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RESEARCH PAPER · Inorganic Chemistry · 2018

Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) Fluorides

Vladislav V. Klepov, Justin B. Felder, Hans‐Conrad zur Loye

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Synthetic Strategies for the Synthesis of Ternary Uranium(IV) and Thorium(IV) FluoridesOriginalExpanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O12Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates7Supramolecular interaction-induced assemblies of polyanions and 2-aminopyridinium in two polyoxometalate-based hybrids3Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability3NanMTh6F30: A Large Family of Quaternary Thorium Fluorides8Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides493d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials14UF4 and the High‐Pressure Polymorph HP‐UF45Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination Polyhedra14The low-temperature barium fluoridozirconate variety α-BaZr2F101Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF510Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis12Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]5Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)3Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)8A Molecular Octafluoridoneptunate(IV) Anion in (NH4)4[NpF8] and Theoretical Investigations of the [MF8]4– System (M = Th – Bk)3Preparation, thermal stability and crystal structure of Li3UF7: New insights into LiF-UF4 binary phase diagram3A Geometrically Frustrated Family of MIIMIIIF5(H2O)2 Mixed–Metal Fluorides with Complex Magnetic Interactions14Uranium: The Nuclear Fuel Cycle and Beyond107Developing Waste Forms for Transuranic Elements: Quaternary Neptunium Fluorides of the Type NaxMNp6F30 (M = Ti, V, Cr, Mn, Fe, Co, Ni, Al, Ga)9Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Crystal Growth and Characterization of the Rare Earth Fluoride Carbonates NaLnCO3F2 (Ln = Eu–Lu)5Improvement of Single-Crystal Structures of Very Heavy Element Compounds by Refining Anomalous Dispersion Parameters3From Magnetic Chains to Sheets: The Impact of Hydrofluoric Acid Quantities in Mild Hydrothermal Synthesis on Mixed-Metal Fluoride Formation2

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24 direct citing papers saved.

  1. Expanding pentafluorouranates: hydrothermal synthesis and characterization of β-NaUF 5 and β-NaUF 5 ·H 2 O

    RSC Advances · 2018-01-01

    Alexander T. Chemey, Joseph M. Sperling, Thomas E. Albrecht‐Schmitt

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  2. Retention of a Paramagnetic Ground State at Low Temperatures in a Family of Structurally Related UIV Phosphates

    Inorganic Chemistry · 2018-07-17

    Justin B. Felder, Stuart Calder, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Supramolecular interaction-induced assemblies of polyanions and 2-aminopyridinium in two polyoxometalate-based hybrids

    Acta Crystallographica Section C Structural Chemistry · 2018-10-18

    Fengxue Duan, Xiaoting Liu, Wei Xu, Yanchun Tao, Bao Li, Lixin Wu

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  4. Insights into the new 3d–5f heterometallic quaternary fluorides: Synthesis, crystal structures, spectroscopic properties, and thermodynamic stability

    Inorganica Chimica Acta · 2018-12-26

    Qi Liu, Huiqin Yin, Hongliang Bao, Zenghui Yue, Kariem Diefenbach, Zhongfeng Tang, Jian Hung Lin, Jian‐Qiang Wang

    Read original paper ↗ ·

  5. NanMTh6F30: A Large Family of Quaternary Thorium Fluorides

    Crystal Growth & Design · 2018-12-31

    Vladislav V. Klepov, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  6. Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides

    Dalton Transactions · 2019-01-01

    Christian A. Juillerat, Vladislav V. Klepov, Gregory W. Morrison, Kristen A. Pace, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. 3d-Metal Induced Magnetic Ordering on U(IV) Atoms as a Route toward U(IV) Magnetic Materials

    Journal of the American Chemical Society · 2019-02-13

    Vladislav V. Klepov, Kristen A. Pace, Stuart Calder, Justin B. Felder, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  8. UF4 and the High‐Pressure Polymorph HP‐UF4

    Chemistry - A European Journal · 2019-03-26

    Benjamin Scheibe, Jörn Bruns, Günter Heymann, Malte Sachs, Antti J. Karttunen, Clemens Pietzonka, Sergei I. Ivlev, Hubert Huppertz, Florian Kraus

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  9. Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination Polyhedra

    Inorganic Chemistry · 2019-09-16

    Gyanendra B. Ayer, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  10. The low-temperature barium fluoridozirconate variety α-BaZr2F10

    Acta Crystallographica Section C Structural Chemistry · 2019-10-04

    Jean Paul Laval

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  11. Structure, Spectroscopy, and Theoretical Analysis of Zero- and Three-Dimensional Lithium Plutonium Fluorides: Li4PuF8 and LiPuF5

    Inorganic Chemistry · 2019-10-24

    Alexander T. Chemey, Cristian Celis‐Barros, Joseph M. Sperling, Dayán Páez‐Hernández, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  12. Examination of Molten Salt Reactor Relevant Elements Using Hydrothermal Synthesis

    Inorganic Chemistry · 2020-03-26

    Cory J. Windorff, Alexander T. Chemey, Joseph M. Sperling, Bonnie E. Klamm, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  13. Structural Relationships and Absorption Spectroscopy of β-[NH4][UF5] and [NH4][Pu3F13]

    Crystal Growth & Design · 2020-04-07

    Alexander T. Chemey, Joseph M. Sperling, Cory J. Windorff, David E. Hobart, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  14. Synthesis and Crystal Structures of Transition Metal(II) Fluoridometallate(IV) Hydrates of Neptunium and Plutonium: AIIMIVF6·3H2O (AII = Mn, Zn; MIV = Np, Pu)

    European Journal of Inorganic Chemistry · 2020-04-29

    Benjamin Scheibe, Juliane März, Moritz Schmidt, Thorsten Stumpf, Florian Kraus

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  15. Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)

    Solid State Sciences · 2020-08-07

    Navindra Keerthisinghe, Vladislav V. Klepov, Eric Zhang, Mark D. Smith, Shani Egodawatte, Stephen H. Foulger, Hans‐Conrad zur Loye

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  16. A Molecular Octafluoridoneptunate(IV) Anion in (NH4)4[NpF8] and Theoretical Investigations of the [MF8]4– System (M = Th – Bk)

    European Journal of Inorganic Chemistry · 2020-09-24

    Benjamin Scheibe, Michael Patzschke, Juliane März, Matthias Conrad, Florian Kraus

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  17. Preparation, thermal stability and crystal structure of Li3UF7: New insights into LiF-UF4 binary phase diagram

    Journal of Alloys and Compounds · 2020-12-03

    Siddhartha Kolay, Srungarpu Nagabhusan Achary, Anil Bhimrao Shinde, P. Siva Ram Krishna, Manidipa Basu, Ratikant Mishra, A. K. Tyagi

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  18. A Geometrically Frustrated Family of MIIMIIIF5(H2O)2 Mixed–Metal Fluorides with Complex Magnetic Interactions

    Inorganic Chemistry · 2021-09-01

    Navindra Keerthisinghe, Anna A. Berseneva, Vladislav V. Klepov, Gregory W. Morrison, Hans‐Conrad zur Loye

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  19. Uranium: The Nuclear Fuel Cycle and Beyond

    International Journal of Molecular Sciences · 2022-04-22

    Bárbara Maria Teixeira Costa Peluzo, Elfi Kraka

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  20. Developing Waste Forms for Transuranic Elements: Quaternary Neptunium Fluorides of the Type NaxMNp6F30 (M = Ti, V, Cr, Mn, Fe, Co, Ni, Al, Ga)

    Journal of the American Chemical Society · 2022-12-19

    Travis K. Deason, Gregory W. Morrison, Amir Mofrad, Hunter B. Tisdale, Jake Amoroso, David DiPrete, Gary S. Was, Kai Sun, Theodore M. Besmann, Hans‐Conrad zur Loye

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  21. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

    Inorganic Chemistry · 2023-07-18

    Navindra Keerthisinghe, Gyanendra B. Ayer, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  22. Crystal Growth and Characterization of the Rare Earth Fluoride Carbonates NaLnCO3F2 (Ln = Eu–Lu)

    Crystal Growth & Design · 2024-08-06

    Navindra Keerthisinghe, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  23. Improvement of Single-Crystal Structures of Very Heavy Element Compounds by Refining Anomalous Dispersion Parameters

    Inorganic Chemistry · 2024-08-08

    Florian Meurer, Gregory W. Morrison, Birgit Hischa, Hans‐Conrad zur Loye, Christoph Hennig, Michael Bodensteiner

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  24. From Magnetic Chains to Sheets: The Impact of Hydrofluoric Acid Quantities in Mild Hydrothermal Synthesis on Mixed-Metal Fluoride Formation

    Chemistry of Materials · 2025-02-18

    Navindra Keerthisinghe, Gregory W. Morrison, Logan S. Breton, Mark D. Smith, Qiang Zhang, Melanie Kirkham, Vladislav V. Klepov, Hans‐Conrad zur Loye

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