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RESEARCH PAPER · Chemistry of Materials · 2007

Two New Noncentrosymmetric Polar Oxides: Synthesis, Characterization, Second-Harmonic Generating, and Pyroelectric Measurements on TlSeVO5 and TlTeVO5

T. Sivakumar, Hong Chang, Jaewook Baek, P. Shiv Halasyamani

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Two New Noncentrosymmetric Polar Oxides: Synthesis, Characterization, Second-Harmonic Generating, and Pyroelectric Measurements on TlSeVO5 and TlTeVO5OriginalBiosynthesis and biological activity of enniatins49Two New Noncentrosymmetric Polar Oxides: Synthesis, Characterization, Second‐Harmonic Generating, and Pyroelectric Measurements on TlSeVO5 and TlTeVO5.1New compounds and structures in the solid state1Analytical methods for calculating Continuous Symmetry Measures and the Chirality Measure105Mg7V4O16(OH)2(H2O): A magnesium vanadate with a novel 3D magnesium oxide open framework12Strong Second Harmonic Generation from the Tantalum Thioarsenates A3Ta2AsS11 (A = K and Rb)265New Polar Oxides: Synthesis, Characterization, Calculations, and Structure−Property Relationships in RbSe2V3O12 and TlSe2V3O12125Twinned crystal structure and compressibility of TlTeVO59Polar or Nonpolar? A+ Cation Polarity Control in A2Ti(IO3)6(A = Li, Na, K, Rb, Cs, Tl)306Magnetodielectric coupling by exchange striction in Y2Cu2O522A Series of New Infrared NLO Semiconductors, ZnY6Si2S14, AlxDy3(SiyAl1−y)S7, and Al0.33Sm3SiS7134New Noncentrosymmetric Material - [N(CH3)4]ZnCl3: Polar Chains of Aligned ZnCl4 Tetrahedra63Three New Coordination Compounds with Push‐Pull Ligand p‐Aminobenzonitrile (4ABN)11Growth and Properties of Single Crystals of Noncentrosymmetric Na3VO2B6O1187New compounds and structures in the solid state1Syntheses, crystal structures, and properties of three new lanthanum( iii ) vanadium iodates56Flux growth and morphology analysis of Na3VO2B6O11 crystals9Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques8Top-Seeded Solution Crystal Growth and Functional Properties of a Polar Material—Na2TeW2O956Polar or Non-Polar? Syntheses, Crystal Structures, and Optical Properties of Three New Palladium(II) Iodates45Explorations of New Second-Order Nonlinear Optical Materials in the Potassium Vanadyl Iodate System268New Quaternary Tellurite and Selenite: Synthesis, Structure, and Characterization of Centrosymmetric InVTe2O8 and Noncentrosymmetric InVSe2O887[R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers34New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)50New mixed metal selenites and tellurites containing Pd 2+ ions in a square planar geometry14Structural and vibrational properties of microcrystalline TlM(MoO4)2 (M=Nd, Pr) molybdates69A new noncentrosymmetric vanadoborate: synthesis, crystal structure and characterization of K2SrVB5O1222Exploration of New Second-Order Nonlinear Optical Compounds Containing Main Group Elements4PbPt(IO3)6(H2O): a new polar material with two types of stereoactive lone-pairs and a very large SHG response80Second-Order Nonlinear Optical Materials Based on Metal Iodates, Selenites, and Tellurites60Syntheses, crystal structures and SHG properties of a series of polar alkali-metal molybdenum(vi) selenites based on strandberg-type [Mo5O15(SeO3)2]4− polyanion28Temperature-induced assembly of MOF polymorphs: Syntheses, structures and physical properties68Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)50Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks17Syntheses, crystal structures and characterizations of new vanadium arsenites and arsenates4Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)47Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Supramolecular Polymers with [Co(en)3]3+Cores (en = ethylenediamine)5Three cobalt(ii) coordination polymers based on V-shaped aromatic polycarboxylates and rigid bis(imidazole) ligand: syntheses, crystal structures, physical properties and theoretical studies46Chemistry of Polar Transition-Metal Oxides1ZnTeMoO6: a strong second-harmonic generation material originating from three types of asymmetric building units53Versatile frameworks constructed from divalent metals with 4,4′-methylenedibenzoic acid and imidazole derivative ligands: Syntheses, crystal structures and physical properties10Synthesis, Structure, and Characterization of Two New Polar Sodium Tungsten Selenites: Na2(WO3)3(SeO3)·2H2O and Na6(W6O19)(SeO3)247Large scale synthesis, second-harmonic generation, and piezoelectric properties of a noncentrosymmetric vanadium phosphate, Li2VPO69Zn2(VO4)(IO3): A Novel Polar Zinc(II) Vanadium(V) Iodate with a Large SHG Response94Syntheses, structures and physical properties of two zinc(II) coordination polymers with 1,3,5-tris(imidazol-1-ylmethyl)-2,4,6-trimethylbenzene and 1,3,5-benzenetricarboxylate11Pb2B3O5.5(OH)2 and [Pb3(B3O7)](NO3): Facile Syntheses of New Lead(II) Borates by Simply Changing the pH Values of the Reaction Systems55Synthesis, crystal structure and optical properties of Ba5V3O12F18VSb(SeO3)4, First Selenite Containing V3+ Cation: Synthesis, Structure, Characterization, Magnetic Properties, and Calculations15Synthesis, Structure and Characterisation of One Two-Dimensional Layered Vanadium Tellurite [H2en] n [V2Te2O10] n2Variable Framework Structures and Centricities in Alkali Metal Yttrium Selenites, AY(SeO3)2 (A = Na, K, Rb, and Cs)51Effect of polarizable lone pair cations on the second-harmonic generation (SHG) properties of noncentrosymmetric (NCS) Bi 2−x Y x TeO 5 (x = 0–0.2)24A series of novel mercury( i ) selenites and tellurites containing SOJT Mo 6+ cations18A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties2Enhanced Photocatalytic Activity of N-doped Li2VPO6 Under Visible Light Irradiation5A series of coordination polymers based on varied polycarboxylates and different imidazole-containing ligands: syntheses, crystal structures and physical properties11A Series of Noncentrosymmetric Antimony Sulfides Ln8Sb2S15 (Ln = La, Pr, Nd) – Syntheses, Crystal and Electronic Structures, and NLO Properties26Syntheses, crystal structures, and NLO properties of the quaternary sulfides RE3Sb0.33SiS7 (RE=La, Pr)24Modulation of Framework and Centricity: Cation Size Effect in New Quaternary Selenites, ASc(SeO3)2 (A = Na, K, Rb, and Cs)41Explorations of New SHG Materials in the Alkali-Metal–Nb5+–Selenite System33IR Spectra of Minerals and Related Compounds, and Reference Samples’ Data21Density functional theory calculations, growth, structure, and optical properties of birefringent LiNaV2O69Alkali earth MO x ( x = 6, 7, 9, 12) polyhedra tuned cadmium selenites with different dimensions and diverse SeO 3 2− coordinations1Bi(IO3)F2: The First Metal Iodate Fluoride with a Very Strong Second Harmonic Generation Effect238Bi(IO3)F2: The First Metal Iodate Fluoride with a Very Strong Second Harmonic Generation Effect71Syntheses, Crystal Structures, and Properties of Two Quaternary Selenite/Tellurite‐Nitrates with Formula of Bi(SeO 3 )(NO 3 ) and Bi 3 (μ 3 ‐OH)(TeO 3 ) 3 (NO 3 ) 216New vanadium tellurites: Syntheses, structures, optical properties of noncentrosymmetric VTeO 4 (OH), centrosymmetric Ba 2 V 4 O 8 (Te 3 O 10 )12Theoretical study on Pb2VO2F5: large birefringence derived from optical anisotropies of VO2F4 groups15A Series of Mixed-Metal Germanium Iodates as Second-Order Nonlinear Optical Materials71Candle Soot-Driven Performance Enhancement in Pyroelectric Energy Conversion19Pb 2 GaF 2 (SeO 3 ) 2 Cl: Band Engineering Strategy by Aliovalent Substitution for Enlarging Bandgap while Keeping Strong Second Harmonic Generation Response178A Facile Route to Nonlinear Optical Materials: Three‐Site Aliovalent Substitution Involving One Cation and Two Anions137A Facile Route to Nonlinear Optical Materials: Three‐Site Aliovalent Substitution Involving One Cation and Two Anions23(H 3 O)HCs 2 Nb(IO 3 ) 9 and SrNbO(IO 3 ) 5 : a facile synthetic method using hydrofluoric acid as a solubilizer19Synthesis, crystal structures, second harmonic generation response and temperature phase transitions of two noncentrosymmetric Cu(II)-hybrid halides compounds: [(R)-C7H16N2][CuX4] (X = Cl or Br)25A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design114A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design25HBa2.5(IO3)6(I2O5) and HBa(IO3)(I4O11): Explorations of Second-Order Nonlinear Optical Materials in the Alkali-Earth Polyiodate System49REI5O14 (RE=Y and Gd): Promising SHG Materials Featuring the Semicircle‐Shaped I5O143− Polyiodate Anion125REI5O14 (RE=Y and Gd): Promising SHG Materials Featuring the Semicircle‐Shaped I5O143− Polyiodate Anion62Four Zinc(II) coordination polymers with dicarboxylate and Tri(4-pyridylphenyl)amine ligand: Syntheses, crystal structures and physical properties6A x Ce 9 (IO 3 ) 36 (A = K, La): the effects of a change in the intermediate valence on the second-harmonic generation response7IR Spectra of Minerals and Related Compounds, and Reference Samples Data3Alignment of Polar Moieties Leading to Strong Second Harmonic Response in KCsMoP2O951Enhancement of Second-Order Optical Nonlinearity in a Lutetium Selenite by Monodentate Anion Partial Substitution58AGa 3 F 6 (SeO 3 ) 2 (A = Rb, Cs): A New Type of Phase-Matchable Hexagonal Tungsten Oxide Material with Strong Second-Harmonic Generation Responses63K 2 Sb(P 2 O 7 )F: Cairo Pentagonal Layer with Bifunctional Genes Reveal Optical Performance297K2Sb(P2O7)F: Cairo Pentagonal Layer with Bifunctional Genes Reveal Optical Performance38Octahedral Lattice Distortion-Driven Ferroelectricity and Canted Antiferromagnetism in Oxalate and Phenanthrolin Ligand-Based Chain Molecular Magnets [{Fe(Δ)Fe(Λ)}1–x{Cr(Δ)Cr(Λ)}x(ox)2(phen)2]n (x = 0, 0.1, and 0.5)3A 2 Bi 2 (SeO 3 ) 3 F 2 (A = K and Rb): Excellent Mid-Infrared Nonlinear Optical Materials with Both Strong SHG Responses and Large Band Gaps64Ba(MoO2F)2(XO3)2 (X = Se and Te): First Cases of Noncentrosymmetric Fluorinated Molybdenum Oxide Selenite/Tellurite Through Unary Substitution for Enlarging Band Gaps and Second Harmonic Generation34Ba(MoO 2 F) 2 (QO 3 ) 2 (Q = Se, Te): Partial Fluorination of MoO 6 Octahedra Enabling Two Polar Solids with Strong and Phase Matchable SHG Response69Vanadoborates: cluster-based architectures, preparation and properties36On the crystal chemistry of inorganic nitrides: crystal-chemical parameters, bonding behavior, and opportunities in the exploration of their compositional space17Structural diversities in centrosymmetric La 8 S 4 Cl 8 La 12 S 8 Cl 4 [SbS 3 ] 8 and non-centrosymmetric Ln 12 S 8 Cl 8 [SbS 3 ] 4 (Ln = La and Ce): syntheses, crystal and electronic structures, and optical properties10Titanium Iodates with a Second-Harmonic-Generation Response8Synthesis, Structure, Characterization, and Calculation of a Noncentrosymmetric Fluorine-Containing Indium Iodate, Ba[InF3(IO3)2]10Giant Second-Harmonic Generation Response and Large Band Gap in the Partially Fluorinated Mid-Infrared Oxide RbTeMo 2 O 8 F149Cd 2 (IO 3 )(PO 4 ) and Cd 1.62 Mg 0.38 (IO 3 )(PO 4 ): metal iodate-phosphates with large SHG responses and wide band gaps28Two Nonlinear Optical Thiophosphates Cu 5 Hg 0.5 P 2 S 8 and AgHg 3 PS 6 Activated by Their Tetrahedra-Stacking Architecture12Flux synthesis, crystal structure, and characterization of a gamma-vanadate selenite polymorph1Solvothermal and hydrothermal methods for preparative solid-state chemistry5Enhanced Second-Harmonic Generation of van der Waals CuInP 2 S 6 via Pressure-Regulated Cationic Displacement61[M(OH) 2 ] 3 (IO 3 )(SeO 4 )·H 2 O (M = Ga and In): metal iodate–selenate nonlinear optical materials with a hexagonal tungsten oxide-type topology20Synthesis and characterization of Cs 2 Zn 4 V 4 O 15 —a new vanadate in the Cs–Zn–V–O quaternary system5Synthesis, structures and properties of two new selenite optical materials: K 2 Zn 3 Se 4 O 12 and K 4 Zn 3 V 4 Se 2 O 192Cd2Nb2Te4O15: A Novel Pseudo‐Aurivillius‐Type Tellurite with Unprecedented Nonlinear Optical Properties and Excellent Stability40From Centrosymmetry to Noncentrosymmetry: Precise Structural Regulation and Characterization on ZnHPO3·2H2O Polymorphs13Rational Design of a Niobium Tellurite Crystal Nb2Te3O11 Exhibiting Good Overall Infrared NLO Performance by Structural Genetic Engineering17Noncentrosymmetric tellurite halides created by a depolymerization strategy: toward strong SHG intensity and wide bandgap16Giant Optical Anisotropy in a Covalent Molybdenum Tellurite via Oxyanion Polymerization43Infrared nonlinear optical materials with multiple strongly ionic cations5Research progress in the chemistry of novel vanadoborates with extended structures of heteropolyvanadates0Pb2TeV2O10: A Lead Vanadate Tellurate with Wide Mid-IR Transparency and Large Birefringence Induced by Multiple Birefringence-Active Groups11Exploring quaternary vanadates containing alkali metals, alkaline earth metals, and [VO 4 ] in the quest for nonlinear optical materials1

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  2. Two New Noncentrosymmetric Polar Oxides: Synthesis, Characterization, Second‐Harmonic Generating, and Pyroelectric Measurements on TlSeVO5 and TlTeVO5.

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  4. Analytical methods for calculating Continuous Symmetry Measures and the Chirality Measure

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  5. Mg7V4O16(OH)2(H2O): A magnesium vanadate with a novel 3D magnesium oxide open framework

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  6. Strong Second Harmonic Generation from the Tantalum Thioarsenates A3Ta2AsS11 (A = K and Rb)

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  7. New Polar Oxides: Synthesis, Characterization, Calculations, and Structure−Property Relationships in RbSe2V3O12 and TlSe2V3O12

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  8. Twinned crystal structure and compressibility of TlTeVO5

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  9. Polar or Nonpolar? A+ Cation Polarity Control in A2Ti(IO3)6(A = Li, Na, K, Rb, Cs, Tl)

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  10. Magnetodielectric coupling by exchange striction in Y2Cu2O5

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  11. A Series of New Infrared NLO Semiconductors, ZnY6Si2S14, AlxDy3(SiyAl1−y)S7, and Al0.33Sm3SiS7

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    Sheng‐Ping Guo, Guo‐Cong Guo, Ming‐Sheng Wang, Jian‐Ping Zou, Gang Xu, Guojian Wang, Xifa Long, Jin‐Shun Huang

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  12. New Noncentrosymmetric Material - [N(CH3)4]ZnCl3: Polar Chains of Aligned ZnCl4 Tetrahedra

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  13. Three New Coordination Compounds with Push‐Pull Ligand p‐Aminobenzonitrile (4ABN)

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  14. Growth and Properties of Single Crystals of Noncentrosymmetric Na3VO2B6O11

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  17. Flux growth and morphology analysis of Na3VO2B6O11 crystals

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  18. Noncentrosymmetric Inorganic Oxide Materials: Synthetic Strategies and Characterisation Techniques

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  19. Top-Seeded Solution Crystal Growth and Functional Properties of a Polar Material—Na2TeW2O9

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  20. Polar or Non-Polar? Syntheses, Crystal Structures, and Optical Properties of Three New Palladium(II) Iodates

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  21. Explorations of New Second-Order Nonlinear Optical Materials in the Potassium Vanadyl Iodate System

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  23. [R-C7H16N2][V2Te2O10] and [S-C7H16N2][V2Te2O10]; new polar templated vanadium tellurite enantiomers

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  24. New Vanadium Selenites: Centrosymmetric Ca2(VO2)2(SeO3)3(H2O)2, Sr2(VO2)2(SeO3)3, and Ba(V2O5)(SeO3), and Noncentrosymmetric and Polar A4(VO2)2(SeO3)4(Se2O5) (A = Sr2+ or Pb2+)

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  26. Structural and vibrational properties of microcrystalline TlM(MoO4)2 (M=Nd, Pr) molybdates

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  29. PbPt(IO3)6(H2O): a new polar material with two types of stereoactive lone-pairs and a very large SHG response

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  31. Syntheses, crystal structures and SHG properties of a series of polar alkali-metal molybdenum(vi) selenites based on strandberg-type [Mo5O15(SeO3)2]4− polyanion

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  33. Two New Noncentrosymmetric (NCS) Polar Oxides: Syntheses, Characterization, and Structure–Property Relationships in BaMTe2O7 (M = Mg2+ or Zn2+)

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  34. Inducing polarity in [VO3]nn− chain compounds using asymmetric hydrogen-bonding networks

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  35. Syntheses, crystal structures and characterizations of new vanadium arsenites and arsenates

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  36. Synthesis, Structure, and Characterization of New Li+ – d0 –Lone-Pair – Oxides: Noncentrosymmetric Polar Li6(Mo2O5)3(SeO3)6 and Centrosymmetric Li2(MO3)(TeO3) (M = Mo6+ or W6+)

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  37. Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks

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  38. Supramolecular Polymers with [Co(en)3]3+Cores (en = ethylenediamine)

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  39. Three cobalt(ii) coordination polymers based on V-shaped aromatic polycarboxylates and rigid bis(imidazole) ligand: syntheses, crystal structures, physical properties and theoretical studies

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  40. Chemistry of Polar Transition-Metal Oxides

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  41. ZnTeMoO6: a strong second-harmonic generation material originating from three types of asymmetric building units

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  42. Versatile frameworks constructed from divalent metals with 4,4′-methylenedibenzoic acid and imidazole derivative ligands: Syntheses, crystal structures and physical properties

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  43. Synthesis, Structure, and Characterization of Two New Polar Sodium Tungsten Selenites: Na2(WO3)3(SeO3)·2H2O and Na6(W6O19)(SeO3)2

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    Sau Doan Nguyen, P. Shiv Halasyamani

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  44. Large scale synthesis, second-harmonic generation, and piezoelectric properties of a noncentrosymmetric vanadium phosphate, Li2VPO6

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  45. Zn2(VO4)(IO3): A Novel Polar Zinc(II) Vanadium(V) Iodate with a Large SHG Response

    Inorganic Chemistry · 2013-04-05

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  46. Syntheses, structures and physical properties of two zinc(II) coordination polymers with 1,3,5-tris(imidazol-1-ylmethyl)-2,4,6-trimethylbenzene and 1,3,5-benzenetricarboxylate

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