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RESEARCH PAPER · Inorganic Chemistry · 2015

Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties

Jeongho Yeon, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic PropertiesOriginalChemInform Abstract: Trivalent Cation‐Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M: Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in situ Reduction Step, Structures, Optical, and Magnetic Properties.0Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties12Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]13Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides18Hydrothermal Synthesis and Crystal Structure of Hexafluorogallate, Na3GaF69Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation11Na2(UO2)(BO3): An All-Uranium(V) Borate Synthesized under Mild Hydrothermal Conditions18In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)25Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride14Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability3NanMTh6F30: A Large Family of Quaternary Thorium Fluorides83d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials14Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination Polyhedra14Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF510Quaternary cerium( iv ) containing fluorides exhibiting Ce 3 F 16 sheets and Ce 6 F 30 frameworks16Transition-Metal Monofluorophosphate Ba2M2(PO3F)F6 (M = Mn, Co, and Ni): Varied One-Dimensional Transition-Metal Chains and Antiferromagnetism19Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]5Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)3Expansion of the Na3MIII(Ln/An)6F30 Series: Incorporation of Plutonium into a Highly Robust and Stable Framework11Developing Waste Forms for Transuranic Elements: Quaternary Neptunium Fluorides of the Type NaxMNp6F30 (M = Ti, V, Cr, Mn, Fe, Co, Ni, Al, Ga)9A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate0Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Investigations on the EPR parameters and local structures for the substitutional Ti3+ and W5+ centers in stishovite2Exploring the Valence Diversity of Uranium by Flux Growth of Uranium Silicate under Inert Atmosphere6Flux Method Growth and Structural Analysis of Two Tetravalent Uranium Orthophosphate Single Crystals, Cs2UIV(PO4)2 and Isostructural Cs2(UIV0.75CeIV0.25)(PO4)24Rich Chemical Behavior and Topological Variation in Uranium Phosphates via Flux Growth under an Inert Atmosphere0

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  1. ChemInform Abstract: Trivalent Cation‐Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M: Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in situ Reduction Step, Structures, Optical, and Magnetic Properties.

    ChemInform · 2015-04-01

    Jeongho Yeon, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Mild hydrothermal crystal growth of new uranium(IV) fluorides, Na3.13Mg1.43U6F30 and Na2.50Mn1.75U6F30: Structures, optical and magnetic properties

    Journal of Solid State Chemistry · 2015-05-04

    Jeongho Yeon, Mark D. Smith, Joshua H. Tapp, Angela Möller, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Compositional and Structural Versatility in an Unusual Family of anti-Perovskite Fluorides: [Cu(H2O)4]3[(MF6)(M′F6)]

    Inorganic Chemistry · 2016-07-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides

    Inorganic Chemistry Frontiers · 2017-01-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  5. Hydrothermal Synthesis and Crystal Structure of Hexafluorogallate, Na3GaF6

    Journal of Chemical Crystallography · 2017-06-21

    Jeongho Yeon, Hans‐Conrad zur Loye

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  6. Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O

    RSC Advances · 2018-01-01

    Alexander T. Chemey, Joseph M. Sperling, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  7. An Ultrastable Heterobimetallic Uranium(IV)/Vanadium(III) Solid Compound Protected by a Redox-Active Phosphite Ligand: Crystal Structure, Oxidative Dissolution, and First-Principles Simulation

    Inorganic Chemistry · 2018-01-10

    Daxiang Gui, Xing Dai, Tao Zheng, Xiangxiang Wang, Mark A. Silver, Lanhua Chen, Chao Zhang, Juan Diwu, Ruhong Zhou, Zhifang Chai, Shuao Wang

    Read original paper ↗ ·

  8. Na2(UO2)(BO3): An All-Uranium(V) Borate Synthesized under Mild Hydrothermal Conditions

    Inorganic Chemistry · 2018-04-02

    Kristen A. Pace, Vancho Kocevski, S. Karakalos, Gregory W. Morrison, Theodore M. Besmann, Hans‐Conrad zur Loye

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  9. In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect

    Inorganic Chemistry · 2018-05-24

    Jian Hung Lin, Zenghui Yue, Mark A. Silver, Meiying Qie, Xiaomei Wang, Wei Liu, Xiao Lin, Hongliang Bao, Linjuan Zhang, Shuao Wang, Jian‐Qiang Wang

    Read original paper ↗ ·

  10. Breaking a Paradigm: Observation of Magnetic Order in the Purple U(IV) Phosphite: U(HPO3)2

    Inorganic Chemistry · 2018-07-31

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  11. Electronic, Magnetic, and Theoretical Characterization of (NH4)4UF8, a Simple Molecular Uranium(IV) Fluoride

    Inorganic Chemistry · 2018-12-20

    Alexander T. Chemey, Cristian Celis‐Barros, Kevin Huang, Joseph M. Sperling, Cory J. Windorff, Ryan Baumbach, David E Graf, Dayán Páez‐Hernández, Michael Ruf, David E. Hobart, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  12. Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability

    Inorganica Chimica Acta · 2018-12-26

    Qi Liu, Huiqin Yin, Hongliang Bao, Zenghui Yue, Kariem Diefenbach, Zhongfeng Tang, Jian Hung Lin, Jian‐Qiang Wang

    Read original paper ↗ ·

  13. NanMTh6F30: A Large Family of Quaternary Thorium Fluorides

    Crystal Growth & Design · 2018-12-31

    Vladislav V. Klepov, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  14. 3d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials

    Journal of the American Chemical Society · 2019-02-13

    Vladislav V. Klepov, Kristen A. Pace, Stuart Calder, Justin B. Felder, Hans‐Conrad zur Loye

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  15. Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination Polyhedra

    Inorganic Chemistry · 2019-09-16

    Gyanendra B. Ayer, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  16. Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF5

    Inorganic Chemistry · 2019-10-24

    Alexander T. Chemey, Cristian Celis‐Barros, Joseph M. Sperling, Dayán Páez‐Hernández, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  17. Quaternary cerium( iv ) containing fluorides exhibiting Ce 3 F 16 sheets and Ce 6 F 30 frameworks

    Dalton Transactions · 2020-01-01

    Gyanendra B. Ayer, Vladislav V. Klepov, Kristen A. Pace, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  18. Transition-Metal Monofluorophosphate Ba2M2(PO3F)F6 (M = Mn, Co, and Ni): Varied One-Dimensional Transition-Metal Chains and Antiferromagnetism

    Inorganic Chemistry · 2020-03-01

    Bei Zhu, Jianhua Jiang, Tianyu Zhu, Haoming Yang, Yong Jin, Kwang‐Yong Choi, Minfeng Lü

    Read original paper ↗ ·

  19. Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]

    Crystal Growth & Design · 2020-04-07

    Alexander T. Chemey, Joseph M. Sperling, Cory J. Windorff, David E. Hobart, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  20. Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)

    European Journal of Inorganic Chemistry · 2020-04-29

    Benjamin Scheibe, Juliane März, Moritz Schmidt, Thorsten Stumpf, Florian Kraus

    Read original paper ↗ ·

  21. Expansion of the Na3MIII(Ln/An)6F30 Series: Incorporation of Plutonium into a Highly Robust and Stable Framework

    Chemistry - A European Journal · 2020-07-10

    Kristen A. Pace, Vladislav V. Klepov, Travis K. Deason, Mark D. Smith, Gyanendra B. Ayer, David P. DiPrete, Jake Amoroso, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  22. Developing Waste Forms for Transuranic Elements: Quaternary Neptunium Fluorides of the Type NaxMNp6F30 (M = Ti, V, Cr, Mn, Fe, Co, Ni, Al, Ga)

    Journal of the American Chemical Society · 2022-12-19

    Travis K. Deason, Gregory W. Morrison, Amir Mofrad, Hunter B. Tisdale, Jake Amoroso, David DiPrete, Gary S. Was, Kai Sun, Theodore M. Besmann, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  23. A three-dimensional uranium-fluorine spin-frustrated CaB6-type lattice as potential conductive and quantum spin liquid candidate

    Ionics · 2023-05-15

    Li Wang, Jie Qin, Youyuan Ran, Lan Chen

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  24. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

    Inorganic Chemistry · 2023-07-18

    Navindra Keerthisinghe, Gyanendra B. Ayer, Mark D. Smith, Hans‐Conrad zur Loye

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  25. Investigations on the EPR parameters and local structures for the substitutional Ti3+ and W5+ centers in stishovite

    Zeitschrift für Naturforschung A · 2024-02-08

    Chen Fu, Zifa Zhou, Jin Zhang, Cuidi Feng

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  26. Exploring the Valence Diversity of Uranium by Flux Growth of Uranium Silicate under Inert Atmosphere

    Inorganic Chemistry · 2024-03-02

    Xu Zhang, Tao Bo, Zhi‐wei Huang, Zhiheng Zhou, Kong‐Qiu Hu, Wei‐Qun Shi, Lei Mei

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  27. Flux Method Growth and Structural Analysis of Two Tetravalent Uranium Orthophosphate Single Crystals, Cs2UIV(PO4)2 and Isostructural Cs2(UIV0.75CeIV0.25)(PO4)2

    Inorganic Chemistry · 2024-09-05

    Yu Wang, Xiaochen Zhang, Lanxin Li, Tao Bo, Lei Zhang

    Read original paper ↗ ·

  28. Rich Chemical Behavior and Topological Variation in Uranium Phosphates via Flux Growth under an Inert Atmosphere

    Inorganic Chemistry · 2026-03-23

    Hui-ye Zhang, Xu Zhang, Kong-qiu Hu, Wei Jin, Tao Bo, Li-yong Yuan, Wei‐Qun Shi, Meng Zhang, Lei Mei, Jing-jing Dong

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