to probe the formation of structural defects in Zr-fumarate metal–organic framework (MOF)19Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species66Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species4The Chemistry of Nucleation: In Situ Pair Distribution Function Analysis of Secondary Building Units During UiO‐66 MOF Formation117In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**23Two Substituted-Tetrazole Based D10 Isomers of M2(Ppt)(Oh)(So4)(H2o) (M = Zn, Cd): The In-Situ Syntheses and Characterization0Two substituted tetrazole-based isomers of [M2(PPT)(OH)(SO4)(H2O)]n (M = Zn, Cd): The in-situ syntheses and characterization2In situ X‐ray Scattering of the Crystallisation of Basic Magnesium Chlorides using a Laboratory Instrument1

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  1. Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation

    Angewandte Chemie International Edition · 2016-10-11

    Yue Wu, Sebastian Henke, Gregor Kieslich, Inke Schwedler, Miaosen Yang, Duncan A. X. Fraser, Dermot M. O'Hare

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  2. Time‐Resolved In Situ X‐ray Diffraction Reveals Metal‐Dependent Metal–Organic Framework Formation

    Angewandte Chemie · 2016-10-11

    Yue Wu, Sebastian Henke, Gregor Kieslich, Inke Schwedler, Miaosen Yang, Duncan A. X. Fraser, Dermot M. O'Hare

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  3. From a Metastable Layer to a Stable Ring: A Kinetic Study for Transformation Reactions of Li2Mo3TeO12 to Polyoxometalates

    Chemistry - A European Journal · 2017-12-07

    Seung‐Jin Oh, Seong‐Ji Lim, Tae‐Soo You, Kang Min Ok

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  4. Green Synthesis of a New Al‐MOF Based on the Aliphatic Linker Mesaconic Acid: Structure, Properties and In Situ Crystallisation Studies of Al‐MIL‐68‐Mes

    Chemistry - A European Journal · 2017-12-11

    Helge Reinsch, Thomas Homburg, Niclas Heidenreich, Dominik Fröhlich, Stefan K. Henninger, Michael Wark, Norbert Stock

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  5. Atomic Force Microscopy Study of the Influence of the Synthesis Conditions on the Single‐Crystal Surface of Interdigitated Metal‐Organic Frameworks

    ChemPhysChem · 2018-05-10

    Yoshinobu Kamakura, Nobuhiko Hosono, Aya Terashima, Susumu Kitagawa, Hirofumi Yoshikawa, Daisuke Tanaka

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  6. Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity

    Chemistry - A European Journal · 2018-05-23

    L.A. Reith, Karla Lienau, Daniel Sean Cook, René Moré, Richard I. Walton, Greta Ricarda Patzke

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  7. In-situ IR monitoring to probe the formation of structural defects in Zr-fumarate metal–organic framework (MOF)

    Polyhedron · 2018-07-22

    Jianwei Ren, Nicholas Mulei Musyoka, Henrietta Wakuna Langmi, Joseph Walker, Mkhulu Kenneth Mathe, Shijun Liao

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  8. Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species

    Angewandte Chemie International Edition · 2018-11-15

    Hamish H.‐M. Yeung, Adam F. Sapnik, Felicity Massingberd‐Mundy, Michael W. Gaultois, Yue Wu, Duncan A. X. Fraser, Sebastian Henke, Roman Pallach, Niclas Heidenreich, Oxana V. Magdysyuk, Nghia Trong Vo, Andrew L. Goodwin

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  9. Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species

    Angewandte Chemie · 2018-11-15

    Hamish H.‐M. Yeung, Adam F. Sapnik, Felicity Massingberd‐Mundy, Michael W. Gaultois, Yue Wu, Duncan A. X. Fraser, Sebastian Henke, Roman Pallach, Niclas Heidenreich, Oxana V. Magdysyuk, Nghia Trong Vo, Andrew L. Goodwin

    Read original paper ↗ ·

  10. The Chemistry of Nucleation: In Situ Pair Distribution Function Analysis of Secondary Building Units During UiO‐66 MOF Formation

    Chemistry - A European Journal · 2018-11-27

    Hui Xu, Sanna Sommer, Nils Lau Nyborg Broge, Junkuo Gao, Bo B. Iversen

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  11. In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**

    Chemistry - A European Journal · 2021-01-22

    Stephen J. I. Shearan, Jannick Jacobsen, Ferdinando Costantino, Roberto D’Amato, Dmitri Novikov, Norbert Stock, Enrico Andreoli, Marco Taddei

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  12. Two Substituted-Tetrazole Based D10 Isomers of M2(Ppt)(Oh)(So4)(H2o) (M = Zn, Cd): The In-Situ Syntheses and Characterization

    SSRN Electronic Journal · 2022-01-01

    Zhehui Weng, Meiqiao Wei, Jingxia Song, Renjie Chen, Hanqing Liu, Ying Wang, Yong-Feng Qiao, Jie Ling, Tong Su, Haidong Ju, Xiao-Hua Zhou

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  13. Two substituted tetrazole-based isomers of [M2(PPT)(OH)(SO4)(H2O)]n (M = Zn, Cd): The in-situ syntheses and characterization

    Inorganica Chimica Acta · 2022-07-22

    Meiqiao Wei, Jingxia Song, Renjie Chen, Hanqing Liu, Ying Wang, Yong-Feng Qiao, Jie Ling, Tong Su, Haidong Ju, Xiao-Hua Zhou, Zhehui Weng

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  14. In situ X‐ray Scattering of the Crystallisation of Basic Magnesium Chlorides using a Laboratory Instrument

    Chemistry - Methods · 2022-08-09

    Katie S. Pickering, Steven Huband, Kirill L. Shafran, Richard I. Walton

    Read original paper ↗ ·
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