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RESEARCH PAPER · Inorganic Chemistry · 2013

U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient In Situ Route That Creates U4+ under Mild Hydrothermal Conditions

Jeongho Yeon, Mark D. Smith, Athena S. Sefat, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient In Situ Route That Creates U4+ under Mild Hydrothermal ConditionsOriginalChemInform Abstract: U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient in situ Route That Creates U4+ under Mild Hydrothermal Conditions.0Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Application of a Mild Hydrothermal Approach Containing an in Situ Reduction Step to the Growth of Single Crystals of the Quaternary U(IV)-Containing Fluorides Na4MU6F30 (M = Mn2+, Co2+, Ni2+, Cu2+, and Zn2+) Crystal Growth, Structures, and Magnetic Properties60Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F1341Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Observation of Multiple Crystal-to-Crystal Transitions in a New Reduced Vanadium Oxalate Hybrid Material, Ba3[(VO)2(C2O4)5(H2O)6]·(H2O)3, Prepared via a Mild, Two-Step Hydrothermal Method27Design and synthesis of a chiral uranium-based microporous metal organic framework with high SHG efficiency and sequestration potential for low-valent actinides58Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties28Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties12Synthesis, characterization, and properties of reduced europium molybdates and tungstates21Single crystal growth and characterization of the first reduced lanthanum molybdenum oxychloride, La20Mo12O63Cl4, with an unusual trigonal prismatic MoO6 unit14Structural study of the ammonium octafluoroneptunate, [NH4]4NpF87Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)9Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]13Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route4Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides18One-step mild hydrothermal method to prepare low valent sodium vanadium(III) monohydrogenphosphate: NaV(HPO4)24Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12[Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials11Complex Inorganic Actinide Materials1Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides24Magnetic and thermal behavior of a family of compositionally related zero-dimensional fluorides4In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates7Complex Topologies from Simple Building Blocks: Uranium(IV) Thiophosphates21Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability3Compréhension des phénomènes d’hydratation et de déshydratation de composés d’actinides0From BiF 3 to BiF 3 ·H 2 O: diverse Bi( iii ) coordination for structural transformation and birefringence regulation14Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis12Characterizing the solid hydrolysis product, UF 4 (H 2 O) 2.5 , generated from neat water reactions with UF 4 at room temperature16Vibrational spectroscopy of uranium tetrafluoride hydrates6Inelastic Neutron Spectra of Uranium Tetrafluoride Hydrate, UF4(H2O)2.54Uranium: The Nuclear Fuel Cycle and Beyond107Structural Characterization of Uranium Tetrafluoride Hydrate (UF4·2.5H2O)3Hydrothermal transformations of hydrated cerium(IV) fluoride in NaOH or HF media. The first crystal structure in the cerium tetrafluoride hydrate family2Water Molecule-Driven Structural Evolution from Na2ZnCl4 to Na2ZnCl4·3H2O: A Route to Promising Deep-UV Nonlinear Optical Crystals0Rare octahedral coordination of cerium(IV) in the trinuclear fluorine complex [F3Ce(µ-Ph2PO2)3Ce(µ-Ph2PO2)3CeF3].3Me2SO0

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  1. ChemInform Abstract: U3F12(H2O), a Noncentrosymmetric Uranium(IV) Fluoride Prepared via a Convenient in situ Route That Creates U4+ under Mild Hydrothermal Conditions.

    ChemInform · 2013-09-12

    Jeongho Yeon, Mark D. Smith, Athena S. Sefat, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source

    Journal of Fluorine Chemistry · 2014-01-03

    Jacob Olchowka, Christophe Volkringer, Natacha Henry, Thierry Loiseau

    Read original paper ↗ ·

  3. Application of a Mild Hydrothermal Approach Containing an in Situ Reduction Step to the Growth of Single Crystals of the Quaternary U(IV)-Containing Fluorides Na4MU6F30 (M = Mn2+, Co2+, Ni2+, Cu2+, and Zn2+) Crystal Growth, Structures, and Magnetic Properties

    Journal of the American Chemical Society · 2014-03-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13

    Inorganic Chemistry · 2014-05-27

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  5. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  6. Observation of Multiple Crystal-to-Crystal Transitions in a New Reduced Vanadium Oxalate Hybrid Material, Ba3[(VO)2(C2O4)5(H2O)6]·(H2O)3, Prepared via a Mild, Two-Step Hydrothermal Method

    Crystal Growth & Design · 2014-08-19

    Dileka Abeysinghe, Mark D. Smith, Jeongho Yeon, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. Design and synthesis of a chiral uranium-based microporous metal organic framework with high SHG efficiency and sequestration potential for low-valent actinides

    Dalton Transactions · 2015-01-01

    Yanlong Wang, Yuxiang Li, Zhuanling Bai, Chengliang Xiao, Zhiyong Liu, Wei Liu, Lanhua Chen, Weiwei He, Juan Diwu, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

    Read original paper ↗ ·

  8. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  9. Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties

    Inorganic Chemistry · 2015-02-05

    Jeongho Yeon, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  10. Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties

    Journal of Solid State Chemistry · 2015-05-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  11. Synthesis, characterization, and properties of reduced europium molybdates and tungstates

    Journal of Solid State Chemistry · 2015-05-18

    Dileka Abeysinghe, Birgit Gerke, Gregory W. Morrison, Chun H. Hsieh, Mark D. Smith, Rainer Pöttgen, Thomas M. Makris, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  12. Single crystal growth and characterization of the first reduced lanthanum molybdenum oxychloride, La20Mo12O63Cl4, with an unusual trigonal prismatic MoO6 unit

    Solid State Sciences · 2015-07-30

    Anthony J. Cortese, Branford O. Wilkins, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  13. Structural study of the ammonium octafluoroneptunate, [NH4]4NpF8

    Inorganica Chimica Acta · 2016-04-30

    Frédéric Poineau, Chinthaka M. Silva, C. B. Yeamans, Gary S. Cerefice, Alfred P. Sattelberger, Kenneth R. Czerwinski

    Read original paper ↗ ·

  14. Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)

    Journal of Solid State Chemistry · 2016-05-09

    Anthony J. Cortese, Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  15. Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]

    Inorganic Chemistry · 2016-07-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  16. Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route

    Solid State Sciences · 2016-08-07

    Anthony J. Cortese, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  17. Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides

    Inorganic Chemistry Frontiers · 2017-01-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  18. One-step mild hydrothermal method to prepare low valent sodium vanadium(III) monohydrogenphosphate: NaV(HPO4)2

    Solid State Sciences · 2017-05-04

    Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  19. Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O

    RSC Advances · 2018-01-01

    Alexander T. Chemey, Joseph M. Sperling, Thomas E. Albrecht‐Schmitt

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  20. [Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials

    Crystal Growth & Design · 2018-01-09

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  21. Complex Inorganic Actinide Materials

    Unknown journal · 2018-01-12

    Matthew L. Marsh, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  22. Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides

    Inorganic Chemistry · 2018-04-10

    Vladislav V. Klepov, Justin B. Felder, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  23. Magnetic and thermal behavior of a family of compositionally related zero-dimensional fluorides

    Solid State Sciences · 2018-04-27

    Justin B. Felder, Mark D. Smith, Athena S. Sefat, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  24. In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect

    Inorganic Chemistry · 2018-05-24

    Jian Hung Lin, Zenghui Yue, Mark A. Silver, Meiying Qie, Xiaomei Wang, Wei Liu, Xiao Lin, Hongliang Bao, Linjuan Zhang, Shuao Wang, Jian‐Qiang Wang

    Read original paper ↗ ·

  25. Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates

    Inorganic Chemistry · 2018-07-17

    Justin B. Felder, Stuart Calder, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  26. Complex Topologies from Simple Building Blocks: Uranium(IV) Thiophosphates

    Inorganic Chemistry · 2018-08-16

    Vladislav V. Klepov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  27. Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability

    Inorganica Chimica Acta · 2018-12-26

    Qi Liu, Huiqin Yin, Hongliang Bao, Zenghui Yue, Kariem Diefenbach, Zhongfeng Tang, Jian Hung Lin, Jian‐Qiang Wang

    Read original paper ↗ ·

  28. Compréhension des phénomènes d’hydratation et de déshydratation de composés d’actinides

    Unknown journal · 2019-12-09

    Artem Belonosov

    Read original paper ↗ ·

  29. From BiF 3 to BiF 3 ·H 2 O: diverse Bi( iii ) coordination for structural transformation and birefringence regulation

    CrystEngComm · 2020-01-01

    Xian Liu, Can Yang, Qi Wu, Juan Sun, Fei Liang

    Read original paper ↗ ·

  30. Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis

    Inorganic Chemistry · 2020-03-26

    Cory J. Windorff, Alexander T. Chemey, Joseph M. Sperling, Bonnie E. Klamm, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  31. Characterizing the solid hydrolysis product, UF 4 (H 2 O) 2.5 , generated from neat water reactions with UF 4 at room temperature

    Dalton Transactions · 2021-01-01

    Jonathan H. Christian, Christopher A. Klug, Michael A. DeVore, Eliel Villa‐Aleman, Bryan J. Foley, Nicholas Groden, Taylor Baldwin, Matthew S. Wellons

    Read original paper ↗ ·

  32. Vibrational spectroscopy of uranium tetrafluoride hydrates

    Vibrational Spectroscopy · 2021-06-24

    Michael A. DeVore, Eliel Villa‐Aleman, Justin B. Felder, Jeongho Yeon, Hans‐Conrad zur Loye, Matthew S. Wellons

    Read original paper ↗ ·

  33. Inelastic Neutron Spectra of Uranium Tetrafluoride Hydrate, UF4(H2O)2.5

    The Journal of Physical Chemistry C · 2021-11-09

    Andrew Miskowiec, Kevin J. Pastoor, Jonathan H. Christian, Jennifer L. Niedziela, Bryan J. Foley, Sara B. Isbill, Ashley E. Shields, Luke L. Daemen, Eric C. Novak, Erik C. Nykwest, Tyler L. Spano, Matthew S. Wellons, Mark P. Jensen, Jenifer C. Shafer

    Read original paper ↗ ·

  34. Uranium: The Nuclear Fuel Cycle and Beyond

    International Journal of Molecular Sciences · 2022-04-22

    Bárbara Maria Teixeira Costa Peluzo, Elfi Kraka

    Read original paper ↗ ·

  35. Structural Characterization of Uranium Tetrafluoride Hydrate (UF4·2.5H2O)

    The Journal of Physical Chemistry C · 2022-08-01

    Kevin J. Pastoor, Andrew Miskowiec, Jennifer L. Niedziela, Jonathan H. Christian, Bryan J. Foley, Sara B. Isbill, Ashley E. Shields, Alicia Maria Manjón-Sanz, Erik C. Nykwest, Tyler L. Spano, Matthew S. Wellons, Jenifer C. Shafer, Mark P. Jensen

    Read original paper ↗ ·

  36. Hydrothermal transformations of hydrated cerium(IV) fluoride in NaOH or HF media. The first crystal structure in the cerium tetrafluoride hydrate family

    Journal of Fluorine Chemistry · 2024-09-04

    Е. Г. Ильин, Artemy S. Parshakov, Andrei V. Churakov, Ludmila Iskhakova, Arina D. Filippova, Sergei Kottsov, Л. И. Демина, Lyudmila V. Goeva, Nikolay P. Simonenko, Victor I. Privalov, Alexander E. Baranchikov, Vladimir K. Ivanov

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  37. Water Molecule-Driven Structural Evolution from Na2ZnCl4 to Na2ZnCl4·3H2O: A Route to Promising Deep-UV Nonlinear Optical Crystals

    Crystal Growth & Design · 2025-07-08

    Mengmeng Chen, Wangfei Che, Cui Chen, Qixian Ren, Juanjuan Lu, Yabo Wu

    Read original paper ↗ ·

  38. Rare octahedral coordination of cerium(IV) in the trinuclear fluorine complex [F3Ce(µ-Ph2PO2)3Ce(µ-Ph2PO2)3CeF3].3Me2SO

    Journal of Fluorine Chemistry · 2026-02-19

    Е. Г. Ильин, Artemy S. Parshakov, V. G. Yarzhemsky, Victor I. Privalov, L. D. Iskhakova, Liudmila Demina, Lyudmila V. Goeva, Elena V. Fatiychina, Nikita A. Selivanov, I. I. Bannykh, Alexandr E. Baranchikov, Vladimir K. Ivanov

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