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RESEARCH PAPER · Inorganic Chemistry · 2018

Complex Topologies from Simple Building Blocks: Uranium(IV) Thiophosphates

Vladislav V. Klepov, Hans‐Conrad zur Loye

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Complex Topologies from Simple Building Blocks: Uranium(IV) ThiophosphatesOriginalFlux crystal growth, structure, magnetic and optical properties of a family of alkali uranium(IV) phosphates10Ag5U(PS4)3: A Transition-Metal Actinide Phosphochalcogenide3La2USe3S2: A Serendipitously Grown Lanthanide/Actinide Chalcogenide from a Eutectic Halide Flux3Size-Driven Stability of Lanthanide Thiophosphates Grown from an Iodide Flux30Targeted Synthesis of Uranium(IV) Thiosilicates9Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) Properties47One-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth12Nearly Identical but Not Isotypic: Influence of Lanthanide Contraction on Cs2NaLn(PS4)2 (Ln = La–Nd, Sm, and Gd–Ho)23Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux14“Soft” Alkali Bromide and Iodide Fluxes for Crystal Growth36Facile Oxide to Chalcogenide Conversion for Actinides Using the Boron-Chalcogen Mixture Method38Dimensional reduction upon calcium incorporation in Cs 0.3 (Ca 0.3 Ln 0.7 )PS 4 and Cs 0.5 (Ca 0.5 Ln 0.5 )PS 45A series of Rb 4 Ln 2 (P 2 S 6 )(PS 4 ) 2 (Ln = La, Ce, Pr, Nd, Sm, Gd) rare earth thiophosphates with two distinct thiophosphate units [P V S 4 ] 3− and [P IV 2 S 6 ] 4−16Revisiting thiophosphate Pb 3 P 2 S 8 : a multifunctional material combining a nonlinear optical response and photocurrent response23Trends in rare earth thiophosphate syntheses: Rb 3 Ln(PS 4 ) 2 (Ln = La, Ce, Pr), Rb 3−x Na x Ln(PS 4 ) 2 (Ln = Ce, Pr; x = 0.50, 0.55), and RbEuPS 4 obtained by molten flux crystal growth5Transuranium Sulfide via the Boron Chalcogen Mixture Method and Reversible Water Uptake in the NaCuTS3 Family21Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications13Synthesis, Characterization, and Magnetic Properties of Uranium-Containing 2H-Perovskite-Related Sulfides: Ba3MUS6 (M = Mn, Fe, Co, Ni) and Ba3Co0.858(5)Mg0.142(5)US65Formation of uranium disulfide from a uranium thioamidate single-source precursor4Rare Bird: U+5 in Uranium Chalcogenides6Centrosymmetric to noncentrosymmetric structure transition of the RbREP 2 Se 6 (RE = La–Nd, Sm, Ho–Yb) series: crystal growth, magnetic and optical properties4

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  1. Flux crystal growth, structure, magnetic and optical properties of a family of alkali uranium(IV) phosphates

    Journal of Solid State Chemistry · 2018-10-26

    Mohammad Usman, Gregory W. Morrison, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

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  2. Ag5U(PS4)3: A Transition-Metal Actinide Phosphochalcogenide

    Inorganic Chemistry · 2018-12-10

    Adel Mesbah, Jai Prakash, Sébastien Lebègue∥, Jessica C. Beard, Christos D. Malliakas, James A. Ibers

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  3. La2USe3S2: A Serendipitously Grown Lanthanide/Actinide Chalcogenide from a Eutectic Halide Flux

    Journal of Chemical Crystallography · 2019-04-17

    Mohammad Usman, Gregory W. Morrison, Hans‐Conrad zur Loye

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  4. Size-Driven Stability of Lanthanide Thiophosphates Grown from an Iodide Flux

    Inorganic Chemistry · 2019-04-23

    Vladislav V. Klepov, Logan S. Breton, Kristen A. Pace, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  5. Targeted Synthesis of Uranium(IV) Thiosilicates

    Inorganic Chemistry · 2019-06-10

    Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

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  6. Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) Properties

    Inorganic Chemistry · 2019-06-19

    Mohammad Usman, Mark D. Smith, Gregory W. Morrison, Vladislav V. Klepov, Weiguo Zhang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. One-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth

    Crystal Growth & Design · 2019-08-21

    Mohammad Usman, Mark D. Smith, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  8. Nearly Identical but Not Isotypic: Influence of Lanthanide Contraction on Cs2NaLn(PS4)2 (Ln = La–Nd, Sm, and Gd–Ho)

    Inorganic Chemistry · 2020-01-22

    Vladislav V. Klepov, Kristen A. Pace, Logan S. Breton, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  9. Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux

    Frontiers in Chemistry · 2020-02-26

    Timothy Ferreira, Jie Xing, Liurukara D. Sanjeewa, Athena S. Sefat

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  10. “Soft” Alkali Bromide and Iodide Fluxes for Crystal Growth

    Frontiers in Chemistry · 2020-06-26

    Vladislav V. Klepov, Christian A. Juillerat, Kristen A. Pace, Gregory W. Morrison, Hans‐Conrad zur Loye

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  11. Facile Oxide to Chalcogenide Conversion for Actinides Using the Boron-Chalcogen Mixture Method

    Journal of the American Chemical Society · 2020-07-27

    Logan S. Breton, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  12. Dimensional reduction upon calcium incorporation in Cs 0.3 (Ca 0.3 Ln 0.7 )PS 4 and Cs 0.5 (Ca 0.5 Ln 0.5 )PS 4

    CrystEngComm · 2020-12-09

    Vladislav V. Klepov, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  13. A series of Rb 4 Ln 2 (P 2 S 6 )(PS 4 ) 2 (Ln = La, Ce, Pr, Nd, Sm, Gd) rare earth thiophosphates with two distinct thiophosphate units [P V S 4 ] 3− and [P IV 2 S 6 ] 4−

    Dalton Transactions · 2021-01-01

    Ceren Kütahyalı Aslani, Logan S. Breton, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  14. Revisiting thiophosphate Pb 3 P 2 S 8 : a multifunctional material combining a nonlinear optical response and photocurrent response

    Physical Chemistry Chemical Physics · 2021-01-01

    Bingheng Ji, Elizabeth Guderjahn, Kui Wu, Tajamul Hussain Syed, Wei Wei, Bingbing Zhang, Jian Wang

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  15. Trends in rare earth thiophosphate syntheses: Rb 3 Ln(PS 4 ) 2 (Ln = La, Ce, Pr), Rb 3−x Na x Ln(PS 4 ) 2 (Ln = Ce, Pr; x = 0.50, 0.55), and RbEuPS 4 obtained by molten flux crystal growth

    CrystEngComm · 2021-01-01

    Logan S. Breton, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  16. Transuranium Sulfide via the Boron Chalcogen Mixture Method and Reversible Water Uptake in the NaCuTS3 Family

    Journal of the American Chemical Society · 2022-07-21

    Anna A. Berseneva, Vladislav V. Klepov, Koushik Pal, Kelly Seeley, Daniel Koury, Joseph C. Schaeperkoetter, Joshua Wright, Scott T. Misture, Mercouri G. Kanatzidis, Chris M. Wolverton, Artem V. Gelis, Hans‐Conrad zur Loye

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  17. Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications

    Crystal Growth & Design · 2023-07-10

    Anna A. Berseneva, Hans‐Conrad zur Loye

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  18. Synthesis, Characterization, and Magnetic Properties of Uranium-Containing 2H-Perovskite-Related Sulfides: Ba3MUS6 (M = Mn, Fe, Co, Ni) and Ba3Co0.858(5)Mg0.142(5)US6

    Inorganic Chemistry · 2023-10-09

    Logan S. Breton, Gregory W. Morrison, Hans‐Conrad zur Loye

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  19. Formation of uranium disulfide from a uranium thioamidate single-source precursor

    Chemical Science · 2024-01-01

    Sheridon N. Kelly, Dominic R. Russo, Erik T. Ouellette, Debashree Roy, Andrew J. Swift, Michael A. Boreen, Patrick William Smith, Liane M. Moreau, John Arnold, Stefan G. Minasian

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  20. Rare Bird: U+5 in Uranium Chalcogenides

    Chemistry of Materials · 2024-08-12

    Anna A. Berseneva, Vladislav V. Klepov, Habiba Binte Kashem, Alevtina A. Maksimova, Gregory W. Morrison, Joshua Wright, Joseph C. Schaeperkoetter, Scott T. Misture, Hans‐Conrad zur Loye

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  21. Centrosymmetric to noncentrosymmetric structure transition of the RbREP 2 Se 6 (RE = La–Nd, Sm, Ho–Yb) series: crystal growth, magnetic and optical properties

    Dalton Transactions · 2026-01-01

    Habiba Binte Kashem, Abdullah Al Muhit, Hope Eden Smith, Eric A. Gabilondo, P. Shiv Halasyamani, Hans‐Conrad zur Loye

    Read original paper ↗ ·
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