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RESEARCH PAPER · Inorganic Chemistry · 2011

Hydrothermal Synthesis and Crystal Structures of Two Novel Acentric Mixed Alkaline Earth Metal Berylloborates Sr3Be2B5O12(OH) and Ba3Be2B5O12(OH)

Colin D. McMillen, Joseph W. Kolis

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Hydrothermal Synthesis and Crystal Structures of Two Novel Acentric Mixed Alkaline Earth Metal Berylloborates Sr3Be2B5O12(OH) and Ba3Be2B5O12(OH)OriginalChemInform Abstract: Hydrothermal Synthesis and Crystal Structures of Two Novel Acentric Mixed Alkaline Earth Metal Berylloborates Sr3Be2B5O12(OH) and Ba3Be2B5O12(OH).0Crystal structures of the novel hydrated borates Ba2B5O9(OH), Sr2B5O9(OH) and Li2Sr8B22O41(OH)227Li5Rb2B7O14: a new congruently melting compound with two kinds of B–O one-dimensional chains and short UV absorption edge25Hydrothermal Synthesis and Crystal Structure of Two New Hydrated Alkaline Earth Metal Borates Sr3B6O11(OH)2 and Ba3B6O11(OH)239Two Novel Acentric Borate Fluorides: M 3 B 6 O 11 F 2 (M = Sr, Ba)97Ba2(BO3)1–x(CO3)xCl1+x: A Mixed Borate and Carbonate Chloride Crystallized from High-Temperature Solution37A combination of multiple chromophores enhances second-harmonic generation in a nonpolar noncentrosymmetric oxide: CdTeMoO681LaBeB3O7: a new phase-matchable nonlinear optical crystal exclusively containing the tetrahedral XO4 (X = B and Be) anionic groups30Synthesis and Characterization of Three New Hexaborates (Li5.5Fe0.5)FeCaB12O24, (Li5.5Fe0.5)FeSrB12O24 and (Li5.5Fe0.5)FeBaB12O241Growth, crystal structure and optical properties of a new layered fluorine beryllium borate, Sr0.23Ca0.77Na2Be2B2O6F25Synthesis, crystal structure and optical properties of a new beryllium borate, CsBe4(BO3)313Hydrothermal synthesis and structural analysis of new mixed oxyanion borates: Ba11B26O44(PO4)2(OH)6, Li9BaB15O27(CO3) and Ba3Si2B6O1625Ba2Cd(B3O6)2: A Congruent‐Melting Compound with Isolated B3O6 Units8Na 11 B 21 O 36 X 2 (X=Cl, Br): Halogen Sodium Borates with a New Graphene‐Like Borate Double Layer38Semiorganic nonlinear optical material: Crystal growth, structure and optical properties of NaB(L-C4H4O5)27Facile Assembly of an Unusual Lead Borate with Different Cluster Building Units via a Hydrothermal Process38Noncentrosymmetric mixed-cation borate: Crystal growth, structure and optical properties of Cs2Ca[B4O5(OH)4]2·8H2O14New alkali-metal bidentate borate–malate NaB(DL-C4H4O5)2 and CsB(DL-C4H4O5)2⋅H2O: Effect of cations on the framework structures and macroscopic centricities10Three New Mixed-Alkali- and Alkaline-Earth-Metal Borates: From 1D Chain to 2D Layer to 3D Framework57Two new organic borates with the large [B14O20(OH)6]4− oxoboron clusters8Deep-Ultraviolet Nonlinear Optical Materials: Na2Be4B4O11 and LiNa5Be12B12O33249ReBe2B5O11 (Re = Y, Gd): Rare-Earth Beryllium Borates as Deep-Ultraviolet Nonlinear-Optical Materials50Noncentrosymmetric versus Centrosymmetric: Influence of the Na+ Substitution on Structural Transition and Second-Harmonic Generation Property50An Acentric Calcium Borate Ca2[B5O9]·(OH)·H2O: Synthesis, Structure, and Nonliner Optical Property94Q 18 Mg 6 (B 5 O 10 ) 3 (B 7 O 14 ) 2 F (Q=Rb and Cs): New Borates Containing Two Large Isolated Polyborate Anions with Similar Topological Structures39A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π‐Conjugated Planar Triangular Units287A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π‐Conjugated Planar Triangular Units59Two New Mixed Metal Borates Made of Mg(B6O7(OH)6)2 and B8O14(OH)4 Cluster Units3A Deep-Ultraviolet Nonlinear Optical Crystal: Strontium Beryllium Borate Fluoride with Planar Be(O/F)3 Groups49Na7[Ga2B13O24(OH)4]: A Luminescent Sodium Gallium Borate Containing Two Different Types of Oxoboron Framework Building Blocks4Solvent-controlled syntheses of mixed-alkali-metal borates exhibiting UV nonlinear optical properties23Facile Syntheses of Ba2[B4O7(OH)2] and Na[B5O7(OH)2](H2O) Borate Salts Exhibiting Nonlinear Optical Activity in the Ultraviolet50An Ultraviolet Nonlinear Optic Borate with 13-Ring Channels Constructed from Different Building Units56NH 4 B 11 O 16 (OH) 2 : a new ammonium borate with wavy-shaped polycyclic 2∞[B 11 O 16 (OH) 2 ] layers27A Member of Fluorooxoborates: Li2Na0.9K0.1B5O8F2 with the Fundamental Building Block B5O10F2 and a Short Cutoff Edge27High-Temperature, High-Pressure Hydrothermal Synthesis, Crystal Structure, Thermal Stability, and Solid State NMR Spectroscopy of an Aluminum Borate, Ba[AlB4O8(OH)]10Two Lanthanide Borate Chlorides LnB4O6(OH)2Cl (Ln = La, Ce) with Wide Ultraviolet Transmission Windows and Large Second-Harmonic Generation Responses25Li 4 Na 2 CsB 7 O 14 : a new edge-sharing [BO 4 ] 5− tetrahedra containing borate with high anisotropic thermal expansion52K 2 [B 4 O 5 (OH) 4 ]·H 2 O and K 2 [B 4 O 5 (OH) 4 ]: two new hydrated potassium borates with isolated [B 4 O 5 (OH) 4 ] 2− units and different structural frameworks8Mg(H 2 O) 6 B 4 O 5 (OH) 4 (H 2 O) 3 : a new hydrated borate with a short DUV cutoff edge9Sr2Pb(BeB5O10)(BO3): An Excellent Ultraviolet Nonlinear-Optical Beryllium Borate by the Pb-Modified Construction of a Conjugated System and Lone-Pair Effect14PbBe 2 B 2 O 6 : an ultraviolet nonlinear-optical crystal with unprecedented π–π interacting BeBO 5 group14High temperature hydrothermal synthesis of inorganic compounds5Review of KBe2BO3F2-like second-order nonlinear optical materials and their structure-performance relationships14NH4B5O7(OH)2 and CsRbB10O14(OH)4·H2O: Two Hydroxyborates Feature Significant Optical Anisotropy and Contain 1∞[B5O7(OH)2] Chains1

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  1. ChemInform Abstract: Hydrothermal Synthesis and Crystal Structures of Two Novel Acentric Mixed Alkaline Earth Metal Berylloborates Sr3Be2B5O12(OH) and Ba3Be2B5O12(OH).

    ChemInform · 2011-08-18

    Colin D. McMillen, Joseph W. Kolis

    Read original paper ↗ ·

  2. Crystal structures of the novel hydrated borates Ba2B5O9(OH), Sr2B5O9(OH) and Li2Sr8B22O41(OH)2

    Journal of Solid State Chemistry · 2011-09-13

    Colin D. McMillen, Carla C. Heyward, Henry G. Giesber, Joseph W. Kolis

    Read original paper ↗ ·

  3. Li5Rb2B7O14: a new congruently melting compound with two kinds of B–O one-dimensional chains and short UV absorption edge

    CrystEngComm · 2012-01-01

    Yun Mo Yang, Shilie Pan, Xueling Hou, Xiaoyu Dong, Xin Su, Zhihua Yang, Min Zhang, Wenwu Zhao, Zhaohui Chen

    Read original paper ↗ ·

  4. Hydrothermal Synthesis and Crystal Structure of Two New Hydrated Alkaline Earth Metal Borates Sr3B6O11(OH)2 and Ba3B6O11(OH)2

    Inorganic Chemistry · 2012-03-12

    Carla C. Heyward, Colin D. McMillen, Joseph W. Kolis

    Read original paper ↗ ·

  5. Two Novel Acentric Borate Fluorides: M 3 B 6 O 11 F 2 (M = Sr, Ba)

    Inorganic Chemistry · 2012-03-12

    Colin D. McMillen, Jared T. Stritzinger, Joseph W. Kolis

    Read original paper ↗ ·

  6. Ba2(BO3)1–x(CO3)xCl1+x: A Mixed Borate and Carbonate Chloride Crystallized from High-Temperature Solution

    Inorganic Chemistry · 2012-03-26

    Jing Zhao, Rukang K. Li

    Read original paper ↗ ·

  7. A combination of multiple chromophores enhances second-harmonic generation in a nonpolar noncentrosymmetric oxide: CdTeMoO6

    Journal of Materials Chemistry C · 2013-01-01

    Sangen Zhao, Xingxing Jiang, Ran He, Shuquan Zhang, Zhihua Sun, Junhua Luo, Zheshuai Lin, Maochun Hong

    Read original paper ↗ ·

  8. LaBeB3O7: a new phase-matchable nonlinear optical crystal exclusively containing the tetrahedral XO4 (X = B and Be) anionic groups

    Journal of Materials Chemistry C · 2013-01-01

    Xue Sheng Yan, Siyang Luo, Zheshuai Lin, Yinchao Yue, Xiaoyang Wang, Lijuan Liu, Chuangtian Chen

    Read original paper ↗ ·

  9. Synthesis and Characterization of Three New Hexaborates (Li5.5Fe0.5)FeCaB12O24, (Li5.5Fe0.5)FeSrB12O24 and (Li5.5Fe0.5)FeBaB12O24

    Journal of Chemical Crystallography · 2013-01-19

    Carla C. Heyward, Colin D. McMillen, Joseph W. Kolis

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  10. Growth, crystal structure and optical properties of a new layered fluorine beryllium borate, Sr0.23Ca0.77Na2Be2B2O6F2

    Journal of Alloys and Compounds · 2013-01-24

    Hongwei Huang, Wenjiao Yao, Xiaoyang Wang, Naixia Zhai, Chuangtian Chen

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  11. Synthesis, crystal structure and optical properties of a new beryllium borate, CsBe4(BO3)3

    Solid State Sciences · 2013-02-01

    Hongwei Huang, Wenjiao Yao, Ran He, Chuangtian Chen, Xiaoyang Wang, Yihe Zhang

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  12. Hydrothermal synthesis and structural analysis of new mixed oxyanion borates: Ba11B26O44(PO4)2(OH)6, Li9BaB15O27(CO3) and Ba3Si2B6O16

    Journal of Solid State Chemistry · 2013-04-25

    Carla C. Heyward, Colin D. McMillen, Joseph W. Kolis

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  13. Ba2Cd(B3O6)2: A Congruent‐Melting Compound with Isolated B3O6 Units

    Zeitschrift für anorganische und allgemeine Chemie · 2013-04-26

    Xiaoyu Dong, Liang Cui, Yunjing Shi, Shilie Pan, Zhongxiang Zhou, Zhihua Yang, Bingbing Zhang, Xiangzhan Jiang, Yun Mo Yang, Zhaohui Chen, Zhenjun Huang

    Read original paper ↗ ·

  14. Na 11 B 21 O 36 X 2 (X=Cl, Br): Halogen Sodium Borates with a New Graphene‐Like Borate Double Layer

    Chemistry - A European Journal · 2013-04-29

    Xiaoyu Dong, Hongping Wu, Yunjing Shi, Hongwei Yu, Zhihua Yang, Bingbing Zhang, Zhaohui Chen, Yun Mo Yang, Zhenjun Huang, Shilie Pan, Zhongxiang Zhou

    Read original paper ↗ ·

  15. Semiorganic nonlinear optical material: Crystal growth, structure and optical properties of NaB(L-C4H4O5)2

    Materials Research Bulletin · 2013-05-04

    Hongwei Huang, Wenjiao Yao, Ying He, Na Tian, Chuangtian Chen, Yihe Zhang

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  16. Facile Assembly of an Unusual Lead Borate with Different Cluster Building Units via a Hydrothermal Process

    Inorganic Chemistry · 2013-05-10

    Han‐Rui Tian, Wenhua Wang, Yan‐E Gao, Tingting Deng, Jiaying Wang, Yun‐Long Feng, Jian‐Wen Cheng

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  17. Noncentrosymmetric mixed-cation borate: Crystal growth, structure and optical properties of Cs2Ca[B4O5(OH)4]2·8H2O

    Journal of Crystal Growth · 2013-06-21

    Hongwei Huang, Ran He, Wenjiao Yao, Zheshuai Lin, Chuangtian Chen, Yihe Zhang

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  18. New alkali-metal bidentate borate–malate NaB(DL-C4H4O5)2 and CsB(DL-C4H4O5)2⋅H2O: Effect of cations on the framework structures and macroscopic centricities

    Journal of Alloys and Compounds · 2013-08-21

    Hongwei Huang, Wenjiao Yao, Zheshuai Lin, Ying He, Na Tian, Chuangtian Chen, Yihe Zhang

    Read original paper ↗ ·

  19. Three New Mixed-Alkali- and Alkaline-Earth-Metal Borates: From 1D Chain to 2D Layer to 3D Framework

    Inorganic Chemistry · 2013-08-26

    Han‐Qing Wu, Ping Ju, Huan He, Bai‐Feng Yang, Guo‐Yu Yang

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  20. Two new organic borates with the large [B14O20(OH)6]4− oxoboron clusters

    Journal of Cluster Science · 2013-11-06

    Li Wei, Bai‐Feng Yang, Huan He, Guo‐Yu Yang

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  21. Deep-Ultraviolet Nonlinear Optical Materials: Na2Be4B4O11 and LiNa5Be12B12O33

    Journal of the American Chemical Society · 2013-11-19

    Hongwei Huang, Lijuan Liu, Shifeng Jin, Wenjiao Yao, Yihe Zhang, Chuangtian Chen

    Read original paper ↗ ·

  22. ReBe2B5O11 (Re = Y, Gd): Rare-Earth Beryllium Borates as Deep-Ultraviolet Nonlinear-Optical Materials

    Inorganic Chemistry · 2014-01-28

    Xue Sheng Yan, Siyang Luo, Zheshuai Lin, Jiyong Yao, Ran He, Yinchao Yue, Chuangtian Chen

    Read original paper ↗ ·

  23. Noncentrosymmetric versus Centrosymmetric: Influence of the Na+ Substitution on Structural Transition and Second-Harmonic Generation Property

    Crystal Growth & Design · 2014-03-13

    Shujuan Han, Ying Wang, Shilie Pan, Xiaoyu Dong, Hongping Wu, Jian Wei Han, Yun Mo Yang, Hongwei Yu, Chunyan Bai

    Read original paper ↗ ·

  24. An Acentric Calcium Borate Ca2[B5O9]·(OH)·H2O: Synthesis, Structure, and Nonliner Optical Property

    Inorganic Chemistry · 2014-10-15

    Qi Wei, Jian‐Wen Cheng, Chao He, Guo‐Yu Yang

    Read original paper ↗ ·

  25. Q 18 Mg 6 (B 5 O 10 ) 3 (B 7 O 14 ) 2 F (Q=Rb and Cs): New Borates Containing Two Large Isolated Polyborate Anions with Similar Topological Structures

    Chemistry - A European Journal · 2014-11-20

    Zheng Wang, Min Zhang, Xin Su, Shilie Pan, Zhihua Yang, Hui Zhang, Lu Liu

    Read original paper ↗ ·

  26. A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π‐Conjugated Planar Triangular Units

    Angewandte Chemie International Edition · 2015-01-28

    Jun‐Ling Song, Chun‐Li Hu, Xiang Xu, Fang Kong, Jiang‐Gao Mao

    Read original paper ↗ ·

  27. A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π‐Conjugated Planar Triangular Units

    Angewandte Chemie · 2015-02-04

    Jun‐Ling Song, Chun‐Li Hu, Xiang Xu, Fang Kong, Jiang‐Gao Mao

    Read original paper ↗ ·

  28. Two New Mixed Metal Borates Made of Mg(B6O7(OH)6)2 and B8O14(OH)4 Cluster Units

    Journal of Cluster Science · 2015-05-15

    Guang Yan Huang, Rui Pan, Huan He, Bai‐Feng Yang, Guo‐Yu Yang

    Read original paper ↗ ·

  29. A Deep-Ultraviolet Nonlinear Optical Crystal: Strontium Beryllium Borate Fluoride with Planar Be(O/F)3 Groups

    Chemistry of Materials · 2016-06-02

    Na Yu, Shichao Wang, Ning Ye, Fei Liang, Zheshuai Lin, Min Luo, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  30. Na7[Ga2B13O24(OH)4]: A Luminescent Sodium Gallium Borate Containing Two Different Types of Oxoboron Framework Building Blocks

    Journal of Cluster Science · 2016-12-29

    Pei-Li Xu, Congcong Jin, Tingting Deng, Er-Rong Wang, Jian‐Wen Cheng

    Read original paper ↗ ·

  31. Solvent-controlled syntheses of mixed-alkali-metal borates exhibiting UV nonlinear optical properties

    Inorganic Chemistry Frontiers · 2017-01-01

    Chao Wu, Longhua Li, Jun‐Ling Song, Gang Yang, Mark Graeme Humphrey, Chi Zhang

    Read original paper ↗ ·

  32. Facile Syntheses of Ba2[B4O7(OH)2] and Na[B5O7(OH)2](H2O) Borate Salts Exhibiting Nonlinear Optical Activity in the Ultraviolet

    Inorganic Chemistry · 2017-01-11

    Chao Wu, Longhua Li, Jun‐Ling Song, Gang Yang, Mark Graeme Humphrey, Chi Zhang

    Read original paper ↗ ·

  33. An Ultraviolet Nonlinear Optic Borate with 13-Ring Channels Constructed from Different Building Units

    Inorganic Chemistry · 2017-06-07

    Er-Rong Wang, Jianhao Huang, Sujuan Yu, You‐Zhao Lan, Jian‐Wen Cheng, Guo‐Yu Yang

    Read original paper ↗ ·

  34. NH 4 B 11 O 16 (OH) 2 : a new ammonium borate with wavy-shaped polycyclic 2∞[B 11 O 16 (OH) 2 ] layers

    New Journal of Chemistry · 2018-01-01

    Chunmei Huang, Fangfang Zhang, Bingbing Zhang, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  35. A Member of Fluorooxoborates: Li2Na0.9K0.1B5O8F2 with the Fundamental Building Block B5O10F2 and a Short Cutoff Edge

    Inorganic Chemistry · 2018-01-02

    Shujuan Han, Ying Wang, Bingbing Zhang, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  36. High-Temperature, High-Pressure Hydrothermal Synthesis, Crystal Structure, Thermal Stability, and Solid State NMR Spectroscopy of an Aluminum Borate, Ba[AlB4O8(OH)]

    Inorganic Chemistry · 2018-01-22

    Chun-Chi Peng, Hsin‐Kuan Liu, Kwang‐Hwa Lii

    Read original paper ↗ ·

  37. Two Lanthanide Borate Chlorides LnB4O6(OH)2Cl (Ln = La, Ce) with Wide Ultraviolet Transmission Windows and Large Second-Harmonic Generation Responses

    Inorganic Chemistry · 2018-11-14

    Fengjiao Guo, Jian Wei Han, Jianian Cheng, Zhihua Yang, Miriding Mutailipu, Shilie Pan

    Read original paper ↗ ·

  38. Li 4 Na 2 CsB 7 O 14 : a new edge-sharing [BO 4 ] 5− tetrahedra containing borate with high anisotropic thermal expansion

    Chemical Communications · 2018-12-26

    Miriding Mutailipu, Min Zhang, Hao Li, Xiao Fan, Zhihua Yang, Shifeng Jin, Gang Wang, Shilie Pan

    Read original paper ↗ ·

  39. K 2 [B 4 O 5 (OH) 4 ]·H 2 O and K 2 [B 4 O 5 (OH) 4 ]: two new hydrated potassium borates with isolated [B 4 O 5 (OH) 4 ] 2− units and different structural frameworks

    New Journal of Chemistry · 2019-01-01

    Tingting Shi, Fangfang Zhang, Abudukadi Tudi, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  40. Mg(H 2 O) 6 B 4 O 5 (OH) 4 (H 2 O) 3 : a new hydrated borate with a short DUV cutoff edge

    Dalton Transactions · 2019-01-01

    Ya Wang, Jian Wei Han, Fengjiao Guo, Shichao Cheng, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  41. Sr2Pb(BeB5O10)(BO3): An Excellent Ultraviolet Nonlinear-Optical Beryllium Borate by the Pb-Modified Construction of a Conjugated System and Lone-Pair Effect

    Inorganic Chemistry · 2021-06-18

    Zhe Dai, Yi-Gang Chen, Yao Guo, Fang Wang, Yuanyu Yang, Xian‐Ming Zhang

    Read original paper ↗ ·

  42. PbBe 2 B 2 O 6 : an ultraviolet nonlinear-optical crystal with unprecedented π–π interacting BeBO 5 group

    Chemical Communications · 2022-01-01

    Yi-Gang Chen, Xingxing Jiang, Yuanyu Yang, Zhe Dai, Zheshuai Lin, Xian‐Ming Zhang

    Read original paper ↗ ·

  43. High temperature hydrothermal synthesis of inorganic compounds

    Elsevier eBooks · 2022-03-29

    Joseph W. Kolis, Colin D. McMillen

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  44. Review of KBe2BO3F2-like second-order nonlinear optical materials and their structure-performance relationships

    Coordination Chemistry Reviews · 2025-04-06

    Junben Huang, Chenglong Zhang, Siying Chen, Ailijiang Abudurusuli

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  45. NH4B5O7(OH)2 and CsRbB10O14(OH)4·H2O: Two Hydroxyborates Feature Significant Optical Anisotropy and Contain 1∞[B5O7(OH)2] Chains

    Inorganic Chemistry · 2025-07-17

    Xueli Du, Haoran Wang, Haoran Liu, Qingyu Liu, Wenhu Wang, Jiahao Jiao, Yuchen Yan, Xueyan Wu, Min Zhang

    Read original paper ↗ ·
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