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RESEARCH PAPER · Journal of the American Chemical Society · 1999

Variable Dimensionality in the Uranium Fluoride/2-Methyl-Piperazine System: Syntheses and Structures of UFO-5, -6, and -7; Zero-, One-, and Two-Dimensional Materials with Unprecedented Topologies

R.J. Francis, P. Shiv Halasyamani, Jared S. Bee, Dermot O’Hare

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Variable Dimensionality in the Uranium Fluoride/2-Methyl-Piperazine System: Syntheses and Structures of UFO-5, -6, and -7; Zero-, One-, and Two-Dimensional Materials with Unprecedented TopologiesOriginal17 Scandium, yttrium, the lanthanides, the actinides and the post-actinides2Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster14Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride63Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties67Hydrothermal Syntheses, Structures, and Fluorescence Spectroscopy of New One-Dimensional Uranium Oxyfluorides Built from Edge-Sharing [UO2F5] Pentagonal Bipyramids78Synthesis and characterisation of (C4N2H12)(UO2)2(PO3H)2{PO2(OH)H}2: a three dimensionally connected actinide framework46Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]44Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions115Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F3143Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O22Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)73A New Oxoanion: [IO4]3-Containing I(V) with a Stereochemically Active Lone-Pair in the Silver Uranyl Iodate Tetraoxoiodate(V), Ag4(UO2)4(IO3)2(IO4)2O282Hydrothermal synthesis of the first organically templated open-framework uranium phosphate66Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)53Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides8[NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structure102Solid State Coordination Chemistry: Bimetallic Organophosphonate Oxide Phases of the M/Cu/O/RPO3 2− Family (M=V, Mo)0The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O29Organically templated uranium(vi) sulfates: understanding phase stability using composition space83Incorporation of uranium( vi ) into metal–organic framework solids, [UO 2 (C 4 H 4 O 4 )]·H 2 O, [UO 2 F(C 5 H 6 O 4 )]·2H 2 O, and [(UO 2 ) 1.5 (C 8 H 4 O 4 ) 2 ] 2 [(CH 3 ) 2 NCOH 2 ]·H 2 O98The Actinides34Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates56The effects of linear diamine chain length in uranium sulfates48[(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework852D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties78A novel scandium fluoride, [C2N2H10]0.5[ScF4], with an unprecedented tungsten bronze-related layer structure.20Crystal Chemistry of Some Organically Templated Metal Fluorides: The Crystal Structure of [C2N2H10]0.5[Y2F7]2[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Hydrothermal Synthesis and Structure of Zero-dimensional Organic–inorganic Perovskites26Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51Synthesis, Structure and Photoluminescent Studies of Two Novel Layered Uranium Coordination Polymers Constructed from UO(OH) Polyhedra and Pyridinedicarboxylates79Hydrothermal scandium fluoride chemistry: syntheses and crystal structures of [C2N2H10][ScF5], [NH4]2[Sc3F11] and [H3O][C6N2H16][ScF6]⋅H2O19UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)81An organically templated yttrium fluoride with a ‘Super-Diamond’ structure28Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6Bis[tris(2-ammonioethyl)amine] bis(pentafluoridooxidomolybdate) difluoride monohydrate5Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Synthetic Approaches for Noncentrosymmetric Molybdates59Oxo ligand functionalization in the uranyl ion (UO22+)335Time- and Temperature-Dependent Study in the Three-Component Zinc-Triazolate-Oxybis(benzoate) System: Stabilization of New Topologies57Structural chemistry of organically-templated metal fluorides61Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18Systematic Investigation of Zinc Aminoalkylphosphonates: Influence of the Alkyl Chain Lengths on the Structure Formation16Polymorph (C2N2H10)0.5RE3F10·xH2O (RE = Ho-Lu, Y) and REF3 nanocrystals: Hydrothermal synthesis, characterization and luminescence7Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Fluoride-coordination chemistry in molecular and low-dimensional magnetism67Hydrothermal syntheses and characterization of uranyl tungstates with electro-neutral structural units0Insight into the Uranyl Oxyfluoride Topologies through the Synthesis, Crystal Structure, and Evidence of a New Oxyfluoride Layer in [(UO2)4F13][Sr3(H2O)8](NO3)·H2O6Anionic uranyl oxyfluorides as a bifunctional platform for highly selective ion-exchange and photocatalytic degradation of organic dyes13Chromium chains as polydentate fluoride ligands for actinides and group IV metals4Organosoluble tetravalent actinide di- and trifluorides2[UF6]2−: A Molecular Hexafluorido Actinide(IV) Complex with Compensating Spin and Orbital Magnetic Moments13[UF6]2−: A Molecular Hexafluorido Actinide(IV) Complex with Compensating Spin and Orbital Magnetic Moments0Solubilité et fluoration d’oxydes d’uranium en milieu liquide ionique0Direct conversion of uranium dioxide UO 2 to uranium tetrafluoride UF 4 using the fluorinated ionic liquid [Bmim][PF 6 ]13

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  1. 17 Scandium, yttrium, the lanthanides, the actinides and the post-actinides

    Annual Reports Section A (Inorganic Chemistry) · 2000-01-01

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  2. Synthesis of the Neutral (CuF(NC5H5)4)2NbOF5 Cluster

    Chemistry of Materials · 2000-06-16

    Alexander J. Norquist, Margaret E. Welk, Charlotte L. Stern, Kenneth Reinhard Poeppelmeier

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  3. Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride

    Inorganic Chemistry · 2000-08-01

    Simon Allen, Stephen H. Barlow, P. Shiv Halasyamani, J. Frederick W. Mosselmans, Dermot O’Hare, Susan M. Walker, Richard I. Walton

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  4. Low-Dimensional Organically Templated Uranium Fluorides (C5H14N2)2U2F12·2H2O and (C2H10N2)U2F10: Hydrothermal Syntheses, Structures, and Magnetic Properties

    Chemistry of Materials · 2000-09-15

    Philip M. Almond, Laura Deakin, Melissa J. Porter, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  5. Hydrothermal Syntheses, Structures, and Fluorescence Spectroscopy of New One-Dimensional Uranium Oxyfluorides Built from Edge-Sharing [UO2F5] Pentagonal Bipyramids

    Journal of Solid State Chemistry · 2000-11-01

    Philip M. Almond, Catherine E. Talley, Amanda C. Bean, Shane M. Peper, Thomas E. Albrecht‐Schmitt

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  6. Synthesis and characterisation of (C4N2H12)(UO2)2(PO3H)2{PO2(OH)H}2: a three dimensionally connected actinide framework

    Chemical Communications · 2001-01-01

    M.B. Doran, Susan M. Walker, Dermot O’Hare

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  7. Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Organically Templated Uranium Aquofluoride: [C5H14N2][U2F10(H2O)]

    Inorganic Chemistry · 2001-01-17

    Philip M. Almond, Laura Deakin, Arthur Mar, Thomas E. Albrecht‐Schmitt

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  8. Structural Relationships, Interconversion, and Optical Properties of the Uranyl Iodates, UO2(IO3)2and UO2(IO3)2(H2O): A Comparison of Reactions under Mild and Supercritical Conditions

    Chemistry of Materials · 2001-03-20

    Amanda C. Bean, Shane M. Peper, Thomas E. Albrecht‐Schmitt

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  9. Hydrothermal Syntheses, Structures, and Magnetic Properties of the U(IV) Fluorides (C5H14N2)2U2F12·5H2O and (NH4)7U6F31

    Journal of Solid State Chemistry · 2001-04-01

    Philip M. Almond, Laura Deakin, A. Mar, Thomas E. Albrecht‐Schmitt

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  10. Organically Templated Zirconium Fluorides: Hydrothermal Syntheses, Structural Relationships, and Thermal Behavior of (C2H10N2)Zr2F10·H2O and (C4H12N2)ZrF6·H2O

    Journal of Solid State Chemistry · 2001-06-01

    Richard E. Sykora, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  11. Excision of Uranium Oxide Chains and Ribbons in the Novel One-Dimensional Uranyl Iodates K2[(UO2)3(IO3)4O2] and Ba[(UO2)2(IO3)2O2](H2O)

    Inorganic Chemistry · 2001-06-30

    Amanda C. Bean, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  12. A New Oxoanion: [IO4]3-Containing I(V) with a Stereochemically Active Lone-Pair in the Silver Uranyl Iodate Tetraoxoiodate(V), Ag4(UO2)4(IO3)2(IO4)2O2

    Journal of the American Chemical Society · 2001-08-15

    Amanda C. Bean, Charles F. Campana, Ohyun Kwon, Thomas E. Albrecht‐Schmitt

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  13. Hydrothermal synthesis of the first organically templated open-framework uranium phosphate

    Chemical Communications · 2001-10-31

    Janet A. Danis, Wolfgang H. Runde, Brian L. Scott, James C. Fettinger, Bryan W. Eichhorn

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  14. Cation Effects on the Formation of the One-Dimensional Uranyl Iodates A2[(UO2)3(IO3)4O2] (A=K, Rb, Tl) and AE[(UO2)2(IO3)2O2] (H2O) (AE=Sr, Ba, Pb)

    Journal of Solid State Chemistry · 2001-11-01

    Amanda C. Bean, Thomas E. Albrecht‐Schmitt

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  15. Poly(tetrafluoroethylene) Impregnation for Ion-Exchange Reactions with Layered Ce(IV) Fluorides

    Chemistry of Materials · 2001-11-17

    Richard E. Sykora, Thomas E. Albrecht‐Schmitt

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  16. [NC 4 H 12 ] 2 [(UO 2 ) 6 (H 2 O) 2 (SO 4 ) 7 ]: the first organically templated actinide sulfate with a three-dimensional framework structure

    Chemical Communications · 2002-01-01

    M.B. Doran, Alexander J. Norquist, Dermot O’Hare

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  17. Solid State Coordination Chemistry: Bimetallic Organophosphonate Oxide Phases of the M/Cu/O/RPO3 2− Family (M=V, Mo)

    Nanostructure science and technology · 2002-01-01

    Robert C. Finn, Jon A. Zubieta

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  18. The first organically templated thorium compounds, [C 4 N 2 H 12 ] 0.5 [ThF 5 ] and [C 5 N 2 H 14 ][ThF 6 ]·0.5H 2 O

    Chemical Communications · 2002-01-01

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  19. Organically templated uranium(vi) sulfates: understanding phase stability using composition space

    Journal of Materials Chemistry · 2002-11-12

    Paul M. Thomas, Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  20. Incorporation of uranium( vi ) into metal–organic framework solids, [UO 2 (C 4 H 4 O 4 )]·H 2 O, [UO 2 F(C 5 H 6 O 4 )]·2H 2 O, and [(UO 2 ) 1.5 (C 8 H 4 O 4 ) 2 ] 2 [(CH 3 ) 2 NCOH 2 ]·H 2 O

    Dalton Transactions · 2003-01-01

    Jong‐Young Kim, Alexander J. Norquist, Dermot O’Hare

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  21. The Actinides

    Elsevier eBooks · 2003-01-01

    Carol J. Burns, Mary P. Neu, Hakim Boukhalfa, Keith E. Gutowski, Nicholas J. Bridges, Robin Don Rogers

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  22. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

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    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  23. Variable Dimensionality in the UO2(CH3CO2)2·2H2O/HF/Isonicotinic Acid System: Synthesis and Structures of Zero-, One-, and Two-Dimensional Uranium Isonicotinates

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  24. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

    Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  25. [(Th2F5)(NC7H5O4)2(H2O)][NO3]: An Actinide−Organic Open Framework

    Journal of the American Chemical Society · 2003-09-26

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  26. 2D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties

    European Journal of Inorganic Chemistry · 2003-10-01

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  27. A novel scandium fluoride, [C2N2H10]0.5[ScF4], with an unprecedented tungsten bronze-related layer structure.

    Chemical Communications · 2004-01-01

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  28. Crystal Chemistry of Some Organically Templated Metal Fluorides: The Crystal Structure of [C2N2H10]0.5[Y2F7]

    MRS Proceedings · 2004-01-01

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  29. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot O’Hare

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  30. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

    Inorganic Chemistry · 2004-11-23

    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  31. Hydrothermal Synthesis and Structure of Zero-dimensional Organic–inorganic Perovskites

    Chemistry Letters · 2005-03-19

    Yuko Takeoka, Keisuke Asai, Masahiro Rikukawa, Kohei Sanui

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  32. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

    Inorganic Chemistry · 2005-07-29

    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  33. Synthesis, Structure and Photoluminescent Studies of Two Novel Layered Uranium Coordination Polymers Constructed from UO(OH) Polyhedra and Pyridinedicarboxylates

    European Journal of Inorganic Chemistry · 2005-09-05

    Yan‐Zhen Zheng, Ming‐Liang Tong, Xiao‐Ming Chen

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  34. Hydrothermal scandium fluoride chemistry: syntheses and crystal structures of [C2N2H10][ScF5], [NH4]2[Sc3F11] and [H3O][C6N2H16][ScF6]⋅H2O

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    Nicholas F. Stephens, Philip Lightfoot

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  35. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

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  36. Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)

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  37. An organically templated yttrium fluoride with a ‘Super-Diamond’ structure

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  38. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  39. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

    Dalton Transactions · 2007-01-01

    Chih-Min Wang, Yi‐Ying Wu, Pei-Lin Chen, Kwang‐Hwa Lii

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  40. Bis[tris(2-ammonioethyl)amine] bis(pentafluoridooxidomolybdate) difluoride monohydrate

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  41. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

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  42. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

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  43. Synthetic Approaches for Noncentrosymmetric Molybdates

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    Desmond J. Hubbard, Alexander R. Johnston, Hernan Sanchez Casalongue, Amy Narducci Sarjeant, Alexander J. Norquist

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  44. Oxo ligand functionalization in the uranyl ion (UO22+)

    Coordination Chemistry Reviews · 2009-06-22

    Skye Fortier, Trevor W. Hayton

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  45. Time- and Temperature-Dependent Study in the Three-Component Zinc-Triazolate-Oxybis(benzoate) System: Stabilization of New Topologies

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    Partha Mahata, N. Manikanda Prabu, Srinivasan Natarajan

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  46. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  47. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

    Inorganic Chemistry · 2010-02-12

    Vandavasi Koteswara Rao, K. Bharathi, Ramanath Prabhu, Manabendra Chandra, Srinivasan Natarajan

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  48. Systematic Investigation of Zinc Aminoalkylphosphonates: Influence of the Alkyl Chain Lengths on the Structure Formation

    Inorganic Chemistry · 2012-02-10

    Corinna Schmidt, Norbert Stock

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  49. Polymorph (C2N2H10)0.5RE3F10·xH2O (RE = Ho-Lu, Y) and REF3 nanocrystals: Hydrothermal synthesis, characterization and luminescence

    Materials Research Bulletin · 2012-08-07

    Li-Ping Jia, Qiang Zhang, Bing Yan

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  50. Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis

    RSC Advances · 2012-11-14

    Qing‐Jiang Pan, Yongming Wang, Run-Xue Wang, Hongyue Wu, Weiting Yang, Zhong‐Ming Sun, Hong‐Xing Zhang

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