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RESEARCH PAPER · Inorganic Chemistry · 2014

Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13

Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

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Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13OriginalChemInform Abstract: Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13.0Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties28Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties12Flux Synthesis, Structure, Properties, and Theoretical Magnetic Study of Uranium(IV)-Containing A2USi6O15 (A = K, Rb) with an Intriguing Green-to-Purple, Crystal-to-Crystal Structural Transition in the K Analogue32Single crystal structures of thallium (I) thorium fluorides and crystal chemistry of monovalent tetravalent cation pentafluorides5Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates61Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]13Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route4Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides18Uranium(IV) Chloride Complexes: UCl62– and an Unprecedented U(H2O)4Cl4 Structural Unit26Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12[Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials11Na2(UO2)(BO3): An All-Uranium(V) Borate Synthesized under Mild Hydrothermal Conditions18Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides24In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates7Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)25Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride14Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability33d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials14UF4 and the High‐Pressure Polymorph HP‐UF45The low-temperature barium fluoridozirconate variety α-BaZr2F101Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF510Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis12Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]5Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)3A Molecular Octafluoridoneptunate(IV) Anion in (NH4)4[NpF8] and Theoretical Investigations of the [MF8]4– System (M = Th – Bk)3Preparation, thermal stability and crystal structure of Li3UF7: New insights into LiF-UF4 binary phase diagram3New insights and coupled modelling of the structural and thermodynamic properties of the LiF-UF4 system27Vibrational spectroscopy of uranium tetrafluoride hydrates6Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component22Using the Quasi-chemical formalism beyond the phase Diagram: Density and viscosity models for molten salt fuel systems24High temperature hydrothermal synthesis of inorganic compounds5A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate0Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Synthesis, Characterization, and Magnetic Properties of Uranium-Containing 2H-Perovskite-Related Sulfides: Ba3MUS6 (M = Mn, Fe, Co, Ni) and Ba3Co0.858(5)Mg0.142(5)US65Equivalent cation-tuning to realize a new Ce( iv ) fluoride with excellent comprehensive nonlinear optical performances12Insight into γ-Irradiation-Induced Structure Evolution of Uranium(IV) Germanates as Crystalline Nuclear Waste Forms2Thermodynamics of RbF-UF4: a potential fuel candidate for molten salt reactors1Rich Chemical Behavior and Topological Variation in Uranium Phosphates via Flux Growth under an Inert Atmosphere0

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  1. ChemInform Abstract: Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13.

    ChemInform · 2014-07-28

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Moeller, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties

    Inorganic Chemistry · 2015-02-05

    Jeongho Yeon, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties

    Journal of Solid State Chemistry · 2015-05-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

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  5. Flux Synthesis, Structure, Properties, and Theoretical Magnetic Study of Uranium(IV)-Containing A2USi6O15 (A = K, Rb) with an Intriguing Green-to-Purple, Crystal-to-Crystal Structural Transition in the K Analogue

    Inorganic Chemistry · 2015-05-15

    Gregory W. Morrison, Harry Ramanantoanina, Werner Urland, Mark D. Smith, Hans‐Conrad zur Loye

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  6. Single crystal structures of thallium (I) thorium fluorides and crystal chemistry of monovalent tetravalent cation pentafluorides

    Journal of Solid State Chemistry · 2015-09-08

    Abdelghani Oudahmane, Malika El‐Ghozzi, Laurent J. Jouffret, Daniel Avignant B

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  7. Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

    Journal of the American Chemical Society · 2016-05-24

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  8. Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]

    Inorganic Chemistry · 2016-07-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

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  9. Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route

    Solid State Sciences · 2016-08-07

    Anthony J. Cortese, Mark D. Smith, Hans‐Conrad zur Loye

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  10. Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides

    Inorganic Chemistry Frontiers · 2017-01-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

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  11. Uranium(IV) Chloride Complexes: UCl62– and an Unprecedented U(H2O)4Cl4 Structural Unit

    Inorganic Chemistry · 2017-07-31

    Jennifer N. Wacker, Monica Vasiliu, Kevin Huang, Ryan Baumbach, Jeffery A. Bertke, David A. Dixon, Karah E. Knope

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  12. Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O

    RSC Advances · 2018-01-01

    Alexander T. Chemey, Joseph M. Sperling, Thomas E. Albrecht‐Schmitt

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  13. [Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials

    Crystal Growth & Design · 2018-01-09

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

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  14. Na2(UO2)(BO3): An All-Uranium(V) Borate Synthesized under Mild Hydrothermal Conditions

    Inorganic Chemistry · 2018-04-02

    Kristen A. Pace, Vancho Kocevski, S. Karakalos, Gregory W. Morrison, Theodore M. Besmann, Hans‐Conrad zur Loye

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  15. Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides

    Inorganic Chemistry · 2018-04-10

    Vladislav V. Klepov, Justin B. Felder, Hans‐Conrad zur Loye

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  16. In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect

    Inorganic Chemistry · 2018-05-24

    Jian Hung Lin, Zenghui Yue, Mark A. Silver, Meiying Qie, Xiaomei Wang, Wei Liu, Xiao Lin, Hongliang Bao, Linjuan Zhang, Shuao Wang, Jian‐Qiang Wang

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  17. Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates

    Inorganic Chemistry · 2018-07-17

    Justin B. Felder, Stuart Calder, Hans‐Conrad zur Loye

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  18. Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)2

    Inorganic Chemistry · 2018-07-31

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

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  19. Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride

    Inorganic Chemistry · 2018-12-20

    Alexander T. Chemey, Cristian Celis‐Barros, Kevin Huang, Joseph M. Sperling, Cory J. Windorff, Ryan Baumbach, David E Graf, Dayán Páez‐Hernández, Michael Ruf, David E. Hobart, Thomas E. Albrecht‐Schmitt

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  20. Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability

    Inorganica Chimica Acta · 2018-12-26

    Qi Liu, Huiqin Yin, Hongliang Bao, Zenghui Yue, Kariem Diefenbach, Zhongfeng Tang, Jian Hung Lin, Jian‐Qiang Wang

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  21. 3d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials

    Journal of the American Chemical Society · 2019-02-13

    Vladislav V. Klepov, Kristen A. Pace, Stuart Calder, Justin B. Felder, Hans‐Conrad zur Loye

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  22. UF4 and the High‐Pressure Polymorph HP‐UF4

    Chemistry - A European Journal · 2019-03-26

    Benjamin Scheibe, Jörn Bruns, Günter Heymann, Malte Sachs, Antti J. Karttunen, Clemens Pietzonka, Sergei I. Ivlev, Hubert Huppertz, Florian Kraus

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  23. The low-temperature barium fluoridozirconate variety α-BaZr2F10

    Acta Crystallographica Section C Structural Chemistry · 2019-10-04

    Jean Paul Laval

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  24. Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF5

    Inorganic Chemistry · 2019-10-24

    Alexander T. Chemey, Cristian Celis‐Barros, Joseph M. Sperling, Dayán Páez‐Hernández, Thomas E. Albrecht‐Schmitt

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  25. Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis

    Inorganic Chemistry · 2020-03-26

    Cory J. Windorff, Alexander T. Chemey, Joseph M. Sperling, Bonnie E. Klamm, Thomas E. Albrecht‐Schmitt

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  26. Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]

    Crystal Growth & Design · 2020-04-07

    Alexander T. Chemey, Joseph M. Sperling, Cory J. Windorff, David E. Hobart, Thomas E. Albrecht‐Schmitt

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  27. Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)

    European Journal of Inorganic Chemistry · 2020-04-29

    Benjamin Scheibe, Juliane März, Moritz Schmidt, Thorsten Stumpf, Florian Kraus

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  28. A Molecular Octafluoridoneptunate(IV) Anion in (NH4)4[NpF8] and Theoretical Investigations of the [MF8]4– System (M = Th – Bk)

    European Journal of Inorganic Chemistry · 2020-09-24

    Benjamin Scheibe, Michael Patzschke, Juliane März, Matthias Conrad, Florian Kraus

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  29. Preparation, thermal stability and crystal structure of Li3UF7: New insights into LiF-UF4 binary phase diagram

    Journal of Alloys and Compounds · 2020-12-03

    Siddhartha Kolay, Srungarpu Nagabhusan Achary, Anil Bhimrao Shinde, P. Siva Ram Krishna, Manidipa Basu, Ratikant Mishra, A. K. Tyagi

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  30. New insights and coupled modelling of the structural and thermodynamic properties of the LiF-UF4 system

    Journal of Molecular Liquids · 2021-03-02

    Jaén A. Ocádiz Flores, Aïmen E. Gheribi, John Vlieland, Kathy Dardenne, Jörg Rothe, Rudy J. M. Konings, Anna L. Smith

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  31. Vibrational spectroscopy of uranium tetrafluoride hydrates

    Vibrational Spectroscopy · 2021-06-24

    Michael A. DeVore, Eliel Villa‐Aleman, Justin B. Felder, Jeongho Yeon, Hans‐Conrad zur Loye, Matthew S. Wellons

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  32. Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component

    Journal of the American Chemical Society · 2021-07-26

    Vladislav V. Klepov, Kristen A. Pace, Anna A. Berseneva, Justin B. Felder, Stuart Calder, Gregory W. Morrison, Qiang Zhang, Melanie Kirkham, David Parker, Hans‐Conrad zur Loye

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  33. Using the Quasi-chemical formalism beyond the phase Diagram: Density and viscosity models for molten salt fuel systems

    Journal of Nuclear Materials · 2022-01-15

    Jaén A. Ocádiz Flores, Rudy J. M. Konings, Anna L. Smith

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  34. High temperature hydrothermal synthesis of inorganic compounds

    Elsevier eBooks · 2022-03-29

    Joseph W. Kolis, Colin D. McMillen

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  35. A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate

    Ionics · 2023-05-15

    Li Wang, Jie Qin, Youyuan Ran, Lan Chen

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  36. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

    Inorganic Chemistry · 2023-07-18

    Navindra Keerthisinghe, Gyanendra B. Ayer, Mark D. Smith, Hans‐Conrad zur Loye

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  37. Synthesis, Characterization, and Magnetic Properties of Uranium-Containing 2H-Perovskite-Related Sulfides: Ba3MUS6 (M = Mn, Fe, Co, Ni) and Ba3Co0.858(5)Mg0.142(5)US6

    Inorganic Chemistry · 2023-10-09

    Logan S. Breton, Gregory W. Morrison, Hans‐Conrad zur Loye

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  38. Equivalent cation-tuning to realize a new Ce( iv ) fluoride with excellent comprehensive nonlinear optical performances

    Inorganic Chemistry Frontiers · 2024-01-01

    Beibei Zhang, Wen‐Ye Gao, Wei Lin Xu, L. Ma, Wenlong Liu, Ru‐Ling Tang, Sheng‐Ping Guo

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  39. Insight into γ-Irradiation-Induced Structure Evolution of Uranium(IV) Germanates as Crystalline Nuclear Waste Forms

    Inorganic Chemistry · 2024-10-25

    Xu Zhang, Liao Meng, Chengguang Yang, Tao Bo, Jiazhuang Chen, Yan Guo, Jipan Yu, Lin Wang, Kong‐Qiu Hu, Wei‐Qun Shi, Meng Zhang, Lei Mei

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  40. Thermodynamics of RbF-UF4: a potential fuel candidate for molten salt reactors

    The Journal of Chemical Thermodynamics · 2026-03-06

    Joshua Findlay, Patrice Chartrand, David Cheneler, David Leblanc, Claude André Degueldre

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  41. Rich Chemical Behavior and Topological Variation in Uranium Phosphates via Flux Growth under an Inert Atmosphere

    Inorganic Chemistry · 2026-03-23

    Hui-ye Zhang, Xu Zhang, Kong-qiu Hu, Wei Jin, Tao Bo, Li-yong Yuan, Wei‐Qun Shi, Meng Zhang, Lei Mei, Jing-jing Dong

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